SAE AMS 3384-2013 Rubber Fluorocarbon Elastomer (FKM) 70 to 80 Hardness Low Temperature Sealing Tg -22 (-30 For Elastomeric Shapes or Parts in Gas Turbine Engine Oil Fuel and Hydra.pdf

1、_SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising theref

2、rom, is the sole responsibility of the user.”SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions.Copyright 2013 SAE InternationalAll rights reserved. No part of this publication may b

3、e reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE.TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada)Tel: +1 724-776-4970 (outside USA)Fax

4、: 724-776-0790Email: CustomerServicesae.orgSAE WEB ADDRESS: http:/www.sae.orgSAE values your input. To provide feedbackon this Technical Report, please visithttp:/www.sae.org/technical/standards/AMS3384AEROSPACEMATERIALSPECIFICATIONAMS3384Issued 2013-08Rubber, Fluorocarbon Elastomer (FKM)70 to 80 Ha

5、rdness, Low Temperature Sealing Tg -22 F (-30 C)For Elastomeric Shapes or Parts in Gas Turbine Engine Oil, Fuel and Hydraulic SystemsRATIONALEThis specification supersedes AMS-R-83485 and creates two specifications: AMS3000-series and AMS7000-series, with a new part specification added. The technica

6、l requirements of AMS-R-83485 have been maintained, with the addition of a long-term compression set requirement, replacement of AMS3021 (diester) with BP Reference Oil 300, AMS3085 (representative of HTS class gas turbine lubricants), and the addition of a glass transition (Tg) value/requirement. A

7、S83485 part standard will supersede AMS-R-83485/1.1. SCOPE1.1 FormThis specification covers a high temperature, compression set and fluid resistant fluorocarbon (FKM) rubber in the form of sheet, strip, tubing, extrusions, and molded shapes for aeronautical and aerospace applications.1.2 Application

8、These products have been used in contact with air and a wide variety of fuels, lubricants, specific hydraulic fluids, and a variety of gas turbine engine lubricants, including higher thermo-oxidative stability (HTS) lubricants, including thoseconforming to MIL-PRF-23699 Class HTS, MIL-PRF-7808 Grade

9、 4 and AS5780 Class HPC; however usage is not limited to such applications. This Material Type has a typical service temperature range of -40 to +400 F (-40 to +204 C). These products are not suitable for use in phosphate ester based hydraulic fluids. Each application should be considered indivuidua

10、lly.1.3 Safety-Hazardous MaterialsWhile the materials, methods, applications, and processes described or referenced in this specification may involve the use of hazardous materials, this specification does not address the hazards which may be involved in such use. It is the sole responsibility of th

11、e user to ensure familiarity with the safe and proper use of any hazardous materials and to take necessary precautionary measures to ensure the health and safety of all personnel involved.2. APPLICABLE DOCUMENTSThe issue of the following documents in effect on the date of the purchase order forms a

12、part of this specification to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that docu

13、ment shall apply.SAE AMS3384 Page 2 of 62.1 SAE PublicationsAvailable from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.org.AMS2279 Tolerances, Rubber ProductsAMS2810 Identification and Packagin

14、g, Elastomeric ProductsAMS3021 Fluid, Reference for Testing Di-Ester (Polyol) Resistant MaterialAMS3085 Fluid, Reference for Testing AS5780 HPC Class (Polyol) Resistant MaterialAMS-R-83485 Rubber, Fluorocarbon Elastomer, Improved Performance at Low TemperaturesAS5780 Specification for Aero and Aero-

15、Derived Gas Turbine Engine LubricantsAS83485 Aerospace Standard, Packing, Preformed, AMS 7XXX, O-ring2.2 ASTM PublicationsAvailable from ASTM International, 100 Barr Harbor Drive, P.O.Box C700, West Conshohocken, PA 19428-2959,Tel: 610-832-9585, www.astm.org.ASTM D 297 Rubber Products - Chemical Ana

16、lysisASTM D 395 Rubber Property - Compression SetASTM D 412 Vulcanized Rubber and Thermoplastic Elastomers - TensionASTM D 471 Rubber Property - Effect of LiquidsASTM D 573 Rubber - Deterioration in an Air OvenASTM D 1329 Rubber Property - Retraction at Low Temperature (TR Test)ASTM D 1418 Standard

17、Practice for Ruubber and Rubber Lastices - NomenclatureASTM D 2240 Rubber Property - Durometer HardnessASTM D 7426 Assignment of the DSC Procedure for Determining Tg of a Polymer or an Elastomeric Compound2.3 U.S. Government PublicationsAvailable from the Document Automation and Production Service (

18、DAPS), Building 4/D, 700 Robbins Avenue, Philadelphia, PA 19111-5094, Tel: (215) 697-6396, http:/quicksearch.dla.mil/.MIL-PRF-7808 Performance Specification Lubricating Oil, Aircraft Turbine Engine, Aircraft Turbine Engine, Synthetic BaseMIL-PRF-23699 Performance Specification Lubricating Oil, Aircr

19、aft Turbine Engine, Aircraft Turbine Engine, Synthetic Base, NATO Code Number O-156SAE AMS3384 Page 3 of 63. TECHNICAL REQUIREMENTS3.1 MaterialThe product shall be prepared from ingredients as shall be necessary to achieve the requirements detailed in this standard. The composition is not defined by

20、 this standard. The basic ingredient shall be based on 100% virgin fluorocarbon (FKM) elastomer meeting ASTM D 1418 Type 3. No reprocessed or non-fluorocarbon polymer is acceptable.3.2 PropertiesTests shall be performed on the product supplied and shall conform to the requirements shown in Table 1 a

21、nd in accordance with specified ASTM methods, insofar as practicable and as described in 4.3.1.1 where specimens cannot be prepared from the product.TABLE 1 PROPERTIESParagraph Property Requirements Test Method3.2.1 Hardness, Durometer “A” or Equivalent 75 5 ASTM D 22403.2.2 Tensile Strength, min 16

22、00 psi(11.03 MPa)ASTM D 4123.2.3 Elongation, min 120% ASTM D 4123.2.4 Specific Gravity Qualification Value 0.02ASTM D 297, hydrostatic method3.2.5 Low-Temperature ResistanceTemperature Retraction, (TR10), F (C) max-20 (-29) ASTM D 1329 (use test slab as specimen)3.2.6 Low-Temperature Resistance Glas

23、s Transition (Tg) Mid-Point, F (C) max-20 (-29) ASTM D 74263.2.7 Aromatic Fuel Resistance ASTM D 471ASTM Reference Fuel B73 F 5 (23 C 2)70 hours 0.53.2.7.1 Hardness Change, Durometer “A” or Equivalent -10 to +5 3.2.7.2 Tensile Strength Change, max -20%3.2.7.3 Elongation Change, max -20%3.2.7.4 Volum

24、e Change, max 1 to +10%3.2.8 Gas Turbine Engine Oil Resistance ASTM D 471 (Note A)AMS3085392 F 5 (200 C 2) 70 hours 0.53.2.8.1 Hardness Change, Durometer “A” or Equivalent -15 to 03.2.8.2 Tensile Strength Change, max -35%3.2.8.3 Elongation Change, max -20%3.2.8.4 Volume Change, max 0 to +20%3.2.8.5

25、Compression Set, max 20% ASTM D 395 Method BAMS3085392 F 5 (200 C 2) 70 hours 0.53.2.8.6 Long Term Compression Set, max 40% ASTM D 395 Method B AS5780AMS3085392 F 5 (200 C 2) 336 hours 0.53.2.9 Dry Heat Resistance ASTM D 573 528 F 5 (275 C 2)70 hours 0.5SAE AMS3384 Page 4 of 6TABLE 1 PROPERTIES (CON

26、T.)Paragraph Property Requirements Test Method3.2.9.2 Tensile Strength Change, max -35%3.2.9.4 Weight Loss, max 12% 4.4.13.2.9.5 Compression Set, % of Original Deflection, max 20% ASTM D 395 Method B 392 F 5 (200 C 2)22 hours 0.53.2.9.6 Long Term Compression Set, max 40% ASTM D 395, Method B392 F 5

27、(200 C 2)336 hours 0.5Note A: Do not dip specimens in acetone; blot dry residual oil from specimen.3.3 QualityThe product, as received by purchaser, shall be uniform in quality and condition, smooth, as free from foreign materials as commercially practicable, and free from imperfections detrimental

28、to usage of the product.3.4 TolerancesShall conform to all applicable requirements of AMS2279.4. QUALITY ASSURANCE PROVISIONS4.1 Responsibility for InspectionThe manufacturer of the product shall supply all samples and shall be responsible for the performance of all required tests. Purchaser reserve

29、s the right to sample and to perform any confirmatory testing deemed necessary to ensure the product conforms to the specified requirements.4.2 Classification of Tests4.2.1 Acceptance TestsRequirements shown in Table 2 are acceptance tests and shall be performed on each lot.TABLE 2Requirement Paragr

30、aphHardness, as received 3.2.1.Tensile Strength, as received 3.2.2Elongation, as received 3.2.3Specific Gravity 3.2.4Compression Set 3.2.9.54.2.2 Preproduction TestsAll technical requirements are preproduction tests and shall be performed prior to or on the initial shipment of a product toa purchase

31、r, when a change in ingredients and/or processing requires reapproval as in 4.4.2, and when purchaser deems confirmatory testing to be required.4.2.3 Sampling and TestingShall be as follows:SAE AMS3384 Page 5 of 64.2.4 For Acceptance TestsSufficient product shall be taken at random from each lot to

32、perform all required tests. The number of determinations for each requirement shall be as specified in the applicable test procedure or, if not specified therein, not less than three.4.2.4.1 If specimens cannot be prepared from the product, ASTM test specimens prepared from the same batch andstate o

33、f cure shall be used. When the product supplied is an extrusion of such shape that suitable test specimens cannot be cut from the product, a separate flat strip test sample from the same production lot shall be supplied upon request. This strip shall be prepared from tubing 1.000 inch 0.063 (25.40 m

34、m 1.60) in OD by 0.075 inch 0.008 (1.90 mm 0.20) in wall thickness, mechanically slit and flattened into a strip while being extruded, and cured in the same manner as production material. When the product is a molded shape from which test specimens cannot be cut, a slab 6 inches (152 mm) square by 0

35、.075 inch 0.008 (1.90 mm 0.20) molded from the same batch of compound shall be supplied upon request.4.2.4.2 A lot shall be all product from the same batch of compound processed in one continuous production run and presented for vendors inspection at one time.4.2.4.3 A batch shall be the quantity of

36、 compound run through a mill or mixer at one time.4.2.4.4 When a statistical sampling plan has been agreed upon by purchaser and vendor, sampling shall be in accordance with such plan in lieu of sampling as in 4.3.1 and the report of 4.5 shall state that such plan was used.4.2.5 For Preproduction Te

37、stsAs agreed upon by purchaser and vendor.4.3 Test Methods4.3.1 Weight Loss TestsThe weight loss test shall be conducted on samples air-aged at 528 F 5 (275 C 2). Test specimens shall be conditioned for 24 hours 0.5 in a desiccator before and after air aging. The specimens shall be weighed immediate

38、ly after the desiccation period before and after aging. The percentage weight loss shall be calculated as shown in Equation 1.100*121WWWLossWeightPercentageg16g32(Equation 1)Where1W = weight of sample before air-aging2W = weight of sample after air-aging4.4 Approval4.4.1 Sample product shall be appr

39、oved by purchaser before product for production use is supplied; unless such approval is waived by purchaser. Results of tests on production product shall be essentially equivalent to those on the approved sample.4.4.2 Manufacturer shall use ingredients, manufacturing procedures, processes, and meth

40、ods of inspection on production product which are essentially the same as those used on the qualification sample. If any change in ingredients, in type of equipment for processing, or in manufacturing procedures is necessary, manufacturer shall submit for reapproval a statement of the proposed chang

41、es in ingredients and/or processing and, when requested, sample product. Production product made by the revised procedure shall not be shipped prior to receipt of re-approval.SAE AMS3384 Page 6 of 64.5 ReportsThe supplier of the product shall make readily available a report showing the results of te

42、sts to determine conformance to the acceptance requirements and stating that the product conforms to the other technical requirements. This report shall include AMS3384, manufacturers identification and product designation, batch/lot number and date of manufacture. For products requiring source insp

43、ection, reports shall be stamped by the third party source inspector.4.6 Resampling and RetestingIf any specimen fails, a retesting of three additional specimens for each nonconforming specimen shall be necessary for product acceptance. The same batch/lot of product used for the failed test shall be

44、 used for retesting. Failure of any retest specimen shall be cause for rejection. Results of all tests shall be reported.5. PREPARATION FOR DELIVERY5.1 Identification and PackagingShall be as stated on the purchase order or contract requirements; when no requirements are stipulated, packaging shall

45、be in accordance with AMS2810.6. ACKNOWLEDGMENTA supplier shall mention this specification number in all quotations and when acknowledging purchase orders.7. REJECTIONSProduct not conforming to this specification, or to modifications authorized by purchaser, will be subject to rejection.8. NOTES8.1

46、A change bar (|) located in the left margin is for the convenience of the user in locating areas where technical revisions, not editorial changes, have been made to the previous issue of this document. An (R) symbol to the left of the document title indicates a complete revision of the document, inc

47、luding technical revisions. Change bars and (R) are not used in original publications, or in documents that contain editorial changes only.8.2 Dimensions and properties in inch/pound units and the Fahrenheit temperatures are primary; dimensions and properties in SI units and the Celsius temperatures

48、 are shown as the approximate equivalent of the primary units and are presented only for information.8.3 Purchase documents should specify not less than the following:AMS3384Form and size or part number of product orderedQuantity of product orderedSpecial packaging, if requiredPREPARED BY AMS COMMITTEE “CE”