SAE AMS 3021E-2017 Fluid Reference for Testing Di-Ester (Polyol) Resistant Material.pdf

1、 _ SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising ther

2、efrom, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions. Copyright 2017 SAE International All rights reserved. No part of this

3、publication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-49

4、70 (outside USA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/standards.sae.org/AMS3021E AEROSPACE MATERIAL SPECIFICATION AMS3021 REV. E Issued 1979-08 Reaffirmed 2004-03 Rev

5、ised 2017-04 Superseding AMS3021D Fluid, Reference for Testing Di-Ester (Polyol) Resistant Material RATIONALE Revised to include the addition of a recommended substitute fluid. 1. SCOPE 1.1 Form This specification covers a neopentyl polyol ester fluid. 1.2 Application This fluid has been used typica

6、lly to evaluate the ability of elastomeric and other polymeric compounds to conform to designated requirements after immersion in the fluid at a specific temperature and time, as required by an applicable specification, and its use is limited to such applications. This fluid is not intended for oper

7、ational use in gas turbine engines (see 8.2). Each application should be considered separately. 1.3 Safety - Hazardous Materials While the materials, methods, applications, and processes described or referenced in this specification may involve the use of hazardous materials, this specification does

8、 not address the hazards which may be involved in such use. It is the sole responsibility of the user to ensure familiarity with the safe and proper use of any hazardous materials and to take necessary precautionary measures to ensure the health and safety of all personnel involved. SAE INTERNATIONA

9、L AMS3021E Page 2 of 5 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specifie

10、d. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that document shall apply. 2.1 SAE Publications Available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada

11、) or +1 724-776-4970 (outside USA), www.sae.org. AMS2825 Material Safety Data Sheets 2.2 ASTM Publications Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM D445 Kinematic Viscosity of Transparent and Opaq

12、ue Liquids (and the Calculation of Dynamic Viscosity) ASTM D664 Neutralization Number by Potentiometric Titration ASTM D1218 Refractive Index and Refractive Dispersion of Hydrocarbon Liquids ASTM D1298 Density, Relative Density (Specific Gravity), or API Gravity of Crude Petroleum and Liquid Petrole

13、um Products by Hydrometer Method ASTM D1744 Water in Liquid Petroleum Products by Karl Fischer Reagent ASTM D4057 Manual Sampling of Petroleum and Petroleum Products 2.3 U.S. Government Publications Copies of these documents are available online at http:/quicksearch.dla.mil. MIL-PRF-23699 Lubricatin

14、g Oil, Aircraft Turbine Enginer, Synthetic Base, NATO Code Numbers: O-152, O-154, O-56, and O-167 3. TECHNICAL REQUIREMENTS 3.1 Material Test fluid shall consist of a refined product of neopentyl ester with 0.5% phenothiazine added as an antioxidant. 3.2 Properties The product shall conform to the r

15、equirements shown in Table 1; tests shall be performed on the fluid supplied and in accordance with specified test methods. SAE INTERNATIONAL AMS3021E Page 3 of 5 Table 1 - Properties Paragraph Property Requirement Test Method 3.2.1 Specific Gravity at 60/60 F (16/16 C) 0.961 to 0.967 ASTM D1298 3.2

16、2 Viscosity at 100 F (38 C) 14.60 to 15.60 cst ASTM D445 3.2.3 Viscosity at 210 F (99 C) 3.0 to 4.0 cst ASTM D445 3.2.4 Acid Number, Max 0.10 mg KOH/g ASTM D664 3.2.5 Water Content by weight, Max 0.10% ASTM D1744 3.2.6 Refractive Index at 73 F (23 C) 1.449 to 1.455 ASTM D1218 3.2.7 C7 Acid Componen

17、t, Min 93% 4.5 3.2.8 Hydroxyl Content, Max 0.1% 4.5 3.3 Quality The fluid, as received by purchaser, shall be free from water, sediment, and suspended matter. The odor shall not be irritating or nauseating. No substance of known toxicity under normal conditions of handling and use shall be present.

18、4. QUALITY ASSURANCE PROVISIONS 4.1 Responsibility for Inspection The manufacturer of fluid shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the fluid conforms to specified r

19、equirements. 4.2 Classification of Tests All technical requirements are acceptance tests and shall be performed prior to shipment of fluid by the manufacturer. 4.3 Sampling and Testing Shall be in accordance with ASTM D4057. The number of determinations for each requirement shall be as specified in

20、the applicable test procedure or, if not specified therein, not less than three. 4.3.1 A lot shall be all fluid from one batch presented for manufacturers inspection at one time. 4.3.2 When a statistical sampling plan has been agreed upon by purchaser and supplier, sampling shall be in accordance wi

21、th such plan in lieu of sampling as in 4.3 and the report of 4.6 shall state that such plan was used. 4.4 Approval If requested by purchaser, sample fluid shall be submitted for approval by the purchaser before fluid for production use is supplied. If necessary to make any change in ingredients, in

22、type of equipment for processing, or in manufacturing procedures, manufacturer shall submit for reapproval a statement of the proposed changes in ingredients and/or processing and, when requested, sample fluid (see 8.5). Production fluid made by the revised procedure shall not be shipped prior to re

23、ceipt of approval. 4.5 Test Methods Shall be as agreed upon by purchaser and manufacturer for determining the C7 acid component (3.2.7) and hydroxyl content (3.2.8). SAE INTERNATIONAL AMS3021E Page 4 of 5 4.6 Reports The supplier of fluid shall furnish with each shipment a report from the manufactur

24、er, showing the results of tests to determine conformance to the technical requirements. This report shall include the purchase order number, lot number, AMS3021E, manufacturers identification, and quantity. 4.6.1 A material safety data sheet conforming to AMS2825, or equivalent, shall be supplied t

25、o each purchaser prior to, or with the first shipment of fluid. 4.7 Resampling and Retesting If any sample used in the above tests fails to meet the specified requirements, disposition of the fluid may be based on the results of testing three additional samples for each original nonconforming sample

26、 Failure of any retest sample to meet the specified requirements shall be cause for rejection of the fluid represented. Results of all tests shall be reported. 5. PREPARATION FOR DELIVERY 5.1 Packaging and Identification 5.1.1 A lot of fluid may be packaged in small quantities and delivered under t

27、he basic lot approval provided lot identification is maintained. 5.1.2 The fluid shall be packaged in airtight containers of such size and design as to keep ullage to a minimum. 5.1.3 Each container of fluid shall be legibly identified, with not less than the following information on an attached lab

28、el, using characters which will not be obliterated by normal handling: FLUID, REFERENCE, FOR TESTING DI-ESTER (POLYOL) RESISTANT MATERIAL AMS3021E PURCHASE ORDER NUMBER MANUFACTURERS IDENTIFICATION LOT (OR BATCH) NUMBER QUANTITY APPROPRIATE WARNINGS OR PRECAUTIONARY NOTICES 5.1.4 Containers of fluid

29、 shall be prepared for shipment in accordance with commercial practice and in compliance with applicable rules and regulations pertaining to the handling, packaging and transportation of the fluid to ensure carrier acceptance and safe delivery. 6. ACKNOWLEDGMENT A supplier shall mention this specifi

30、cation number and its revision letter in all quotations and when acknowledging purchase orders. 7. REJECTIONS Fluid not conforming to this specification, or to modifications authorized by purchaser, will be subject to rejection. SAE INTERNATIONAL AMS3021E Page 5 of 5 8. NOTES 8.1 Revision Indicator

31、A change bar (l) located in the left margin is for the convenience of the user in locating areas where technical revisions, not editorial changes, have been made to the previous issue of this document. An (R) symbol to the left of the document title indicates a complete revision of the document, inc

32、luding technical revisions. Change bars and (R) are not used in original publications, nor in documents that contain editorial changes only. 8.2 This fluid is intended for use in evaluating the response of materials in contact with, or immersion in, MIL-PRF-7808 and similar lubricants. 8.3 This flui

33、d is also known Hatco 7700 and can be purchased from: Hatco Corporation Domestic Order Desk Attention: Loretta Gimbert Phone: 1 732 738 3600 Fax: 1 732 738 9385 Email: 8.4 Terms used in AMS are clarified in ARP1917. 8.5 Dimensions and properties in inch/pound units and the Fahrenheit temperatures a

34、re primary; dimensions and properties in SI units and the Celsius temperatures are shown as the approximate equivalents of the primary units and are presented only for information. 8.6 Purchase documents should specify not less than the following: AMS3021E Size of containers desired Quantity of fluid desired Special packaging, if required 8.7 Mobil Jet Oil II (O-1D) per MIL-PRF-23699 is an acceptable substitute should AMS3021 become commercially unavailable for purchase. PREPARED BY AMS COMMITTEE “CE”