SAE AMS 5583E-2013 Nickel Alloy Corrosion and Heat-Resistant Seamless Tubing 72Ni - 15 5Cr - 0 95Cb (Nb) - 2 5Ti - 0 70Al - 7 0Fe Vacuum Melted Solution Heat Treated Precipitation .pdf

1、_SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising theref

2、rom, is the sole responsibility of the user.”SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions.Copyright 2012 SAE InternationalAll rights reserved. No part of this publication may b

3、e reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE.TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada)Tel: +1 724-776-4970 (outside USA)Fax

4、: 724-776-0790Email: CustomerServicesae.orgSAE WEB ADDRESS: http:/www.sae.orgSAE values your input. To provide feedbackon this Technical Report, please visithttp:/www.sae.org/technical/standards/AMS5583EAEROSPACEMATERIALSPECIFICATIONAMS5583 REV. EIssued 1977-07Revised 2013-01Superseding AMS5583DNick

5、el Alloy, Corrosion and Heat-Resistant, Seamless Tubing72Ni - 15.5Cr - 0.95Cb (Nb) - 2.5Ti - 0.70Al - 7.0FeVacuum MeltedSolution Heat Treated, Precipitation Hardenable to 170 ksi (1172 MPa) Tensile Strength(Composition similar to UNS N07750)RATIONALEAMS5583E is a Five Year Review and update of this

6、specification.1. SCOPE1.1 FormThis specification covers a precipitation hardenable corrosion and heat-resistant nickel alloy in the form of seamless tubing. 1.2 ApplicationThis tubing has been used typically for fluid lines requiring high strength up to 1300 F (704 C) and oxidation resistance up to

7、1800 F (982 C), but usage is not limited to such applications. Parts may be formed and then heat treated to improve strength at elevated temperatures. 2. APPLICABLE DOCUMENTSThe issue of the following documents in effect on the date of the purchase order forms a part of this specification to the ext

8、ent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that document shall apply.SAE AMS5583E Page 2

9、of 72.1 SAE PublicationsAvailable from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or 724-776-4970 (outside USA), www.sae.org.AMS2263 Tolerances, Nickel, Nickel Alloy, and Cobalt Alloy TubingAMS2269 Chemical Check Analysis Limits, N

10、ickel, Nickel Alloys, and Cobalt AlloysAMS2371 Quality Assurance Sampling and Testing, Corrosion and Heat-Resistant Steels and Alloys, Wrought Products and Forging StockAMS2634 Ultrasonic Inspection, Thin Wall Metal TubingAMS2750 PyrometryAMS2807 Identification, Carbon and Low-Alloy Steels, Corrosio

11、n and Heat-Resistant Steels and Alloys, Sheet, Strip, Plate, and Aircraft Tubing2.2 ASTM PublicationsAvailable from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org.ASTM E 8/E 8M Tension Testing of Metallic MaterialsASTM E 18

12、 Rockwell Hardness of Metallic MaterialsASTM E 112 Determining Average Grain SizeASTM E 354 Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt AlloysASTM E 426 Electromagnetic (Eddy-Current) Examination of Seamless and Welded Tubular Products, Tit

13、anium, Austenitic Stainless Steel and Similar AlloysASTM E 1417 Liquid Penetrant Testing3. TECHNICAL REQUIREMENTS3.1 CompositionShall conform to the percentages by weight shown in Table 1, determined by wet chemical methods in accordance with ASTM E 354, by spectrochemical methods, or by other analy

14、tical methods acceptable to purchaser.SAE AMS5583E Page 3 of 7TABLE 1 - COMPOSITIONElement min maxCarbon - 0.08Manganese - 0.35Silicon - 0.35Phosphorus - 0.015Sulfur - 0.010Chromium 14.00 17.00Nickel 70.00 -Columbium (Niobium) 0.70 1.20Titanium 2.25 2.75Aluminum 0.40 1.00Iron 5.00 9.00Cobalt (3.1.1)

15、 - 1.00Tantalum - 0.05Copper - 0.503.1.1 Determination not required for lot acceptance.3.1.2 Check AnalysisComposition variations shall meet the applicable requirements of AMS2269.3.2 Melting PracticeAlloy shall be multiple melted using consumable electrode practice in the remelt cycle. If consumabl

16、e electrode remelting is not performed in vacuum, electrodes which have been produced by vacuum induction melting shall be used for remelting.3.3 ConditionSolution heat treated, and unless solution heat treatment is performed in an atmosphere yielding a bright finish, pickled as required.3.4 Heat Tr

17、eatmentTubing shall be solution heat treated by heating to a temperature not lower than 1800 F (982 C), holding at the selected temperature within 25 F (14 C) for a time commensurate with cross-sectional thickness, and cooling at a rate equivalent to an air cool or faster. Pyrometry shall be in acco

18、rdance with AMS2750.3.5 FabricationTubing shall be produced by a seamless and drawn process. Any surface finishing operation applied to remove objectionable pits and blemishes shall be performed prior to solution heat treatment. Only light polishing to improve external surface appearance is permitte

19、d after solution heat treatment.SAE AMS5583E Page 4 of 73.6 PropertiesTubing shall conform to the following requirements:3.6.1 As Solution Heat Treated3.6.1.1 Tensile PropertiesShall be as shown in Table 2, determined in accordance with ASTM E 8/E 8M.TABLE 2 - SOLUTION HEAT TREATED TENSILE PROPERTIE

20、SProperty ValueTensile Strength, maximum 140 ksi (965 MPa)Yield Strength at 0.2% Offset, maximum 80 ksi (552 MPa)Elongation in 2 inches (50.8 mm) or 4D, minimumStrip SpecimenFull Tube30%35%3.6.1.2 Average Grain SizeShall be ASTM No. 5 or finer, determined in accordance with ASTM E 112.3.6.1.3 Flarab

21、ilitySpecimens as in 4.3.1 from tubing 0.188 to 2.000 inches (4.78 to 50.80 mm), inclusive, in nominal OD shall withstand flaring at room temperature, without formation of cracks or other visible defects, by being forced axially with steady pressure over a hardened and polished tapered steel pin hav

22、ing a 74-degree included angle to produce a flare having a permanent expanded OD not less than 1.20 times the original nominal OD.3.6.2 Response to Precipitation Heat TreatmentTubing shall have the following properties after being precipitation heat treated by heating to 1350 F 25 (732 C 14), holdin

23、g at heat for not less than 8 hours, cooling at a rate of 100 F (56 C) degrees per hour to 1150 F 25 (621 C 14), holding at 1150 F 25 (621 C 14) for 8 hours 0.5, and cooling at a rate equivalent to cooling in air. Instead of the 100 F (56 C) degrees per hour cooling rate to 1150 F 25 (621 C 14), tub

24、ing may be furnace cooled at any rate provided the time at 1150 F 25 (621 C 14) is adjusted to give a total precipitation heat treatment time of notless than 18 hours.3.6.2.1 Tensile PropertiesShall be as shown in Table 3, determined in accordance with ASTM E 8/E 8M.SAE AMS5583E Page 5 of 7TABLE 3 -

25、 MINIMUM TENSILE PROPERTIES AFTER PRECIPITATION HEAT TREATMENTProperty ValueTensile Strength 170 ksi (1172 MPa)Yield Strength at 0.2% Offset 115 ksi ( 793 MPa)Elongation in 2 inches (50.8 mm) or 4DStrip SpecimenFull Tube12%15%3.6.2.2 HardnessShould be not lower than 30 HRC, or equivalent (See 8.2),

26、determined in accordance with ASTM E 18. Tubing shall not be rejected on the basis of hardness if the tensile property requirements of 3.5.2.1 are acceptable, determined on specimens taken from the same sample as that with nonconforming hardness or from another sample with similar nonconforming hard

27、ness.3.7 QualityTubing, as received by purchaser, shall be uniform in quality and condition and shall have a finish conforming to the best practice for high quality aircraft tubing. It shall be smooth and free from grease, oil and other foreign matter, heavy scale or oxide, burrs, seams, tears, groo

28、ves, laminations, slivers, pits, and other imperfections detrimental to usage of the tubing. Surface imperfections such as handling marks, straightening marks, light mandrel and die marks, shallow pits, and scale pattern will not be considered injurious if the imperfections are removable within the

29、tolerances specified for wall thickness but removal of such imperfections is not required.3.7.1 When specified by purchaser (See 8.5), tubing shall be subjected to fluorescent penetrant inspection in accordance with ASTM E 1417, to ultrasonic inspection in accordance with AMS2634, to electromagnetic

30、 (eddy-current) inspection in accordance with ASTM E 426, or to any combination thereof. Tubing shall meet the requirements of acceptance criteria established by the cognizant engineering organization.3.8 TolerancesShall conform to all applicable requirements of AMS2263.4. QUALITY ASSURANCE PROVISIO

31、NS4.1 Responsibility for InspectionThe vendor of tubing shall supply all samples for vendors tests and shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the tubing conforms to

32、 specified requirements.4.2 Classification of Tests4.2.1 Acceptance TestsComposition (3.1), tensile properties (3.6.1.1) response to precipitation heat treatment (3.6.2.1), average grain size (3.6.1.2), hardness (3.6.2.2), nondestructive inspection when specified (3.7.1), and tolerances (3.8) are ac

33、ceptance tests and shall be performed on each heat or lot as applicable.SAE AMS5583E Page 6 of 74.2.2 Periodic TestsFlarability (3.6.1.3) is a periodic test and shall be performed at a frequency selected by the vendor unless frequency of testing is specified by purchaser.4.3 Sampling and TestingShal

34、l be in accordance with AMS2371 and the following:4.3.1 Specimens for flarability test (3.6.1.3) shall be full tubes or sections cut from a tube. The end of the specimen to be flared shall be cut square, with the cut end smooth and free from burrs, but not rounded.4.4 ReportsThe vendor of the produc

35、t shall furnish with each shipment a report showing the following results of tests and relevant information:4.4.1 For each heat:Composition.4.4.2 For each lot:Tensile properties solution heat treatedTensile properties and hardness precipitation heat treatedAverage grain sizeWhen specified, results o

36、f nondestructive inspection.4.4.3 A statement that the product conforms to the other technical requirements.4.4.4 Purchase order numberHeat and lot numbersAMS5583ESizeQuantity.4.5 Resampling and RetestingShall be in accordance with AMS2371.5. PREPARATION FOR DELIVERY5.1 SizesExcept when exact length

37、s or multiples of exact lengths are ordered, straight tubing will be acceptable in mill lengths of 6 to 24 feet (1.8 to 7.3 m) but not more than 25% of any shipment shall be supplied in lengths shorter than 10 feet (3 m).5.2 IdentificationShall be in accordance with AMS2807.SAE AMS5583E Page 7 of 75

38、.3 PackagingTubing shall be prepared for shipment in accordance with commercial practice and in compliance with applicable rules and regulations pertaining to the handling, packaging, and transportation of the tubing to ensure carrier acceptance and safe delivery.6. ACKNOWLEDGMENTA vendor shall ment

39、ion this specification number and its revision letter in all quotations and when acknowledging purchase orders.7. REJECTIONSTubing not conforming to this specification, or to modifications authorized by purchaser, will be subject to rejection.8. NOTES8.1 A change bar (|) located in the left margin i

40、s for the convenience of the user in locating areas where technical revisions, not editorial changes, have been made to the previous issue of this document. An (R) symbol to the left of the document title indicates a complete revision of the document, including technical revisions. Change bars and (

41、R) are not used in original publications, nor in documents that contain editorial changes only.8.2 Hardness conversion tables for metals are presented in ASTM E 140.8.3 Terms used in AMS are clarified in ARP1917.8.4 Dimensions and properties in inch/pound units and the Fahrenheit temperatures are pr

42、imary; dimensions and properties in SI units and the Celsius temperatures are shown as the approximate equivalents of the primary units and are presented only for information.8.5 Purchase documents should specify not less than the following:AMS5583ESize of tubing desired Whether non-destructive testing is required (See 3.7 1)Quantity of tubing desired.PREPARED BY AMS COMMITTEE “F“