SAE AMS 3301H-2011 Silicone Rubber General Purpose 40 Durometer《通用40硬度计硅橡胶》.pdf

1、_ SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising there

2、from, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions. Copyright 2011 SAE International All rights reserved. No part of this publication m

3、ay be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-4970 (outside U

4、SA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/www.sae.org/technical/standards/AMS3301H AEROSPACE MATERIAL SPECIFICATION AMS3301 REV. H Issued 1950-10 Reaffirmed 2007-06 Re

5、vised 2011-06Superseding AMS3301G Silicone, Rubber General Purpose 40 Durometer RATIONALE This is the periodic review and reaffirmation of this specification with only minor, editorial changes. The requirements for low temperature modulus per ASTM D 797 were eliminated per committee agreement since

6、this test specification is obsolete. 1. SCOPE 1.1 Form This specification covers a silicone rubber in the form of sheet, strip, tubing, extrusions, and molded shapes. 1.2 Application This product has been used typically for parts required to operate or seal from -85 to +401 F (-65 to +205 C). Silico

7、ne elastomer is resistant to deterioration by weathering and petroleum-base lubricating oil and remains flexible over the temperature range noted, but usage is not limited to such applications. These products are not normally suitable for use in contact with gasoline or aromatic fuels and low-anilin

8、e-point petroleum-base fluids due to excessive swelling of the elastomer. 1.3 Safety-Hazardous Materials While the materials, methods, applications, and processes described or referenced in this specification may involve the use of hazardous materials, this specification does not address the hazards

9、 which may be involved in such use. It is the sole responsibility of the user to ensure familiarity with safe and proper use of any hazardous materials and to take necessary precautionary measures to ensure the health and safety of all personnel involved. 2. APPLICABLE DOCUMENTS The issue of the fol

10、lowing documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no supersedi

11、ng document has been specified, the last published issue of that document shall apply. SAE AMS3301H Page 2 of 6 2.1 SAE Publications Available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.o

12、rg. AMS2279 Tolerances, Rubber Products AMS2810 Identification and Packaging, Elastomeric Products 2.2 ASTM Publications Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM D 297 Rubber Products - Chemical A

13、nalysis ASTM D 395 Rubber Property - Compression Set ASTM D 412 Rubber Properties in Tension ASTM D 471 Rubber Property - Effect of Liquids ASTM D 573 Rubber - Deterioration in an Air Oven ASTM D 624 Rubber Property - Tear Resistance ASTM D 2137 Rubber Property - Brittleness Point of Flexible Polyme

14、rs and Coated Fabrics ASTM D 2240 Rubber Property - Durometer Hardness 3. TECHNICAL REQUIREMENTS 3.1 Material Shall be a compound, based on a silicone rubber, suitably cured to produce a product meeting the requirements of 3.2. 3.2 Properties This product shall conform to the following requirements;

15、 tests shall be performed on the product supplied and in accordance with specified ASTM methods, insofar as practicable: SAE AMS3301H Page 3 of 6 TABLE 1 3.2.1 As Received 3.2.1.1 Hardness, Durometer “A” or equivalent 40 5 ASTM D 2240 3.2.1.2 Tensile Strength, minimum 700 psi (4.83 MPa) ASTM D 412,

16、Die B or C 3.2.1.3 Elongation, minimum 250% ASTM D 412, Die B or C 3.2.1.4 Tensile Stress at 100% Elongation, maximum 200 psi (1.38 MPa) ASTM D 412, Die B or C Stretch specimen to 125% elongation twice within 5 minutes before testing. 3.2.1.5 Tear Resistance, minimum 55 pounds force per inch (9.63 k

17、N/m) ASTM D 624, Die B 3.2.1.6 Specific Gravity Preproduction Value 0.03 ASTM D 297 3.2.2 Petroleum Lubricating Oil Resistance (Immediate Deteriorated Properties) ASTM D 471 Medium: ASTM Oil No. 1 Temperature: 302 F 5 (150 C 3) Time: 70 hours 0.5 3.2.2.1 Hardness Change, Durometer “A” or equivalent

18、-15 to +5 3.2.2.2 Tensile Strength, Change, maximum -25% 3.2.2.3 Elongation Change, maximum -20% 3.2.2.4 Volume Change, maximum 0 to 15% 3.2.2.5 Decomposition None 3.2.2.6 Surface Tackiness None 3.2.3 Dry Heat Resistance ASTM D 573 Temperature: 437 F 5 (225 C 3) 3.2.3.1 Hardness Change, Durometer “A

19、” or equivalent 10 Time: 70 hours 0.5 3.2.3.2 Tensile Strength Change, maximum -20% 3.2.3.3 Elongation Change, maximum -40% 3.2.3.4 Bend (flat) No cracking or checking 3.2.4 Compression Set ASTM D 395, Method B Temperature: 302 F 5 (150 C 3) 3.2.4.1 Percent of Original Deflection, maximum 25 Time: 7

20、0 hours 0.5 3.2.5 Low Temperature Resistance 3.2.5.1 Brittleness Pass ASTM D 2137, Method A Temperature: -85 F 5 (-65 C 3) Time: 3 minutes 0.3 SAE AMS3301H Page 4 of 6 3.2.6 Weathering When specified, the product shall have weather resistance acceptable to purchaser, determined by a procedure agreed

21、 upon by purchaser and vendor. 3.2.7 Corrosion The product shall not have a corrosive effect on other materials when exposed to conditions normally encountered in service, determined by a procedure agreed upon by purchaser and vendor. Discoloration of metal shall not be considered objectionable. 3.3

22、 Quality The product, as received by purchaser, shall be uniform in quality and condition, smooth, as free from foreign material as commercially practicable, and free from imperfections detrimental to usage of the product. 3.4 Tolerances Shall conform to all applicable requirements of AMS2279. 4. QU

23、ALITY ASSURANCE PROVISIONS 4.1 Responsibility for Inspection The vendor of the product shall supply all samples for vendors tests and shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ens

24、ure that the product conforms to specified requirements. 4.2 Classification of Tests 4.2.1 Acceptance Tests Tests for the following requirements are acceptance tests and shall be performed on each lot: TABLE 2 Requirement Paragraph Reference Hardness, as received 3.2.1.1 Tensile Strength, as receive

25、d 3.2.1.2 Elongation, as received 3.2.1.3 Specific Gravity 3.2.1.6 4.2.2 Preproduction Tests Tests for all technical requirements are preproduction tests and shall be performed prior to or on the initial shipment of a product to a purchaser, when a change in ingredients and/or processing requires re

26、approval as in 4.4.2, and when purchaser deems confirmatory testing to be required. SAE AMS3301H Page 5 of 6 4.3 Sampling and Testing Shall be as follows: 4.3.1 For Acceptance Tests Sufficient product shall be taken at random from each lot to perform all required tests. The number of determinations

27、for each requirement shall be as specified in the applicable test procedure or, if not specified therein, not less than three. 4.3.1.1 If specimens cannot be prepared from the product, ASTM test specimens prepared from the same batch and state of cure shall be used. When the product supplied is an e

28、xtrusion of such shape that suitable test specimens cannot be cut from the product, a separate flat strip test sample from the same production lot shall be supplied upon request. This strip shall be prepared from tubing 1.000 inch 0.063 (25.40 mm 1.60) in OD by 0.075 inch 0.008 (1.90 mm 0.20) in wal

29、l thickness, mechanically slit and flattened into a strip while being extruded, and cured in the same manner as production product. When the product is a molded shape from which test specimens cannot be cut, a slab 6 inches (152 mm) square by 0.075 inch 0.008 (1.90 mm 0.20) molded from the same batc

30、h of compound shall be supplied upon request. 4.3.1.2 A lot shall be all product from the same batch of compound processed in one continuous production run and presented for vendors inspection at one time. 4.3.1.3 A batch shall be the quantity of compound run through a mill or mixer at one time. 4.3

31、.1.4 When a statistical sampling plan has been agreed upon by purchaser and vendor, sampling shall be in accordance with such plan in lieu of sampling as in 4.3.1 and the report of 4.5 shall state that such plan was used. 4.3.2 For Preproduction Tests As agreed upon by purchaser and vendor. 4.4 Appr

32、oval 4.4.1 Sample product shall be approved by purchaser before product for production use is supplied; unless such approval be waived by purchaser. Results of tests on production product shall be essentially equivalent to those on the approved sample. 4.4.2 Vendor shall use ingredients, manufacturi

33、ng procedures, processes, and methods of inspection on production product which are essentially the same as those used on the approved sample product. If necessary to make any change in ingredients, in type of equipment for processing, or in manufacturing procedures, vendor shall submit for reapprov

34、al a statement of the proposed changes in ingredients and/or processing and, when requested, sample product. Production product made by the revised procedure shall not be shipped prior to receipt of reapproval. 4.5 Reports The vendor of the product shall furnish with each shipment a report showing t

35、he results of tests to determine conformance to the acceptance test requirements and stating that the product conforms to the other technical requirements. This report shall include the purchase order number, lot number, AMS3301H, vendors compound number, form and size or part number, and quantity.

36、SAE AMS3301H Page 6 of 6 4.6 Resampling and Retesting If any specimen used in the above tests fails to meet the specified requirements, disposition of the product may be based on the results of testing three additional specimens for each original nonconforming specimen. Failure of any retest specime

37、n to meet the specified requirements shall be cause for rejection of the product represented and no additional testing shall be permitted. Results of all tests shall be reported. 5. PREPARATION FOR DELIVERY 5.1 Identification and Packaging Shall be in accordance with AMS2810. 6. ACKNOWLEDGMENT A ven

38、dor shall mention this specification number and its revision letter in all quotations and when acknowledging purchase orders. 7. REJECTIONS Product not conforming to this specification, or to modifications authorized by purchaser, will be subject to rejection. 8. NOTES 8.1 A change bar (l) located i

39、n the left margin is for the convenience of the user in locating areas where technical revisions, not editorial changes, have been made to the previous issue of this document. An (R) symbol to the left of the document title indicates a complete revision of the document, including technical revisions. Change bars and (R) are not used in original publications, nor in documents that contain editorial changes only. PREPARED BY AMS COMMITTEE “CE“