SAE AMS 3046F-2009 Magnetic Particles Fluorescent Wet Method Oil Vehicle Aerosol Packaged《气溶胶包装的以油为媒介物的荧光磁性粒子用湿方法》.pdf

1、AEROSPACE MATERIAL SPECIFICATION AMS3046 REV. F Issued 1974-03 Revised 2009-04 Reaffirmed 2014-12 Superseding AMS3046E Magnetic Particles, Fluorescent Wet Method, Oil Vehicle, Aerosol Packaged RATIONALE AMS3046F has been reaffirmed to comply with the SAE five-year review policy. _ SAE Technical Stan

2、dards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising therefrom, is the sole re

3、sponsibility of the user.” SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions. Copyright 2014 SAE International All rights reserved. No part of this publication may be re

4、produced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-4970 (outside USA) Fax:

5、 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/www.sae.org/technical/standards/AMS3046F 1. SCOPE 1.1 Form This specification covers one type of fluorescent magnetic particles in th

6、e form of a mixed, ready-to-use suspension in an odorless, inspection oil vehicle and packaged in aerosol cans. 1.2 Application This product has been used typically as the inspection medium in a wet, fluorescent magnetic particle inspection system as defined in AMS2640 or ASTM E 1444, but usage is n

7、ot limited to such applications. 1.3 Safety - Hazardous Materials While the materials, methods, applications, and processes described or referenced in this specification may involve the use of hazardous materials, this specification does not address the hazards which may be involved in such use. It

8、is the sole responsibility of the user to ensure familiarity with the safe and proper use of any hazardous materials and to take necessary precautionary measures to ensure the health and safety of all personnel involved. 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the d

9、ate of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the

10、 last published issue of that document shall apply. 2.1 SAE Publications Available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.org. AMS2640 Magnetic Particle Inspection AMS2641 Vehicle, Ma

11、gnetic Particle Inspection, Petroleum Base AMS2820 Packaging, Aerosol AMS3044 Magnetic Particles, Fluorescent, Wet Method, Dry Powder AS5282 Tool Steel Ring for Magnetic Particle Inspection 2.2 ASTM Publications Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohock

12、en, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM D 1966 Test Method for Foots in Raw Linseed Oil (Gravimetric Method) ASTM E 1444 Magnetic Particle Testing 3. TECHNICAL REQUIREMENTS 3.1 Material The product shall be composed of durable fluorescent magnetic particles, which have been dyed or

13、otherwise treated to attain the color specified. The particles shall be supplied mixed in the proper proportion with an inspection vehicle and packaged in aerosol cans. 3.1.1 Fluorescent magnetic particles shall conform to AMS3044. 3.1.2 Magnetic particle inspection vehicle shall conform to AMS2641.

14、 3.2 Storage Life The product shall meet the requirements of 3.3 when tested at any time up to 12 months from date of manufacture. 3.3 Properties The product shall conform to the following requirements; tests shall be performed on the product supplied in accordance with specified test methods, using

15、 a test suspension prepared by spraying the complete contents of several aerosol cans into a clean container to produce at least 1 quart (1 L) of suspension, agitating the aerosol cans frequently to exhaust all particulate material: 3.3.1 Contamination The product shall show no evidence of foreign m

16、aterial, agglomeration, or scum, determined by visual examination of the test suspension at the following times: 3.3.1.1 During preparation of the test suspension as in 3.3. 3.3.1.2 After mixing the test suspension, allowing it to stand for not less than 30 minutes, and agitating it slightly. 3.3.1.

17、3 During tests to determine other characteristics of the product. _ SAE INTERNATIONAL AMS3046F Page 2 of 63.3.2 Concentration The concentration of fluorescent magnetic particles in the freshly-sprayed suspension shall be 0.15 to 0.30 mL of fluorescent magnetic particles in 100 mL of suspension, dete

18、rmined by mixing the test suspension thoroughly, filling a 100 mL calibrated centrifuge tube as specified in ASTM D 1966, allowing it to stand undisturbed for at least 30 minutes, and reading, on the calibrated tube, the volume of the particles settled from the suspension. 3.3.3 Sensitivity 3.3.3.1

19、Ring Test The product shall provide a seven-hole indication on the ring test specimen defined in AS5282, determined by placing the ring on a 1-inch (25-mm) diameter copper bar and circularly magnetizing the ring in a standard magnetic particle inspection unit by passing 2500 amperes of direct curren

20、t through the bar immediately before flushing the ring with the agitated test suspension that has passed the contamination (3.3.1) and concentration (3.3.2) tests. Examine the ring in a darkened area under UV-A illumination of at least 1000 W/cm2at the inspection surface. Visible light shall not exc

21、eed 2 foot-candles (20 lux) at the inspection surface. 3.3.3.2 Flaw-to-Background Test Obtain a test part, or prepare a test specimen, containing flaws of the size expected to be found in routine inspection. The surface finish of the test specimen shall be representative of production parts. Magneti

22、ze and flush the specimen as specified in 3.3.3.1, using a sample of agitated test suspension that has passed the contamination (3.3.1) and concentration (3.3.2) tests. View the flaw indications in a darkened area under ultraviolet light as defined in 3.3.3.1. Indications shall be sharp and distinct

23、 Background fluorescence around the flaws shall be of a level which will neither obscure the flaw indications nor cause difficulty in flaw detection. 3.4 Aerosol Spray Cans The aerosol cans selected for test shall be maintained at room temperature for not less than 12 hours prior to testing. During

24、 testing, the aerosol can may be immersed in water at 77 F 2 (25 C 1) periodically to maintain the container and its contents at room temperature. 3.4.1 Sprayability and Leakage 3.4.1.1 All aerosol pressure cans shall be equipped with a spray nozzle. The nozzle shall provide a fine, steady spray and

25、 shall deposit the product evenly on a flat or vertical surface. No chunks of solids shall be expelled and no clogging of the nozzle shall occur. 3.4.1.2 The characteristics of the spray pattern and the performance of the spray nozzle shall be evaluated by vigorously shaking the can for not less tha

26、n 30 seconds with the contained pellet sounding on each shake and spraying a pattern on large sheets of newspaper or a similar surface to determine the coverage and evenness of the spray. After spraying several patterns, the nozzle shall be examined for evidence of chunks or solids and clogging. The

27、 can shall then be immersed for not less than 15 minutes in water at 126 to 129 F (52 to 54 F); there shall be no visible evidence of leakage from, or distortion of, the pressurized container. The pressurized can shall then be immersed in water at 77 F 2 (25 C 1) until the temperature has stabilized

28、 and, after vigorous shaking, two more patterns shall be sprayed. The spray characteristics shall have not changed and there shall be no chunking of particles or clogging of the nozzle. 3.4.1.2.1 CAUTION: DO NOT HEAT THE PRESSURIZED CAN OVER 129 F (54 C). _ SAE INTERNATIONAL AMS3046F Page 3 of 63.4.

29、2 Complete Expulsion The complete usable portion of the contents shall have been expelled before the propellant is expended. The expelled contents shall be not less than 5 fluid ounces (50 mL) and the particle content shall conform to the aerosol spray requirements. Vigorously shake for not less tha

30、n 30 seconds each unused can to be tested, with the contained pellet sounding on each shake, and expel the contents in a series of short blasts into a clean glass container graduated in ounces (mL) in such a manner that the entire contents of the can will be retained in the glass container. The aero

31、sol can may be immersed periodically in water at 77 F 2 (25 C 1) to maintain the can and its contents at room temperature. Repeat the vigorous shaking and short blasts until there is no further escape of gas. 4. QUALITY ASSURANCE PROVISIONS 4.1 Responsibility for Inspection The vendor of the product

32、 shall supply all samples for vendors tests and shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the product conforms to the specified requirements. 4.2 Classification of Tes

33、ts 4.2.1 Acceptance Tests All technical requirements of this specification, except storage life (3.2), are acceptance tests and shall be performed on each lot. 4.2.2 Preproduction Tests All technical requirements of this specification are preproduction tests and shall be performed prior to or on the

34、 initial shipment of product to a purchaser, when a change in material and/or processing requires reapproval as in 4.4.2, and when purchaser deems confirmatory testing to be required. 4.3 Sampling and Testing Shall be as follows: 4.3.1 For Acceptance Tests Sufficient product shall be taken at random

35、 from each lot to perform all required test. The number of determinations for each requirement shall be as specified in the applicable test procedure or, if not specified therein, not less than three. 4.3.1.1 A lot shall be all product produced in a single production run from the same batches of raw

36、 materials under the same fixed conditions and presented for vendors inspection at one time. A lot may be packaged in smaller quantities and delivered under the basic lot approval provided lot identification is maintained. 4.3.2 For Preproduction Tests As agreed upon by purchaser and vendor. 4.4 App

37、roval 4.4.1 Sample product shall be approved by purchaser before product for production use is supplied, unless such approval be waived by purchaser. Results of tests on production product shall be essentially equivalent to those on the approved sample. _ SAE INTERNATIONAL AMS3046F Page 4 of 64.4.2

38、Vendor shall use ingredients, manufacturing procedures, processes, and methods of inspection on production product which are essentially the same as those used on the approved sample product. If necessary to make any changes in ingredients, processing techniques, or manufacturing procedures vendor s

39、hall submit for reapproval a statement of the proposed changes in ingredients and/or processing and when requested, sample product. Production product shall not be shipped prior to receipt of reapproval. 4.5 Reports The vendor of the product shall furnish with each shipment a report showing the resu

40、lts of tests to determine conformance to the acceptance test requirements and stating that the product conforms to the other technical requirements. This report shall include the purchase order number, AMS3046F, vendors material designation, lot number, date of manufacture, and quantity. 4.6 Resampl

41、ing and Retesting If any sample used in the above tests fails to meet the specified requirements, disposition of the product may be based on the results of testing three additional samples for each original nonconforming sample. Failure of any retest sample to meet the specified requirements shall b

42、e cause for rejection of the product represented. Results of all tests shall be reported. 5. PREPARATION FOR DELIVERY 5.1 Packaging and Identification 5.1.1 The magnetic particles shall be packaged in aerosol cans conforming to AMS2820 and meeting the requirements of 3.4. Magnetic particles shall be

43、 completely mixed with vehicle and each can shall contain a pellet to aid in agitation or mixing of the product prior to spraying. The aerosol cans shall be of suitable size for hand application of the product or as otherwise ordered. 5.1.2 Each aerosol can shall be identified with not less than the

44、 following information on a durable label bearing characters of such size as to be legible and which will not be obliterated by normal handling: MAGNETIC PARTICLE, FLUORESCENT, WET METHOD, OIL VEHICLE, AEROSOL PACKAGED AMS3046F MANUFACTURERS IDENTIFICATION _ DATE OF MANUFACTURE* _ LOT NUMBER* _ QUAN

45、TITY _ MANUFACTURERS INSTRUCTIONS FOR USE* _ APPROPRIATE WARNINGS OR PRECAUTIONARY NOTICES _ * May be included in the manufacturers identification or lot number. * May be stamped on the can * May be on a separate sheet. 5.1.3 The aerosol cans shall be packaged in an exterior shipping container capab

46、le of protecting the product, during shipment and storage, against damage from exposure to weather or any other normal hazard. 5.1.4 Containers of the product shall be prepared for shipment in accordance with commercial practice and in compliance with applicable rules and regulations pertaining to the handling, packaging, and transportation of the product to ensure carrier acceptance and safe delivery. _ SAE INTERNATIONAL AMS3046F Page 5 of 66. ACKNOWLEDGMENT A vendor shall mention this specification number and its