SAE AMS 5355J-2009 Steel Corrosion Resistant Investment Castings 16Cr - 4 1Ni - 0 28Cb - 3 2Cu Homogenization and Solution Heat Treated or Homogenization Solution and Precipitation.pdf

1、 SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising there

2、from, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions. Copyright 2015 SAE International All rights reserved. No part of this p

3、ublication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-497

4、0 (outside USA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/www.sae.org/technical/standards/AMS5355J AEROSPACE MATERIAL SPECIFICATION AMS5355 REV. J Issued 1955-03 Revised 2

5、009-10 Reaffirmed 2015-10 Superseding AMS5355H Steel, Corrosion Resistant, Investment Castings 16Cr - 4.1Ni - 0.28Cb - 3.2Cu Homogenization and Solution Heat Treated or Homogenization, Solution, and Precipitation Heat Treated (Composition similar to UNS J92200) RATIONALE AMS5355J has been reaffirmed

6、 to comply with the SAE five-year review policy. 1. SCOPE 1.1 Form This specification covers a corrosion resistant steel in the form of investment castings. 1.2 Application These castings have been used typically for parts requiring good corrosion resistance and strength up to 600 F (316 C), but usa

7、ge is not limited to such applications (See 8.3). 1.2.1 Certain processing procedures and service conditions may cause these castings to become subject to stress-corrosion cracking; ARP1110 recommends practices to minimize such conditions. Where stress-corrosion is considered to be a factor, precipi

8、tation heat treatment should be performed at a temperature not lower than 1000 F (538 C). 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a subsequent

9、revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that document shall apply. 2.1 SAE Publications Available from SAE International, 400 Commonwealth Drive,

10、Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.org. AMS2175 Castings, Classification and Inspection of AMS2248 Chemical Check Analysis Limits, Corrosion and Heat-Resistant Steels and Alloys, Maraging and Other Highly-Alloyed Steels, and Ir

11、on Alloys AMS2360 Room Temperature Tensile Properties of Castings AMS2694 In-Process Welding of Aerospace Castings AMS2700 Passivation of Corrosion Resistant Steels AMS 2804 Identification, Castings AMS-H-6875 Heat Treatment of Steel Raw Materials ARP1110 Minimizing Stress Corrosion Cracking in Wrou

12、ght Forms of Steels and Corrosion Resistant Steels and Alloys 2.2 ASTM Publications Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM E 8/E 8M Tension Testing of Metallic Materials ASTM E 18 Rockwell Hardn

13、ess of Metallic Materials ASTM E 353 Chemical Analysis of Stainless, Heat Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys ASTM E 1417 Liquid Penetrant Testing ASTM E 1444 Magnetic Particle Testing ASTM E 1742 Radiographic Examination 3. TECHNICAL REQUIREMENTS 3.1 Composition Casti

14、ngs shall conform to the percentages by weight shown in Table 1, determined by wet chemical methods in accordance with ASTM E 353, by spectrochemical methods, or by other analytical methods acceptable to purchaser (See 8.2.1 and 8.2.2). TABLE 1 - COMPOSITION Element min max Carbon Manganese Silicon

15、Phosphorus Sulfur Chromium Nickel Columbium Copper Tantalum Aluminum Tin Nitrogen - - 0.50 - - 15.50 3.60 0.15 2.80 - - - - 0.06 0.70 1.00 0.025 0.025 16.70 4.60 0.40 3.50 0.05 0.05 0.02 0.05 SAE INTERNATIONAL AMS5355J Page 2 of 11_ 3.1.1 Vendor may test for any element not listed in Table 1 and inc

16、lude this analysis in the report of 4.5. Limits of acceptability may be specified by purchaser (See 8.2.3). 3.1.2 Check Analysis Composition variations shall meet the applicable requirements of AMS2248. 3.2 Melting Practice Castings and specimens shall be poured at the casting vendors facility eithe

17、r from a melt (See 8.2.4) of a master heat or directly from a master heat (See 8.2.5). 3.2.1 Revert (gates, sprues, risers, and rejected castings) may be used only in the preparation of master heats; revert shall not be remelted directly, without refining, for pouring of castings. Melting of revert

18、creates a new master heat. 3.2.2 Portions of two or more qualified master heats (See 3.4.2) may be melted together and poured into castings using a procedure authorized by purchaser (See 8.2.6). 3.2.3 If modifications such as alloy additions or replenishments are made at remelt by the vendor, vendor

19、 shall have a written procedure acceptable to purchaser which defines the controls, tests, and traceability criteria for both castings and separately-cast specimens. Control factors of 4.4.2.2 shall apply. 3.3 Condition Castings shall be homogenization and solution heat treated, except as specified

20、in 3.3.1 or 3.3.2. 3.3.1 When specified by purchaser, castings shall be solution heat treated, omitting homogenization heat treatment. 3.3.2 When specified by purchaser, castings shall be solution heat treated twice, omitting homogenization heat treatment. 3.3.3 Precipitation heat treatment of casti

21、ngs shall not be performed by vendor unless purchaser specifies that castings are to be supplied in one of the age conditions specified in 3.5.3 (See 8.5). 3.4 Test Specimens Specimens shall be either separately-cast, integrally-cast (See 8.2.7), or machined from castings, and shall conform to 3.2.

22、3.4.1 If specimens are separately-cast, vendor shall have a written procedure acceptable to purchaser. Control factors of 4.4.2.2 shall apply. 3.4.2 Each master heat shall be qualified by evaluation of chemical and tensile specimens. 3.4.2.1 If alloy additions or replenishments are made at remelt as

23、 in 3.2.3, the frequency of sampling and testing used by the vendor for qualification to 3.4.2 shall be acceptable to purchaser. 3.4.2.2 The tensile tests of 3.4.2 are not required if these tests are conducted using integrally-cast specimens (4.3.3.2) or specimens machined from castings (4.3.3.3). 3

24、4.2.3 Tensile specimens shall be heat treated to the H925 condition of 3.5.3. Qualifications of separately-cast specimens to conditions other than H925 need be performed only when specifically required by purchaser (See 8.5). 3.4.3 Chemical Analysis Specimens Shall be of any convenient size and sha

25、pe. SAE INTERNATIONAL AMS5355J Page 3 of 11_ 3.4.4 Tensile Specimens Shall be of standard proportions in accordance with ASTM E 8/E 8MM with 0.250 inch (6.35 mm) diameter at the reduced parallel gage section. 3.4.4.1 Separately-cast and integrally-cast specimens may be either cast to size, or cast o

26、versize and subsequently machined to 0.250 inch (6.35 mm) diameter. 3.4.4.2 When integrally-cast specimens and specimens machined from castings are specified, specimen size and location shall be agreed upon by purchaser and vendor (See 8.2.8 and 8.5). 3.5 Heat Treatment Castings and representative t

27、ensile specimens shall be heat treated in accordance with AMS-H-6875 except as specified in 3.5.1 and 3.5.2. 3.5.1 Castings and Tensile Specimens 3.5.1.1 Homogenization Heat Treatment Heat to 2100 F 25 (1149 C 14), hold at heat for not less than 90 minutes, and cool as required to below 70 F (21 C).

28、 3.5.1.2 Solution Heat Treatment Heat to 1900 F 25 (1038 C 14), hold at heat for 1 hour per inch (25 mm) of section thickness but not less than 30 minutes, and cool as required to below 70 F (21 C). 3.5.2 Specimens After heat treatment in accordance with 3.5.1, specimens shall, unless otherwise spec

29、ified, be heat treated in accordance with the following: 3.5.2.1 Precipitation Heat Treatment Heat to 925 F 10 (496 C 6), hold at heat for not less than 90 minutes, and cool in air. 3.5.3 Alternative Precipitation Heat Treatments Castings, when specified, and representative tensile specimens, precip

30、itation heat treated to a particular condition in accordance with the corresponding temperatures and times shown in Table 2 and cooled in air, shall exhibit the properties of Tables 3 and 4 for the specified condition. Tensile and hardness tests shall be made in only one precipitation heat treated c

31、ondition. Unless otherwise specified, the precipitation heat treated testing condition shall be H925 (See 3.3.3 and 3.4.2.3). TABLE 2 - PRECIPITATION HEAT TREAT PARAMETERS Condition Temperature Minimum Time at Heat H900 900 F 10 (482 C 6) 90 minutes H925 925 F 10 (496 C 6) 90 minutes H1000 1000 F 10

32、 (538 C 6) 90 minutes H1025 1025 F 10 (552 C 6) 90 minutes H1100 1100 F 10 (593 C 6) 90 minutes H1150 1150 F 10 (621 C 6) 90 minutes SAE INTERNATIONAL AMS5355J Page 4 of 11_ 3.5.4 Tensile specimens used for master heat qualification may be heat treated separately from castings. 3.6 Properties Confor

33、mance shall be based upon testing of separately-cast specimens unless purchaser specifies integrally-cast specimens or specimens machined from castings. Properties for integrally-cast specimens or specimens machined from castings shall be specified by purchaser (See 8.5). 3.6.1 Room Temperature Tens

34、ile Properties Shall be as specified in 3.6.1.1, determined in accordance with ASTM E 8/E 8M. Properties other than those listed may be defined as specified in AMS2360. 3.6.1.1 Separately-Cast Specimens Shall be as shown in Table 3. TABLE 3A - MINIMUM TENSILE PROPERTIES, INCH/POUND UNITS Condition (

35、See 3.5.3) Tensile Strengthksi Yield Strength at 0.2% Offset ksi Elongationin 4D, % Reduction of Area, % H900 180 160 6 15 H925 180 150 6 15 H1000 150 130 8 20 H1025 150 130 10 20 H1100 130 120 10 25 H1150 125 110 12 25 TABLE 3B - MINIMUM TENSILE PROPERTIES, SI UNITS Condition (See 3.5.3) Tensile St

36、rengthMPa Yield Strength at 0.2% Offset MPa Elongationin 4D, % Reduction of Area, % H900 1241 1103 6 15 H925 1241 1034 6 15 H1000 1034 896 8 20 H1025 1034 896 10 20 H1100 896 827 10 25 H1150 862 758 12 25 3.6.2 Hardness Shall be as follows, determined in accordance with ASTM E 18. 3.6.2.1 Castings C

37、astings, which are heat treated to the condition of 3.3, shall have hardness not higher than 36 HRC. SAE INTERNATIONAL AMS5355J Page 5 of 11_ 3.6.2.2 Alternative Hardness Requirements Shall be not lower than shown in Table 4 for the corresponding precipitation heat treated condition. TABLE 4 - MINIM

38、UM HARDNESS Condition (See 3.5.3) HardnessHRC H900 40 H925 40 H1000 34 H1025 34 H1100 30 H1150 28 3.6.2.3 Representative Specimens Hardness not applicable. 3.7 Quality 3.7.1 Castings, as received by purchaser, shall be uniform in quality and condition. Castings shall, to the extent defined in 3.7.2,

39、 3.7.3, and 3.7.4, or in supplemental standards specified by the purchaser, be free from porosity, foreign materials, and imperfections detrimental to their performance. Castings shall be free of cracks, laps, hot tears, and cold shuts, and free of scale and other surface contamination which would o

40、bscure defects. 3.7.1.1 Unless otherwise specified, castings shall be sufficiently cleaned such that, after passivation by purchaser, the cast surfaces shall meet the corrosion test requirement of AMS2700. 3.7.2 Castings shall be produced under radiographic control. This control shall consist of rad

41、iographic examination of each casting part number until foundry manufacturing controls in accordance with 4.4.2 have been established. Additional radiography shall be conducted in accordance with the frequency of inspection specified by purchaser or as necessary to ensure continued maintenance of in

42、ternal quality. 3.7.2.1 Radiographic inspection shall be conducted in accordance with ASTM E 1742 or another method specified by purchaser. 3.7.3 When specified, additional nondestructive testing shall be performed as follows: 3.7.3.1 Fluorescent penetrant inspection in accordance with ASTM E 1417 o

43、r another method specified by purchaser. 3.7.3.2 Magnetic particle inspection in accordance with ASTM E 1444 or another method specified by purchaser. 3.7.4 Acceptance standards for radiographic, magnetic particle, fluorescent penetrant, visual, and other inspection methods shall be agreed upon by p

44、urchaser and vendor (See 8.2.8). AMS2175 may be used to specify acceptance standards (casting grade) and frequency of inspection (casting class). 3.7.4.1 When acceptance standards are not specified, Grade C of AMS2175 shall apply for each applicable method of inspection. 3.7.5 Castings shall not be

45、peened, plugged, impregnated, or welded unless authorized by purchaser. 3.7.5.1 When authorized by purchaser, welding in accordance with AMS2694 or another welding program acceptable to purchaser may be used. SAE INTERNATIONAL AMS5355J Page 6 of 11_ 4. QUALITY ASSURANCE PROVISIONS 4.1 Responsibility

46、 for Inspection The vendor of castings shall supply all samples for vendors tests and shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the castings conform to specified requi

47、rements. 4.2 Classification of Tests 4.2.1 Acceptance Tests Composition (3.1), tensile properties in H925 condition (3.6.1), hardness of castings (3.6.2.1), and applicable requirements of quality (3.7) are acceptance tests and shall be performed as specified in 4.3. 4.2.2 Periodic Tests Tensile properties in other than condition H925 (3.6.1), corrosion resistance (3.7.1.1), and radiographic soundness (3.7.2) are periodic tests and shall be performed at a frequency sel