SAE AMS 3050-2017 Performance Specification Anti-Seize Thread Compound High Temperature.pdf

1、_ SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising there

2、from, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions. Copyright 2017 SAE International All rights reserved. No part of this p

3、ublication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-497

4、0 (outside USA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/standards.sae.org/AMS3050 AEROSPACE MATERIAL SPECIFICATION AMS3050 Issued 2017-12 Performance Specification Anti-

5、Seize Thread Compound, High Temperature RATIONALE This document has been revised to distinguish this foundation specification (AMS3050) and the associated category specifications (AMS3050/1 through AMS3050/9) and to classify different anti-seize greases conforming to this specification by the type o

6、f anti-seize additive. The category specifications have been added to the Applicable Documents section. The specification is a direct copy from MIL-PRF-907F 17 November 2004, except that it is intended to be used (by slash sheet designation) to exclude anti-seize materials not required on commercial

7、 aircraft, aircraft engines, engine pylons and aircraft components. All material referring to Mil Supply and usage; Contacts and addresses have been removed as not required for SAE purposes. No importance should be given to this type of material for future balloting of this specification. SAE INTERN

8、ATIONAL AMS3050 Page 2 of 11 TABLE OF CONTENTS 1. SCOPE 3 1.1 Form 3 1.1.1 Foundation and Category Specifications 3 2. APPLICABLE DOCUMENTS 3 2.1 General 3 2.2 Government Publications 3 2.2.1 Specifications, Standards and Handbooks . 3 2.3 Non-Government Publications 4 2.4 Order of Precedence . 4 3.

9、 REQUIREMENTS . 5 3.1 Qualification 5 3.2 Material 5 3.3 Corrosion on Copper . 5 3.4 Toxicity 5 3.5 Homogeneity . 5 3.6 Oil Separation . 5 3.7 Storage Stability 5 3.8 Performance 5 4. VERIFICATION . 5 4.1 Classification of Inspections 5 4.2 Qualification Inspection . 6 4.3 Conformance Inspection . 6

10、 4.3.1 Lot . 6 4.3.2 Examination of Filled Containers 6 4.3.3 Sample Material for Testing 6 4.3.4 Sampling for Production Check Tests . 6 4.4 Tests 7 4.4.1 Test Procedures 7 4.4.2 Performance Tests 7 4.4.3 Storage Stability 9 5. QUALITY ASSURANCE PROVISIONS 9 5.1 Responsibility for Inspection . 9 5.

11、2 Acceptance Tests 9 5.2.1 Batch . 9 5.2.2 Random Sampling . 9 5.2.3 Report 9 5.2.4 Report Contents 9 5.3 Change Management 9 6. PREPARATION FOR DELIVERY . 9 6.1 Packaging . 9 6.2 Identification 10 7. ACKNOWLEDGMENT 10 8. REJECTIONS . 10 9. NOTES 10 9.1 Revision Indicator 10 Figure 1 Test fixture 11

12、 Table 1 Test methods 7 SAE INTERNATIONAL AMS3050 Page 3 of 11 1. SCOPE 1.1 Form This foundation specification (AMS3050) and its associated category specifications (AMS3050/1 through AMS3050/9) cover anti-seize compounds for use on threads of nuts, studs, bolts, and other mating surfaces, including

13、those of superheated steam installations, at temperatures up to 1050 F (566 C). Compounds containing PTFE are limited to 600 F/315 C maximum. Materials for nuts, studs, bolts and other mating surfaces include, but are not limited to Steel, Nickel alloys, Stainless Steel, Silver coated materials. 1.1

14、.1 Foundation and Category Specifications This foundation specification establishes the requirements for all anti-seize compounds conforming to this specification. The individual Category specifications establish the requirements by separate anti-seize additives. Synthetic fluids and lithium complex

15、 soap thickeners are typically part of greases of this type, but other base fluids and thickeners may be acceptable. 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplie

16、r may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that document shall apply. 2.1 General The documents listed in this section are

17、 specified in Sections 3, 4, or 5 of this specification. This section does not include documents cited in other sections of this specification or recommended for additional information or as examples. While every effort has been made to ensure the completeness of this list, document users are cautio

18、ned that they must meet all specified requirements of documents cited in Sections 3, 4, or 5 of this specification, whether or not they are listed. 2.2 Government Publications 2.2.1 Specifications, Standards and Handbooks The following specifications, standards, and handbooks form a part of this doc

19、ument to the extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the solicitation or contract. DEPARTMENT OF DEFENSE SPECIFICATIONS MIL-PRF-907 MIL-PRF-680 Degreasing Solvent MIL-DTL-1222 Studs, Bolts, Hex Cap Screws and Nuts (Copies of these documen

20、ts are available at http:/quicksearch.dla.mil.) FEDERAL STANDARDS FED-STD-791 Lubricants, Liquid Fuels and Related Products; Methods of Testing (Copies of these documents are available at http:/quicksearch.dla.mil.) SAE INTERNATIONAL AMS3050 Page 4 of 11 2.3 Non-Government Publications The following

21、 documents form a part of this document to the extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the solicitation or contract. ASTM INTERNATIONAL ASTM A109 Standard Specification for Steel, Strip, Carbon (0.25 Maximum Percent), Cold-Rolled. (DOD ad

22、opted) ASTM A193 Standard Specification for Alloy-Steel and Stainless Steel Bolting Materials for High-Temperature Service. (DOD adopted) ASTM A194 Standard Specification for Carbon and Alloy Steel Nuts for Bolts for High Pressure or High Temperature Service, or Both. (DoD adopted) ASTM A515 Standar

23、d Specification for Pressure Vessel Plates, Carbon Steel, for Intermediate and Higher-Temperature Service. (DOD adopted) (Copies of these documents are available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org.) SAE AMS

24、3050 Performance Specification Anti-Seize Thread Compound, High Temperature AMS3050/1 Performance Specification Anti-Seize Thread Compound, High Temperature - Copper Only AMS3050/2 Performance Specification Anti-Seize Thread Compound, High Temperature - Aluminum Only AMS3050/3 Performance Specificat

25、ion Anti-Seize Thread Compound, High Temperature - Nickel Only AMS3050/4 Performance Specification Anti-Seize Thread Compound, High Temperature - Molybdenum Disulphide; Graphite Only AMS3050/5 Performance Specification Anti-Seize Thread Compound, High Temperature - PTFE Only AMS3050/6 Performance Sp

26、ecification Anti-Seize Thread Compound, High Temperature - Nickel+Graphite Only AMS3050/7 Performance Specification Anti-Seize Thread Compound, High Temperature - Copper+Graphite+Aluminum Only AMS3050/8 Performance Specification Anti-Seize Thread Compound, High Temperature - Graphite+Aluminum Only A

27、MS3050/9 Performance Specification Anti-Seize Thread Compound, High Temperature - Graphite+Calcium Fluoride Only (Copies of these documents are available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or +1 724-776-4970 (outside U

28、SA), www.sae.org.) 2.4 Order of Precedence In the event of a conflict between the text of this document and the references cited herein, the text of this document takes precedence. Nothing in this document, however, supersedes applicable laws and regulations unless a specific exemption has been obta

29、ined. SAE INTERNATIONAL AMS3050 Page 5 of 11 3. REQUIREMENTS 3.1 Qualification For this specification as per OEM requirements. 3.2 Material The compound supplied under this specification shall be a smooth homogeneous mixture, uniform in appearance, free from lumps, abrasive materials, or other undes

30、irable fillers or impurities. There shall be no odor of rancidity or perfume. 3.3 Corrosion on Copper After 24-hour exposure, the compound shall show no green color, no pitting or etching on the copper, nor shall a dark brown or black stain remain on the copper strip after washing with N-hexane. A s

31、light brown stain shall not be cause for failure. 3.4 Toxicity The compound shall comply with REACH and/or TCSA regulations. It shall have no adverse effect on the health of personnel when used for its intended purpose and shall not cause any environmental problems during waste disposal. 3.5 Homogen

32、eity The compound shall be completely homogeneous at the time of inspection or during storage awaiting completion of the qualification tests. It shall possess a smooth greasy consistency without lumps, crusts or granular particles when examined. 3.6 Oil Separation The vehicle of the compound shall s

33、eparate not more than 10% of the compounds weight in 30 hours when tested at 150 F 5 F (66 C 3 C). 3.7 Storage Stability After the compound has been stored for 6 months at a temperature of 150 F 5 F (66 C 3 C), it shall be examined. The compound shall be a smooth homogeneous mixture free from lumps

34、and granular materials. 3.8 Performance There shall be no galling of the stud threads, the nut threads, the nut contacting surface and the corresponding plate contacting surface when the test apparatus is disassembled following the performance test. The average breakaway torque for loosening of the

35、nuts from the studs shall be as specified in 4.4.2.1.4. 3.9 Recycled, recovered, or environmentally preferable materials. Recycled, recovered, or environmentally preferable materials should be used to the maximum extent possible, provided that the material meets or exceeds the operational and mainte

36、nance requirements, and promotes economically advantageous life cycle costs. 4. VERIFICATION 4.1 Classification of Inspections The inspection requirements specified herein are classified as follows: a. Qualification inspection (see 4.2). b. Conformance inspection (see 4.3). SAE INTERNATIONAL AMS3050

37、 Page 6 of 11 4.2 Qualification Inspection Qualification inspection shall be conducted at a laboratory acceptable to the command or agency concerned. Qualification inspection shall consist of examination and tests specified in 4.3 and 4.4. 4.3 Conformance Inspection 4.3.1 Lot For the purposes of sam

38、pling, a lot shall consist of all compound manufactured as one batch. Any container in the sample having one or more defects, or under required fill shall cause rejection of the container and if the number of defective containers in any sample exceeds the acceptable number for the appropriate sampli

39、ng plan as specified in the contract or order, this shall cause rejection of the lot represented by the sample. 4.3.2 Examination of Filled Containers A sample of filled containers selected from each lot in accordance with MIL-STD-1916 as specified in the contract or order shall be examined to verif

40、y compliance with all stipulations of this specification regarding fill, closure, marking and other requirements not involving tests. Containers shall be examined for defects of the container and the closure, for evidence of leakage, and for unacceptable markings; each sample filled container shall

41、also be weighed to determine the amount of the contents. Any container in the sample having one or more defects, or under required fill shall cause rejection of the container and if the number of defective containers in any sample exceeds the acceptable number for the appropriate sampling plan as sp

42、ecified in the contract or order, this shall cause rejection of the lot represented by the sample. 4.3.2.1 Examination of Compound Material Portions of the compound material shall be taken from top, bottom and intermediate parts of the sample of containers and examined visually to determine that the

43、re is no apparent difference in appearance or consistency. The material shall be homogeneous and show a smooth greasy consistency without lumps, crusts or granular particles. It shall not have an odor of rancidity or perfume. 4.3.3 Sample Material for Testing From each lot, a 5-pound container shall

44、 be selected, sealed and marked. The 5-pound sample specimen shall be retained by the manufacturer or contractor for verification testing, if required, at a later date. 4.3.4 Sampling for Production Check Tests Unless otherwise specified, (see 5.2), from the first lot produced on a contract or order

45、 and thereafter at such intervals as may be considered necessary by the command or agency concerned to verify the consistency of production quality, one 2-pound sample and two 1-pound samples of compound shall be forwarded to a laboratory acceptable to the command or agency concerned. These samples

46、shall meet the requirements of 3.6 and any other tests deemed necessary by the command or agency concerned to determine conformance of the product. SAE INTERNATIONAL AMS3050 Page 7 of 11 4.4 Tests 4.4.1 Test Procedures The following tests shall be performed in accordance with Table 1. Table 1 - Test

47、 methods Test Applicable FED-STD-791 Test Method Test Paragraph Acceptance Criteria Required for Qualification Corrosion on copper 5309 - 3.3 X Oil separation (150 F/66 C) ASTM D6184 - 3.6 X Storage stability 3467 4.4.3 3.7 X Performance 4.4.2 3.8 X 4.4.2 Performance Tests 4.4.2.1 Torque, Galling an

48、d Seizing Test 4.4.2.1.1 Apparatus The test apparatus shall consist of the following: A fixture made of carbon steel, using material in accordance with ASTM A515, Grade 70, 13 by 3 inches by approximately 1-1/2 inches thick for the end blocks which have five equally spaced holes, 13/16 inch in diame

49、ter, with surface finish of 250 roughness height rating (RHR), to allow for insertion of 3/4 inch ten UNC studs (see Figure 1). The top and bottom faces of the steel end blocks shall have a surface finish of 250 RHR and be parallel within 0.002. Five unused coarse thread studs, in accordance with grade B16 of MIL-DTL-1222, ASTM A193 or equal, cut from the same length of a continuously threaded