SAE AMS 2980 4B-2014 Carbon Fiber Fabric and Epoxy Resin Wet Lay-Up Repair Material Part 4 - Purchasing Specification - Resin《技术规范 碳纤维织物和环氧树脂湿浸渍增强修复材料采购规范 树脂》.pdf

1、_SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising theref

2、rom, is the sole responsibility of the user.”SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions.Copyright 2014 SAE InternationalAll rights reserved. No part of this publi

3、cation may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE.TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada)Tel: +1 724-776-4970 (out

4、side USA)Fax: 724-776-0790Email: CustomerServicesae.orgSAE WEB ADDRESS: http:/www.sae.orgSAE values your input. To provide feedbackon this Technical Report, please visithttp:/www.sae.org/technical/standards/AMS2980/4BAEROSPACE MATERIAL SPECIFICATIONAMS2980/4 REV. BIssued 1996-11Revised 2014-04Supers

5、eding AMS2980/4ACarbon Fiber Fabric and Epoxy Resin Wet Lay-Up Repair MaterialPart 4 - Purchasing Specification - ResinRATIONALEAMS2980/4B is a Five Year Review and update of this specification.FOREWORDThis Purchasing Specification (PS) is part of the Technical Specification system described in AMS2

6、980.TABLE OF CONTENTS1. SCOPE 21.1 Limitation. 22. APPLICABLE DOCUMENTS 22.1 SAE Publications. 22.2 ASTM Publications 22.3 EN Publications . 22.4 ISO Publications 32.5 PRI Publications 33. DEFINITIONS . 34. REQUIREMENTS . 35. RELEASE TESTING . 35.1 Test Report . 35.2 Manufacturer Additional Inspecti

7、on. 45.2.1 Conformance to Weight 45.2.2 Inspection of Packaging 45.3 Retest 45.4 Rejection . 45.5 Sampling . 46. PREPARATION FOR DELIVERY . 46.1 Packing 46.2 Marking 46.3 Storage and Shipment. 57. NOTES 5TABLE OF TABLESTABLE 1 - Batch Release Tests for Resin Systems 3SAE INTERNATIONAL AMS2980/4B Pag

8、e 2 of 51. SCOPEThis PS, AMS2980/4, specifies the batch release and delivery requirements for epoxy resin systems (base resin and curing agent) used for wet lay-up repair purposes.1.1 LimitationThis specification relates to qualified epoxy resin systems listed in the associated PRI QPL AMS2980.2. AP

9、PLICABLE DOCUMENTSThe issue of the following documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced docume

10、nt has been cancelled and no superseding document has been specified, the last published issue of that document shall apply.2.1 SAE PublicationsAvailable from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA)

11、, www.sae.org.AMS2980 Technical Specification: Carbon Fiber Fabric and Epoxy Resin Wet Lay-Up Repair Material Part 0 IntroductionAMS2980/1 Technical Specification: Carbon Fiber Fabric and Epoxy Resin Wet Lay-Up Repair Material Part 1 -General Requirements2.2 ASTM PublicationsAvailable from ASTM Inte

12、rnational, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org.ASTM D 1652 Standard Test Method for Epoxy Content of Epoxy ResinsASTM D 2471 Standard Test Method for Gel Time and Peak Exothermic Temperature of Reacting Thermosetting ResinsASTM D 28

13、96 Total Base Number of Petroleum Products by Potentiometric Perchloric Acid TitrationASTM E 203 Standard Test Method for Water Using Volumetric Karl Fischer TitrationASTM E 1252 Standard Practice for General Techniques for Qualitative Infrared Analysis2.3 EN PublicationsAvailable from CEN-Comit Eur

14、open de Normalisation, Secretariat Central, Rue de Stassart 36, B-1050 Bruxelles, Belgium or www.cenorm.be.EN 6042 Aerospace Series: Analysis of Organic Compounds by Infrared SpectroscopySAE INTERNATIONAL AMS2980/4B Page 3 of 52.4 ISO PublicationsAvailable from International Organization for Standar

15、dization, 1, rue de Varembe, Case postale 56, CH-1211 Geneva 20, Switzerland, Tel: +41 22 749 01 11, www.iso.org.ISO 760 Determination of Water. Karl Fischer Method (General Method) First EditionISO 2555 Plastics - Resins in the Liquid State or as Emulsions or Dispersions - Determination of Apparent

16、 Viscosity by the Brookfield Test MethodISO 3001 Plastics - Epoxy Compounds - Determination of Epoxy Equivalent2.5 PRI PublicationsAvailable from Performance Review Institute, 161 Thornhill Road, Warrendale PA 15086-7527, Tel: 724-772-1616, www.pri-network.orgPRI QPL AMS2980 Qualified product list o

17、f AMS29803. DEFINITIONSRefer to AMS2980/1.4. REQUIREMENTSThe resin system to be delivered shall meet the general requirements in accordance with AMS2980/1 and the requirements of this PS and the relevant Appendix of PRI QPL AMS2980 of the material to be purchased.5. RELEASE TESTING5.1 Test ReportThe

18、 resin manufacturer shall test each resin batch in accordance with Table 1 and the sampling plan in paragraph 5.5. The manufacturer shall provide the purchaser with a test report certifying that the resin batch meets the requirements of Section 4.TABLE 1 - BATCH RELEASE TESTS FOR RESIN SYSTEMSProper

19、ty Test Method1RemarksEpoxide Equivalent ASTM D 1652 or ISO 3001 Base resinAmine Value ASTM D 2896 Curing agentIR Spectrum (qualitatively) EN 6042 or ASTM E 1252 Base resin and curing agentWater Content ASTM E 203 or ISO 760 Base resin and curing agent2Viscosity at 25 C ISO 2555 Base resin and curin

20、g agentGel Time at 25 C ASTM D 2471 Blending ratio is specified in the relevant Appendix of PRI QPL AMS29801Use test methods specified in the relevant Appendix of PRI QPL AMS2980. Use three samples per test.2If required by the relevant Appendix of PRI QPL AMS2980.The resin release test report shall

21、contain at least the following:a. Specification numberb. Manufacturers resin batch number and production datec. Manufacturers identificationd. Test resultsSAE INTERNATIONAL AMS2980/4B Page 4 of 5The purchaser reserves the right to perform any of the inspections and/or tests required by this specific

22、ation and may reject any material which fails to meet the requirements.5.2 Manufacturer Additional Inspection5.2.1 Conformance to WeightThe base resin and curing agent shall be inspected for conformance to paragraph 6.2 h.5.2.2 Inspection of PackagingThe manufacturer shall perform inspections as nec

23、essary to assure that the packaging, packing, preservation and shipment requirements are in accordance with Section 6.5.3 RetestThis section specifies batch release retest by the resin manufacturer. If a sample unit fails to meet the requirements of this specification and/or the relevant Appendix of

24、 PRI QPL AMS2980, a review of all test results, test procedures, test equipment, specimen manufacturing and test specimen(s) shall be performed. If a cause for the deviation is found, a retest of the property that has failed shall be performed.New samples may be taken from different containers and t

25、he resin shall be retested one time.The results of the original test, together with those of the retest and the reasons for the first failure, shall be included in the resin release test report.5.4 RejectionAny failure of the resin system to meet the batch release requirements of this specification

26、shall be cause for rejection.5.5 SamplingThe sampling plan for batch release testing shall be specified in the relevant Appendix of PRI QPL AMS2980. This sampling plan shall be a part of the PCD.6. PREPARATION FOR DELIVERY6.1 PackingThe base resin and curing agent shall be packaged in containers dif

27、ferent in size and/or form to minimize risk of erroneous exchange.6.2 MarkingThe base resin and curing agent containers shall be legibly and durably marked in such a manner and location that it remains in place until all material has been used.Markings shall include but not be limited to the followi

28、ng information:a. Specification numberb. Resin manufacturer namec. Resin manufacturers identificationd. Resin manufacturers batch numbere. Date of manufacturingSAE INTERNATIONAL AMS2980/4B Page 5 of 5f. Expiration date of unopened containers at room temperature and at 5 Cg. Manufacturing planth. Qua

29、ntity in the package6.3 Storage and ShipmentUpon delivery, store the base resin and curing agent in accordance with the relevant Appendix of PRI QPL AMS2980. Transportation shall not affect the storage life as defined in the relevant Appendix of PRI QPL AMS2980.The responsibility for shipping shall

30、be agreed to between the purchaser and material manufacturer.Storage life extension procedures may be described in the relevant Appendix of PRI QPL AMS2980.7. NOTES7.1 A change bar (|) located in the left margin is for the convenience of the user in locating areas where technical revisions, not edit

31、orial changes, have been made to the previous issue of this document. An (R) symbol to the left of the document title indicates a complete revision of the document, including technical revision. Change bars and (R) are not used in original publications, nor in documents that contain editorial changes only.PREPARED BY ATA/IATA/SAE COMMERCIAL AIRCRAFT COMPOSITE REPAIR COMMITTEE