SAE AMS 5377G-2013 Nickel Alloy Corrosion and Heat-Resistant Investment Castings 73Ni - 12Cr - 4 5Mo - 2 0Cb - 0 70Ti - 0 05C - 6 0Al - 0 010B - 0 10Zr Vacuum Cast As-Cast (UNS N07.pdf

1、_ SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising there

2、from, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions. Copyright 2013 SAE International All rights reserved. No part of this p

3、ublication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-497

4、0 (outside USA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/www.sae.org/technical/standards/AMS5377G AEROSPACE MATERIAL SPECIFICATION AMS5377 REV. G Issued 1971-05 Revised 2

5、013-12 Superseding AMS5377F Nickel Alloy, Corrosion and Heat-Resistant, Investment Castings 73Ni - 12Cr - 4.5Mo - 2.0Cb - 0.70Ti - 0.05C - 6.0Al - 0.010 - 0.10Zr Vacuum Cast, As-Cast (Composition similar to UNS N07713) RATIONALE AMS5377G revises Stress Rupture Testing (3.6.2.2), Control Factors (4.4

6、.3.2) and Reports (4.5) and is a Five Year Review and update of this specification. 1. SCOPE 1.1 Form This specification covers a corrosion and heat-resistant nickel alloy in the form of investment castings. 1.2 Application These castings have been used typically for small parts, such as turbine bla

7、des and integral wheels, requiring high strength up to 1800 F (982 C) and oxidation resistance up to 2000 F (1093 C), but usage is not limited to such applications. 2. APPLICABLE DOCUMENTS The issue of the following documents in effect on the date of the purchase order forms a part of this specifica

8、tion to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been canceled and no superseding document has been specified, the last published issue of that document shall apply. 2.1 S

9、AE Publications Available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.org. AMS2175 Castings, Classification and Inspection of AMS2269 Chemical Check Analysis Limits, Nickel, Nickel Alloys,

10、 and Cobalt Alloys AMS2360 Room Temperature Tensile Properties of Castings AMS2362 Stress-Rupture Properties of Castings SAE INTERNATIONAL AMS5377G Page 2 of 9 AMS2694 In-Process Welding of Castings AMS2804 Identification, Castings 2.2 ASTM Publications Available from ASTM International, 100 Barr Ha

11、rbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM E8/ E 8M Tension Testing of Metallic Materials ASTM E139 Conducting Creep, Creep-Rupture, and Stress-Rupture Tests of Metallic Materials ASTM E354 Chemical Analysis of High-Temperature, Electrical, Mag

12、netic, and Other Similar Iron, Nickel, and Cobalt Alloys ASTM E1417/E 1417M Liquid Penetrant Testing ASTM E1742/E 1742M Radiographic Examination 3. TECHNICAL REQUIREMENTS 3.1 Composition Shall conform to the percentages by weight shown in Table 1, determined by wet chemical methods in accordance wit

13、h ASTM E 354, by spectrochemical methods, or by other analytical methods acceptable to purchaser (See 8.2.1 and 8.2.2). TABLE 1 COMPOSITION Element min max Carbon 0.03 0.07 Manganese - 0.25 Silicon - 0.50 Phosphorus - 0.015 Sulfur - 0.015 Chromium 11.00 13.00 Molybdenum 3.80 5.20 Columbium (Niobium)

14、 1.50 2.50 Titanium 0.50 0.90 Aluminum 5.50 6.50 Boron 0.005 0.015 Zirconium 0.05 0.15 Cobalt - 1.00 Tantalum - 0.15 Iron - 0.50 Copper - 0.50 Other Elements (3.1.1) - - Nickel remainder 3.1.1 Vendor may test for any element not otherwise listed in Table 1 and include this analysis in the report of

15、4.5. Limits of acceptability may be specified by purchaser (See 8.2.3). 3.1.2 Check Analysis Composition variations shall meet the applicable requirements of AMS2269. 3.2 Melting Practice Castings and specimens shall be poured at casting vendors facility either from a melt (See 8.2.4) of a master he

16、at, or directly from a master heat (See 3.4.2 and 8.2.5). SAE INTERNATIONAL AMS5377G Page 3 of 9 3.2.1 The metal for castings and specimens shall be melted and poured under vacuum without loss of vacuum between melting and pouring. When authorized by purchaser (See 8.2.6), protective atmosphere may

17、be used in lieu of vacuum for pouring of castings. 3.2.2 Revert (gates, sprues, risers, and rejected castings) may be used only in the preparation of master heats; revert shall not be remelted directly without refining for pouring of castings. Melting of revert creates a new master heat. 3.2.3 Porti

18、ons of two or more qualified master heats (See 3.4.2) may be melted together and poured into castings using a procedure authorized by purchaser. 3.2.4 If melts (See 8.2.4) are modified by replenishment (See 8.2.7), vendor shall have a written procedure acceptable to purchaser which defines the contr

19、ols, test, and traceability criteria for both castings and separately-cast specimens. Control factors of 4.4.2.2 shall apply. 3.3 Condition Castings shall be delivered in the as-cast condition. 3.4 Test Specimens Specimens shall be either separately-cast, integrally-cast (See 8.2.8), or machined fro

20、m a casting, and shall conform to 3.2. 3.4.1 If specimens are separately-cast, vendor shall have a written procedure acceptable to purchaser. Control factors of 4.4.2.2 shall apply. 3.4.2 Each master heat shall be qualified by evaluation of chemical, tensile, and stress-rupture specimens. 3.4.2.1 If

21、 replenishments are made at remelt as in 3.2.3, frequency of sampling and testing used by the vendor for qualification to 3.4.2 shall be acceptable to purchaser. 3.4.2.2 Tensile and stress-rupture tests of 3.4.2 are not required if these tests are conducted using integrally-cast specimens (4.3.3.2)

22、and/or specimens machined-from-casting (4.3.3.3). 3.4.3 Chemical Analysis Specimens Shall be of any convenient size and shape. 3.4.4 Tensile and Stress-Rupture Specimens Shall be of standard proportions in accordance with ASTM E 8/E 8M (See 8.3), or ASTM E 139, respectively. 3.4.4.1 Separately-cast

23、and integrally-cast specimens may be either cast to size, and/or cast oversize and subsequently machined to 0.250-inch (6.35-mm) diameter. 3.4.4.2 When integrally-cast specimens or specimens machined-from-casting are specified, specimen size and location shall be agreed upon by purchaser and vendor

24、(See 8.2.9 and 8.5). 3.5 Heat Treatment Not applicable. 3.6 Properties Conformance shall be based upon testing of separately-cast specimens unless purchaser specifies integrally-cast specimens or specimens machined-from-casting. Properties for integrally-cast specimens and specimens machined-from-ca

25、sting shall be as specified by purchaser (See 8.5). SAE INTERNATIONAL AMS5377G Page 4 of 9 3.6.1 Room Temperature Tensile Properties Shall be as specified in 3.6.1.1, determined in accordance with ASTM E 8/E 8M (See 8.3). Properties other than those listed in Table 2 may be defined as specified in A

26、MS2360. 3.6.1.1 Separately-Cast Specimens Shall be as shown in Table 2. TABLE 2 - MINIMUM TENSILE PROPERTIES OF SEPARATELY-CAST SPECIMENS Property Value Tensile Strength 110 ksi (758 MPa) Yield Strength at 0.2% Offset 100 ksi (689 MPa) Elongation in 4D 5% Reduction of Area 8% 3.6.2 Stress-Rupture Pr

27、operties at 1800 F (982 C) Shall be as follows, determined in accordance with ASTM E 139. Properties other than those listed may be defined as specified in AMS 2362. 3.6.2.1 Specimens, maintained at 1800 F 3 (982 C 2) while a load sufficient to produce an initial axial stress of 22.0 ksi (152 MPa) o

28、r higher is applied continuously, shall not rupture in less than 30 hours. The test shall be continued to rupture without change of load. Elongation after rupture, measured at room temperature, shall be not less than 5% in 4D. 3.6.2.2 The test of 3.6.2.1 may be conducted using incremental loading. I

29、n such case, the load required to produce an initial axial stress of 22.0 ksi (152 MPa) or higher shall be used to rupture or for 30 hours, whichever occurs first. After the 30 hours and at intervals of 8 hours, minimum, thereafter, the stress shall be increased in increments of 2.0 ksi (14.0 MPa).

30、Time to rupture and elongation requirements shall be as specified in 3.6.2.1. 3.6.3 Hardness Not applicable. 3.7 Quality 3.7.1 Castings, as received by purchaser, shall be uniform in quality and condition, sound, and free from foreign materials and from imperfections detrimental to usage of the cast

31、ings. Castings shall be free of cracks, laps, hot tears, and cold shuts, and free of scale and other process induced surface contamination which would obscure defects. 3.7.2 Castings shall be produced under radiographic control. This control shall consist of radiographic examination of each casting

32、part number until foundry manufacturing controls in accordance with 4.4.2 have been established. Additional radiography shall be conducted in accordance with the frequency of inspection specified by purchaser, or as necessary to ensure continued maintenance of internal quality. 3.7.2.1 Radiographic

33、inspection shall be conducted in accordance with ASTM E 1742/E 1742M or other method specified by purchaser. 3.7.3 When specified, castings shall be subjected to fluorescent penetrant inspection in accordance with ASTM E 1417/E 1417M or other method specified by purchaser. 3.7.4 Acceptance standards

34、 for radiographic, fluorescent penetrant, visual, and other inspection methods shall be as agreed upon by purchaser and vendor (See 8.2.9). AMS2175 may be used to specify acceptance standards (casting grade) and frequency of inspection (casting class). 3.7.4.1 When acceptance standards are not speci

35、fied, Grade C of AMS2175 as applicable to steel castings shall apply for each specified method of inspection. SAE INTERNATIONAL AMS5377G Page 5 of 9 3.7.5 Castings shall not be peened, plugged, impregnated, or welded unless authorized by purchaser. 3.7.5.1 When authorized by purchaser, welding in ac

36、cordance with AMS2694 or other welding program acceptable to purchaser may be used. 4. QUALITY ASSURANCE PROVISIONS 4.1 Responsibility for inspection The vendor of castings shall supply all samples for vendors tests and shall be responsible for the performance of all required tests. Purchaser reserv

37、es the right to sample and to perform any confirmatory testing deemed necessary to ensure that the castings conform to specified requirements. 4.2 Classification of Tests 4.2.1 Acceptance Tests Composition (3.1), room temperature tensile properties (3.6.1), stress rupture properties (3.6.2) and the

38、applicable requirements of quality (3.7) are acceptance tests and shall be performed as specified in 4.3. 4.2.2 Periodic Tests Radiographic soundness (3.7.2) is a periodic test and shall be performed at a frequency selected by the vendor unless a frequency of testing is specified by purchaser. 4.2.3

39、 Preproduction Tests All technical requirements are preproduction tests and shall be performed on sample castings (4.3.2), when a change in control factors occurs (4.4.2.2), and when purchaser deems confirmatory testing to be required. 4.3 Sampling and Testing The minimum testing performed by vendor

40、 shall be in accordance with the following: 4.3.1 One chemical analysis specimen or a casting from each master heat shall be tested for conformance with Table 1; if 3.4.2.1 applies, test frequency shall be acceptable to purchaser. 4.3.2 One preproduction casting in accordance with 4.4 shall be teste

41、d to requirements of the casting drawing and to all technical requirements. 4.3.2.1 Dimensional inspection sample quantity shall be as specified by purchaser. 4.3.3 Room temperature tensile property and stress-rupture tests shall be conducted to determine conformance with 3.6.1 and 3.6.2. Sampling a

42、nd test frequency is dependent upon the type and origin of the specimen specified by purchaser (See 3.4.4 and 3.6) or selected by vendor (See 4.3.3.4). When 3.4.2.1 applies, specimen source and test frequency shall be acceptable to purchaser. 4.3.3.1 For separately-cast specimens in the as-cast cond

43、ition, two specimens from each master heat shall be tested; one for conformance to Table 2 and one for conformance to 3.6.2. 4.3.3.2 For integrally-cast specimens in the as-cast condition, two specimens shall be randomly selected from each lot and tested for conformance with properties specified by

44、purchaser (See 3.6 and 8.5). 4.3.3.3 For specimens machined-from-casting, one casting shall be randomly selected from each lot and tested in the as-cast condition at each location shown on the engineering drawing for conformance with properties specified by purchaser (See 3.6 and 8.5). 4.3.3.3.1 Whe

45、n size and location of specimens are not shown, two specimens shall be tested, one from the thickest section and one from the thinnest section. Once established under 4.4.2.2, test locations may be changed only as agreed upon by purchaser and vendor. SAE INTERNATIONAL AMS5377G Page 6 of 9 4.3.3.4 Wh

46、en acceptable to purchaser, specimens machined-from-casting may be used in lieu of both separately-cast and integrally-cast specimens, and integrally-cast specimens may be used in lieu of separately-cast specimens. In each case, the resultant properties shall conform to the requirements of 3.6 or to

47、 alternative requirements specified by purchaser (See 8.5). 4.3.3.4.1 When specimens are selected for test as in 4.3.3.4 from an origin other than that specified by purchaser, vendor shall include in the report of 4.5 a description of the source of the specimen that was tested. 4.3.3.5 When casting

48、size, section thickness, gating method, or other factors do not permit conformance with 4.3.3.2 or 4.3.3.3, sampling and testing shall be agreed upon by purchaser and vendor. 4.3.4 Castings shall be inspected in accordance with 3.7 to the methods, frequency, and acceptance standards specified by pur

49、chaser. 4.4 Approval 4.4.1 Sample casting(s) from new or reworked master patterns produced under the casting procedure of 4.4.2 shall be approved by purchaser before castings for production use are supplied, unless such approval be waived by purchaser. 4.4.2 For each casting part number, vendor shall establish parameters for process control factors that will consistently produce castings and test specimens meeting the