SAE AMS 3906B-1992 Glass Tape and Flat Sheet Non-Woven Cloth Epoxy Resin Impregnated for Hand and Machine Layup《手工和机器铺叠用环氧树脂浸渍的玻璃带、平板和非机织织物》.pdf

1、SAE-AMS3906ADOPTION NOTICESAE-AMS3906, “GLASS TAPE AND FLAT SHEET, NON-WOVEN CLOTH EPOXYRESIN IMPREGNATED, FOR HAND AND MACHINE LAYUP“, was adopted on30-SEP-89 for use by the Department of Defense (DoD). Proposedchanges by DoD activities must be submitted to the DoD AdoptingActivity: Commander, Nava

2、l Air Warfare Center, Aircraft Division,Code 414100B120-3, Highway 547, Lakehurst, NJ 08733-5100. Copiesof this document may be purchased from the Society of AutomotiveEngineers 400 Commonwealth Drive Warrendale, Pennsylvania, UnitedStates, 15096-0001. http:/www.sae.org/_Custodians: Adopting Activit

3、y:Navy - ASArmy - MRNavy - ASAir Force - 11AREA CMPSDISTRIBUTION STATEMENT A: Approved for public release; distributionis unlimited.Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-SAE Technical Standar

4、ds Board Rules provide that: “This report is published by SAE to advance the state of technical and enginee ring sciences. The use of this report is entirelyvoluntary, and its applicability and suitability for any particular use, including any patent infringement arising therefrom, is the sole respo

5、nsibility of the user.”SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invit es your written comments and suggestions.Copyright 1997 Society of Automotive Engineers, Inc.All rights reserved. Printed in U.S.A.QUESTIONS REGARDI

6、NG THIS DOCUMENT: (412) 772-7154 FAX: (412) 776-0243TO PLACE A DOCUMENT ORDER: (412) 776-4970 FAX: (412) 776-0790400 Commonwealth Drive, Warrendale, PA 15096-0001AEROS PACE MATERIAL SPECIFIC ATIONSubmitted for recognition as an American National StandardAMS 3906BIssued JUN1975Revised JUL 1992Reaffir

7、med OCT 1997Superseding AMS 3906AGlass T ape and Flat Sheet, Non-Woven ClothEpoxy Resin Impregnated, For Hand and Machine Layup1. SCOPE:1.1 Form: This specification and its supplementary detail specification cover various types of non-woven glass cloth in the form of tape and flat sheet impregnated

8、with epoxy resin, the resin to be supplied in a “B” staged condition.1.2 Application: These products have been used typically for fabricating high strength composite parts, using autoclave, press, vacuum bag, or filament winding techniques for fabrication, but usage is not limited to such applicatio

9、ns.1.3 Classification: The tapes and flat sheets shall be as specified in the applicable detail specification wherein each product is defined by basic fiber, property characteristics, and maximum continuous service temperature. An example is shown in 8.2. The product covered by each detail specifica

10、tion appears in the title.1.4 Safety - Hazardous Materials: While the materials, methods, applications, and processes described or referenced in this specification may involve the use of hazardous materials, this specification does not address the hazards which may be involved in such use. It is the

11、 sole responsibility of the user to ensure familiarity with the safe and proper use of any hazardous materials and to take necessary precautionary measures to ensure the health and safety of all personnel involved.Copyright SAE International Provided by IHS under license with SAENot for ResaleNo rep

12、roduction or networking permitted without license from IHS-,-AMS 3906B SAE AMS 3906B- 2 -2. APPLICABLE DOCUMENTS:The following publications form a part of this specification to the extent specified herein. The latest issue of SAE publications shall apply. The applicable issue of other publications s

13、hall be the issue in effect on the date of the purchase order.2.1 SAE Publications:Available from SAE, 400 Commonwealth Drive, Warrendale, PA 15096-0001.AMS 2825 Material Safety Data SheetsAMS 3898 Interleaf Carrier Material, Composite Tape2.2 ASTM Publications:Available from ASTM, 100 Barr Harbor D

14、rive, West Conshohocken, PA 19428-2959.ASTM D 695 Compressive Properties of Rigid PlasticsASTM D 695M Compressive Properties of Rigid Plastics (Metric)ASTM D 790 Flexural Properties of Unreinforced and Reinforced Plastics and Electrical Insulating Materials ASTM D 790M Flexural Properties of Unreinf

15、orced and Reinforced Plastics and Electrical Insulating Materials (Metric)ASTM D 792 Specific Gravity (Relative Density) and Density of Plastics by DisplacementASTM D 2344 Apparent Interlaminar Shear Strength of Parallel Fiber Composites by Short Beam MethodASTM D 2734 Void Content of Reinforced Pla

16、sticsASTM D 3039 Tensile Properties of Fiber-Resin CompositesASTM D 3529 Resin Solids Content of Carbon Fiber-Epoxy PrepregASTM D 3530 Volatiles Content of Carbon Fiber-Epoxy PrepregASTM D 3531 Resin Flow of Carbon Fiber-Epoxy PrepregASTM D 3532 Gel Time of Carbon Fiber-Epoxy Prepreg2.3 U.S. Governm

17、ent Publications:Available from DODSSP, Subscription Services Desk, Building 4D, 700 Robbins Avenue, Philadelphia, PA 19111-5094.MIL-R-60346 Roving, Glass, FibrousMIL-STD-2073-1 DOD Materiel, Procedures for Development and Application of Packaging RequirementsCopyright SAE International Provided by

18、IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-AMS 3906B SAE AMS 3906B- 3 -2.4 AIA Publications: Available from National Standards Association, Inc., 1321 Fourteenth Street, N. W., Washington, DC 20005.NAS 992 Reel Composite Filament Tape -

19、 Automated Machine Lay-up3. TECHNICAL REQUIREMENTS:3.1 Detail Specification: The requirements for a specific product shall consist of all requirements specified herein in addition to requirements specified in the applicable detail specification. In case of conflict between requirements of this basic

20、 specification and an applicable detail specification, requirements of the detail specification shall govern.3.2 Material: 3.2.1 Construction: The product shall consist of parallel, non-woven, unidirectional glass fibers meeting the requirements of MIL-R-60346, impregnated with an epoxy resin meetin

21、g the requirements of the applicable detail specification , and arranged in a single in-plane layer.3.2.2 Storage Life: The product shall meet the requirements of the applicable detail specification when tested at any time up to 12 months from date of receipt of the product by purchaser provided the

22、 product has been stored in the original waterproof, heat-sealed container at a temperature not higher than 4 C (39 F).3.2.3 Working Life: The product shall meet the requirements of the applicable detail specification when tested after continuous exposure to a relative humidity not higher than 70% a

23、nd a temperature not higher than 27 C (81 F) for not less than three months.3.3 Properties: 3.3.1 Uncured Impregnated Material: The product as received shall conform to the requirements of this specification and the applicable detail specification. Tests shall be performed on the product supplied an

24、d in accordance with applicable test procedures specified in 4.5 and in the detail specifications.3.3.2 Cured Laminate: Test laminates shall conform to the requirements of this specification and the applicable detail specification. Tests shall be performed in accordance with applicable test procedur

25、es on specimens cut from laminates produced as in 4.5.1.3.4 Quality: The product, as received by purchaser, shall be uniform in quality and condition, and free from foreign materials and from imperfections detrimental to usage of the product.Copyright SAE International Provided by IHS under license

26、with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-AMS 3906B SAE AMS 3906B- 4 -3.5 Sizes and Tolerances: Tape and sheet shall be supplied to the dimensions specified in the purchase order. The width shall vary not more than 0.04 inch (1.0 mm) for each 3 inches (

27、76 mm) of width specified, and the length shall be not less than the net length ordered.4. QUALITY ASSURANCE PROVISIONS: 4.1 Responsibility for Inspection: The vendor of the product shall supply all samples for vendors tests and shall be responsible for performing all required tests. Purchaser reser

28、ves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the product conforms to the requirements of this specification.4.2 Classification of Tests: 4.2.1 Acceptance Tests: Tests for construction (3.2.1); properties of uncured impregnated material (3.3.1); long

29、itudinal flexural strength, modulus of elasticity in flexure, short beam shear strength at room temperature, density, void content, and fiber volume of cured laminate (3.3.2); and sizes and tolerances (3.5) are acceptance tests and shall be performed on each lot.4.2.2 Preproduction Tests: Tests for

30、all technical requirements of this specification and the applicable detail specification are preproduction tests and shall be performed prior to or on the initial shipment of the product to a purchaser, when a change in ingredients and/or processing, requires reapproval as in 4.4.2, and when purchas

31、er deems confirmatory testing to be required.4.2.2.1 For direct U.S. Military procurement, substantiating test data and, when requested, preproduction test material shall be submitted to the cognizant agency as directed by the procuring activity, contracting officer, or request for procurement.4.3 S

32、ampling and Testing: Shall be as follows:4.3.1 For Acceptance Tests: Sufficient product shall be taken at random from each lot and each inspection unit to perform all required tests. The number of determinations for each requirement shall be as stated in 4.3.3, or if not specified herein, not less t

33、han three.4.3.1.1 A lot shall be all product produced at one time without significant change in treater settings using a single batch of resin and reinforcement and presented for vendors inspection at one time. An inspection unit shall not exceed 1000 square yards (836 m 2 ).4.3.1.2 When a statistic

34、al sampling plan has been agreed upon by purchaser and vendor, sampling shall be in accordance with such plan in lieu of sampling as in 4.3.1 and the report of 4.6 shall state that such plan was used.Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or n

35、etworking permitted without license from IHS-,-AMS 3906B SAE AMS 3906B- 5 -4.3.2 For Preproduction Tests: As agreed upon by purchaser and vendor.4.3.3 The minimum number of specimens per test requirement and test frequency are shown in Table 1.4.4 Approval: 4.4.1 Sample product shall be approved by

36、purchaser before product for production use is supplied, unless such approval be waived by purchaser. Results of tests on production product shall be essentially equivalent to those on the approved sample.TABLE 1 - Minimum Number of Specimens and Test FrequencyRequirementNumber of Specimens perRequi

37、rement, minimum Test FrequencyVolatile Content 3 Each lotTotal Non-Fiber Content 3 Each lotResin Flow 3 Each lotGel Time 3 Each lotTack 1 Each lotTotal Weight per Unit Area 3 Each lotUncured Pl y Thickness 1Tensile Strength andModulus of Elasticity 4 PreproductionCompression Strength andModulus of E

38、lasticity 4 PreproductionFlexural Strength andModulus of Elasticity 4 Each Inspection UnitInterlaminar Shear Strength 4 Each Inspection UnitDensity 3 Each Inspection UnitVoid Content 3 Each Inspection UnitFiber Volume 3 Each Inspection UnitCopyright SAE International Provided by IHS under license wi

39、th SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-AMS 3906B SAE AMS 3906B- 6 -4.4.2 Vendor shall use ingredients, manufacturing procedures, processes, and methods of inspection on production product which are essentially the same as those used on the approved sam

40、ple product. If necessary to make any change in ingredients, in type of equipment for processing, or in manufacturing procedures, vendor shall submit for reapproval a statement of the proposed changes in ingredients and/or processing and, when requested, sample product. Production product made by th

41、e revised procedure shall not be shipped prior to receipt of reapproval.4.5 Test Methods: Shall be as follows: properties of cured product shall be determined on test laminates prepared as in 4.5.1:4.5.1 Preparation of Test Laminates: Test laminates of suitable area shall be prepared from sufficient

42、 plies of impregnated cloth oriented unidirectionally to produce cured thicknesses as close as possible to 0.030 inch (0.76 mm) for tensile strength and modulus of elasticity and as close as possible to 0.125 inch (3.18 mm) for all other tests of cured product. Laminates shall be cured at a temperat

43、ure and pressure which will provide optimum properties; the temperature and pressure used shall be noted in the report. The resulting laminates shall each be uniform in thickness within 0.003 inch (0.08 mm).4.5.2 Tack: 4.5.2.1 Cut two pieces of impregnated glass cloth approximately 1 x 3 inches (25

44、x 76 mm), retaining the protective film until immediately before using the specimens. Fiber direction shall be parallel to the 1-inch (25-mm) dimension. For cloth under 3 inches (76 mm) wide, butt sufficient pieces on the panel to produce a 3-inch (76-mm) wide specimen.4.5.2.2 Remove the protective

45、film from one side of one specimen and apply the cloth to the center of a clean piece of austenitic corrosion resistant steel sheet with a commercial 2D finish, any thickness by approximately 4 x 8 inches (102 x 203 mm). Apply light pressure with a squeegee or roller over the backing film. Remove th

46、e backing film and apply the second specimen to the first, in exactly the same manner, making certain that the opposing faces of the cloth are not covered with protective backing film. The second layer of narrow cloth shall be so positioned that the butt joints do not coincide with those of the firs

47、t layer. Remove the protective film from the exposed surface of the cloth and maintain the test plate and the long dimension of the test specimen in a vertical position for not less than 30 minutes at 20 to 30 C (68 to 86 F) and 50 to 70% relative humidity.4.5.2.3 Report results as pass or fail. If

48、a specimen fails to adhere for the test period, record the elapsed time at failure.4.5.3 Total Weight Per Unit Area: 4.5.3.1 Cut sufficient cloth for each of three specimens 24 square inches (155 cm 2 ) in area and weigh to the nearest mg (W 9 ).4.5.3.2 Remove the interleaf carrier from the specimen

49、 and weigh it to the nearest mg (W 10 ).Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-AMS 3906B SAE AMS 3906B- 7 -4.5.3.3 Calculate total weight per unit area as shown in Equation 1 and Equation 2.(Eq.1)(Eq.2)where, W 9 = Weight of specimen and interleaf carrier, grams/24 square inches (g/155 cm 2 )W 10 = Weight of interleaf carrier, grams/24