SAE AMS 5357D-2017 Steel Corrosion-Resistant Investment Castings 15Cr - 4 6Ni - 0 22Cb - 2 8Cu Solution Heat Treated Precipitation Hardenable (UNS J92110).pdf

1、 SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising there

2、from, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions. Copyright 2017 SAE International All rights reserved. No part of this p

3、ublication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-497

4、0 (outside USA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/standards.sae.org/AMS5357D AEROSPACE MATERIAL SPECIFICATION AMS5357 REV. D Issued 1978-10 Reaffirmed 2006-04 Revi

5、sed 2017-06 Superseding AMS5357C Steel, Corrosion-Resistant, Investment Castings 15Cr - 4.6Ni - 0.22Cb - 2.8Cu Solution Heat Treated, Precipitation Hardenable (Composition similar to UNS J92110) RATIONALE AMS5357D revises Quality (3.7.4.1), Reports (4.5.1) and Identification (5.1.1), and is a Five-Y

6、ear Review and update of this specification. 1. SCOPE 1.1 Form This specification covers a corrosion-resistant steel in the form of investment castings. 1.2 Application These castings have been used typically for parts which will be machined in the solution heat treated condition and, after precipit

7、ation heat treatment, will require good corrosion resistance and strength up to 600 F (316 C), but usage is not limited to such applications (see 8.3). 1.2.1 Certain processing procedures and service conditions may cause these castings to become subject to stress-corrosion cracking; ARP1110 recommen

8、ds practices to minimize such conditions. Where stress-corrosion is considered to be a factor, precipitation heat treatment should be performed at a temperature not lower than 1000 F (538 C). 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the date of the purchase order for

9、ms a part of this specification to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that

10、 document shall apply. SAE INTERNATIONAL AMS5357D Page 2 of 11 2.1 SAE Publications Available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or +1 724-776-4970 (outside USA), www.sae.org. AMS2175 Castings, Classification and Inspe

11、ction of AMS2248 Chemical Check Analysis Limits Corrosion and Heat-Resistant Steels and Alloys, Maraging and Other Highly-Alloyed Steels, and Iron Alloys AMS2360 Room Temperature Tensile Properties of Castings AMS2694 In-Process Welding of Castings AMS2700 Passivation of Corrosion Resistant Steels A

12、MS2804 Identification Castings AMS5346 Steel, Corrosion-Resistant, Investment Castings 15Cr - 4.6Ni - 0.22Cb (Nb) - 2.8Cu Solution and Precipitation Heat Treated (H925) 180 ksi (1241 MPa) Tensile Strength (15-5) AMS5347 Steel, Corrosion-Resistant, Investment Castings 15Cr - 4.6Ni - 0.22Cb (Nb) - 2.8

13、Cu Solution and Precipitation Heat Treated (H1000) 150 ksi (1034 MPa) Tensile Strength (15-5) AMS5356 Steel, Corrosion Resistant, Investment Castings 15Cr - 4.6Ni - 0.22Cb - 2.8Cu Solution and Precipitation Heat Treated (H1100) 130 ksi (896 MPa) Tensile Strength AMS5400 Steel, Corrosion-Resistant, I

14、nvestment Castings 15Cr - 4.6Ni - 0.22Cb - 2.8Cu Solution and Precipitation Heat Treated (H935) 170 ksi (1172 MPa) Tensile Strength AMS-H-6875 Heat Treatment of Steel Raw Materials ARP1110 Minimizing Stress Corrosion Cracking in Wrought Forms of Steels and Corrosion Resistant Steels and Alloys ARP19

15、17 Clarification of Terms Used in Aerospace Metals Specifications 2.2 ASTM Publications Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM E8/E8M Tension Testing of Metallic Materials ASTM E18 Rockwell Hard

16、ness and Rockwell Superficial Hardness of Metallic Materials ASTM E353 Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys ASTM E1417/E1417M Liquid Penetrant Testing ASTM E1444/E1444M Magnetic Particle Testing ASTM E1742E1742M Radiographic Examinat

17、ion SAE INTERNATIONAL AMS5357D Page 3 of 11 3. TECHNICAL REQUIREMENTS 3.1 Composition Castings shall conform to the percentages by weight shown in Table 1, determined by wet chemical methods in accordance with ASTM E353, by spectrochemical methods, or by other analytical methods acceptable to purcha

18、ser (see 8.2.1 and 8.2.2). Table 1 - Composition Element Min Max Carbon Manganese Silicon Phosphorus Sulfur Chromium Nickel Columbium Copper Tantalum Nitrogen - - 0.50 - - 14.00 4.20 0.15 2.50 - - 0.05 0.60 1.00 0.025 0.025 15.50 5.00 0.30 3.20 0.05 0.05 3.1.1 Producer may test for any element not l

19、isted in Table 1 and include this analysis in the report of 4.5. Limits of acceptability may be specified by purchaser (see 8.2.3). 3.1.2 Check Analysis Composition variations shall meet the applicable requirements of AMS2248. 3.2 Melting Practice Castings and specimens shall be poured at casting pr

20、oducers facility either from a melt (see 8.2.4) of a master heat, or directly from a master heat (see 8.2.5). 3.2.1 Revert (gates, sprues, risers, and rejected castings) may be used only in the preparation of master heats; revert shall not be remelted directly, without refining, for pouring of casti

21、ngs. Melting revert creates a new master heat. 3.2.2 Portions of two or more qualified master heats (see 3.4.2) may be melted together and poured into castings using a procedure authorized by purchaser (see 8.2.6). 3.2.3 If modifications such as alloy additions or replenishments are made at remelt b

22、y the producer, producer shall have a written procedure acceptable to purchaser which defines the controls, tests, and traceability criteria for both castings and separately-cast specimens. Control factors of 4.4.2.2 shall apply. 3.3 Condition Castings shall be solution heat treated, except as speci

23、fied in 3.3.1 or 3.3.2. 3.3.1 When specified by or when acceptable to purchaser, castings shall be solution heat treated twice. 3.3.2 When specified by purchaser, castings shall be homogenization and solution heat treated. 3.3.3 Precipitation heat treatment of castings shall not be performed by vend

24、or unless purchaser specifies that castings are to be supplied in one of the age conditions specified in 3.5.3 (see 8.5). 3.4 Test Specimens Specimens shall be either separately-cast, integrally-cast (see 8.2.7), or machined from casting, and shall conform to 3.2. SAE INTERNATIONAL AMS5357D Page 4 o

25、f 11 3.4.1 If specimens are separately-cast, producer shall have a written procedure acceptable to purchaser. Control factors of 4.4.2.2 shall apply. 3.4.2 Each master heat shall be qualified by evaluation of chemical and tensile specimens. 3.4.2.1 If alloy additions or replenishments are made at re

26、melt as in 3.2.3, the frequency of sampling and testing used by the producer for qualification to 3.4.2 shall be acceptable to purchaser. 3.4.2.2 Tensile tests of 3.4.2 are not required if these tests are conducted using integrally-cast specimens (4.3.3.2) or specimens machined from castings (4.3.3.

27、3). 3.4.2.3 Tensile specimens shall be heat treated to the H925 condition of 3.5.2. Qualifications of separately-cast specimens to conditions other than H925 need be performed only when specifically required by purchaser (see 8.5). 3.4.3 Chemical Analysis Specimens Shall be of any convenient size an

28、d shape. 3.4.4 Tensile Specimens Shall be of standard proportions in accordance with ASTM E8/E8M with 0.250 inch (6.35 mm) diameter at the reduced parallel gage section. 3.4.4.1 Separately-cast and integrally-cast specimens may be either cast to size or cast oversize, and subsequently machined to 0.

29、250 inch (6.35 mm) diameter. 3.4.4.2 When integrally-cast specimens or specimens machined from casting are specified, specimen size and location shall be agreed upon by purchaser and producer (see 8.2.8 and 8.5). 3.5 Heat Treatment Castings and representative tensile specimens shall be heat treated

30、in accordance with AMS-H-6875 except as specified in 3.5.1 and 3.5.2. 3.5.1 Castings and Specimens 3.5.1.1 Homogenization Heat Treatment (When Specified) Heat to 2100 F 25 F (1149 C 14 C), hold at heat for not less than 90 minutes, and cool as required. 3.5.1.2 Solution Heat Treatment Heat to 1900 F

31、 25 F (1038 C 14 C), hold at heat for 60 minutes per inch (25.4 mm) of section thickness but not less than 30 minutes, and cool as required to below 90 F (32 C). 3.5.2 Specimens After heat treatment in accordance with 3.5.1, specimens shall, unless otherwise specified, be heat treated in accordance

32、with the following: 3.5.2.1 Precipitation Heat Treatment Heat to 925 F 10 F (496 C 6 C), hold at heat for not less than 90 minutes, and cool in air. SAE INTERNATIONAL AMS5357D Page 5 of 11 3.5.3 Alternative Precipitation Heat Treatments Castings, when specified, and representative tensile specimens,

33、 precipitation heat treated to a particular condition in accordance with the corresponding temperatures and times shown in Table 2 and cooled in air, shall exhibit the properties of Table 3 for the specified condition. Tensile and hardness tests shall be made in only one precipitation heat treated c

34、ondition. Unless otherwise specified, the precipitation heat treated testing condition shall be H925 (see 3.3.3 and 3.4.2.3). Table 2 - Precipitation heat treatment parameters Condition Temperature Time H925 925 F 10 F (496 C 6 C) 90 minutes min H935 935 F 10 F (502 C 6 C) 4 hours 0.25 hour H1000 10

35、00 F 10 F (538 C 6 C) 4 hours 0.25 hour H1100 1100 F 10 F (593 C 6 C) 4 hours 0.25 hour H1150 1150 F 10 F (621 C 6 C) 4 hours 0.25 hour 3.5.4 Tensile specimens used for master heat qualification may be heat treated separately from castings. 3.6 Properties Conformance shall be based upon testing of s

36、eparately-cast specimens unless purchaser specifies integrally-cast specimens or specimens machined from a casting. Properties for integrally-cast specimens or specimens machined from casting shall be specified by purchaser (see 8.5). 3.6.1 Room Temperature Tensile Properties Shall be as specified i

37、n 3.6.1.1, determined in accordance with ASTM E8/E8M. Properties other than those listed may be defined as specified in AMS2360. 3.6.1.1 Separately-Cast Specimens Shall be as shown in Table 3. Table 3 Table 3A - Minimum tensile properties, inch/pound units Condition (see 3.5.3) Tensile Strength ksi

38、Yield Strength at 0.2% Offset ksi Elongation in 4D, % Reduction of Area, % H925 H935 H1000 H1100 H1150 180 170 150 130 125 160 150 130 120 110 6 7 8 8 12 15 16 18 20 30 Table 3B - Minimum tensile properties, SI units Condition (see 3.5.3) Tensile Strength MPa Yield Strength at 0.2% Offset MPa Elonga

39、tion in 4D, % Reduction of Area, % H925 H935 H1000 H1100 H1150 1241 1172 1034 896 862 1103 1034 896 827 758 6 7 8 8 12 15 16 18 20 30 SAE INTERNATIONAL AMS5357D Page 6 of 11 3.6.2 Hardness Shall be as follows, determined in accordance with ASTM E18. 3.6.2.1 Castings Castings heat treated to the cond

40、ition of 3.3 shall have hardness not higher than 36 HRC. 3.6.2.2 Alternative Hardness Requirements Shall be as shown in Table 4 for the corresponding precipitation heat treated condition. Table 4 - Hardness Condition (see 3.5.3) Hardness HRC H925 40 to 47 H935 38 to 47 H1000 35 to 42 H1100 33 to 40

41、H1150 28 to 36 3.6.2.3 Representative Specimens Hardness not applicable. 3.7 Quality 3.7.1 Castings, as received by purchaser, shall be uniform in quality and condition. Castings shall, to the extent defined in 3.7.2, 3.7.3, and 3.7.4, or in supplemental standards specified by the purchaser, be free

42、 from porosity, foreign materials, and imperfections detrimental to their performance. Castings shall be free of cracks, laps, hot tears, and cold shuts, and free of scale and other surface contamination which would obscure defects. 3.7.1.1 Unless otherwise specified, castings shall be sufficiently

43、cleaned such that, after passivation by purchaser, the cast surfaces shall meet the corrosion test requirement of AMS2700. 3.7.2 Castings shall be produced under radiographic control. This control shall consist of radiographic examination of each casting part number until foundry manufacturing contr

44、ols, in accordance with 4.4.2, have been established. Additional radiography shall be conducted in accordance with the frequency of inspection specified by purchaser or as necessary to ensure continued maintenance of internal quality. 3.7.2.1 Radiographic inspection shall be conducted in accordance

45、with ASTM E1742/E1742M or another method specified by purchaser. 3.7.3 When specified, additional nondestructive testing shall be performed as follows: 3.7.3.1 Fluorescent penetrant inspection in accordance with ASTM E1417E/1417M or another method specified by purchaser. 3.7.3.2 Magnetic particle in

46、spection in accordance with ASTM E1444/E1444M or another method specified by purchaser. 3.7.4 Acceptance standards for radiographic, fluorescent penetrant, magnetic particle, visual, and other inspection methods shall be as agreed upon by purchaser and producer (see 8.2.8). AMS2175 may be used to sp

47、ecify acceptance standards (casting grade) and frequency of inspection (casting class). 3.7.4.1 When acceptance standards are not specified, castings shall meet Grade C of AMS2175 and radiographic indications of gas holes, sand spots, and inclusions shall be cause for rejection when closer to the ed

48、ge than twice their maximum dimension. SAE INTERNATIONAL AMS5357D Page 7 of 11 3.7.5 Castings shall not be peened, plugged, impregnated, or welded unless authorized by purchaser. 3.7.5.1 When authorized by purchaser, welding in accordance with AMS2694 or another welding program acceptable to purchas

49、er may be used. 4. QUALITY ASSURANCE PROVISIONS 4.1 Responsibility for Inspection The producer of castings shall supply all samples for producers tests and shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the castings conform t