SAE AMS 5854C-2015 Nickel Alloy Corrosion and Heat-Resistant Bars Wire Forgings and Rings 61Ni - 20 5Cr - 8 5Mo - 3 4Cb(Nb) - 1 3Ti - 5 0Fe Consumable Electrode or Vacuum Induction.pdf

1、_SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising theref

2、rom, is the sole responsibility of the user.”SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions.Copyright 2015 SAE InternationalAll rights reserved. No part of this publi

3、cation may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE.TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada)Tel: +1 724-776-4970 (out

4、side USA)Fax: 724-776-0790Email: CustomerServicesae.orgSAE WEB ADDRESS: http:/www.sae.orgSAE values your input. To provide feedbackon this Technical Report, please visithttp:/www.sae.org/technical/standards/AMS5854CAEROSPACEMATERIAL SPECIFICATIONAMS5854 REV. CIssued 1991-01Reaffirmed 2006-04Revised

5、2015-12Superseding AMS5854BNickel Alloy, Corrosion and Heat-Resistant, Bars, Wire, Forgings, and Rings61Ni -20.5Cr -8.5Mo -3.4Cb(Nb) -1.3Ti -5.0FeConsumable Electrode or Vacuum Induction MeltedSolution Heat Treated(Composition similar to UNS N07716)RATIONALEAMS5854C revises Condition (3.3.2), Proper

6、ties (3.5.1.2.3) and Reports (4.4), and is a Five Year Review and update of this specification.1. SCOPE1.1 FormThis specification covers a corrosion and heat-resistant nickel alloy in the form of bars, wire, forgings, flash welded rings, and extrusions 4 inches (102 mm) and under in nominal diameter

7、 or least distance between parallel sides, and stock for forging or flash welded rings.1.2 ApplicationThese products have been used typically for parts requiring both corrosion and oxidation resistance up to 1,000 F (538 C), and where such parts may require welding during fabrication and are then pr

8、ecipitation heat treated to develop required properties, but usage is not limited to such applications.2. APPLICABLE DOCUMENTSThe issue of the following documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a

9、 subsequent revision of a document unless a specific document issue is specified. When the referenced document has been cancelled and no superseding document has been specified, the last published issue of that document shall apply.2.1 SAE PublicationsAvailable from SAE International, 400 Commonweal

10、th Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or +1 724-776-4970 (outside USA), www.sae.org.AMS2261 Tolerances, Nickel, Nickel Alloy, and Cobalt Alloy Bars, Rods, and WireAMS2269 Chemical Check Analysis Limits, Nickel, Nickel Alloys, and Cobalt AlloysSAE INTERNATIONA

11、L AMS5854C Page 2 of 7AMS2371 Quality Assurance Sampling and Testing, Corrosion and Heat-Resistant Steels and Alloys, Wrought Products and Forging StockAMS2374 Quality Assurance Sampling and Testing, Corrosion and Heat-Resistant Steel and Alloy ForgingsAMS2750 PyrometryAMS2806 Identification Bars, W

12、ire, Mechanical Tubing, and Extrusions, Carbon and Alloy Steels and Corrosion and Heat-Resistant Steels and AlloysAMS2808 Identification ForgingsAMS7490 Rings, Flash Welded, Corrosion and Heat-Resistant Austenitic Steels, Austenitic-Type Iron, Nickel, or Cobalt Alloys, or Precipitation-Hardenable Al

13、loys2.2 ASTM PublicationsAvailable from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org.ASTM E8/E8M Tension Testing of Metallic MaterialsASTM E10 Brinell Hardness of Metallic MaterialsASTM E18 Rockwell Hardness of Metallic M

14、aterialsASTM E112 Determining Average Grain SizeASTM E354 Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys3. TECHNICAL REQUIREMENTS3.1 CompositionShall conform to the percentages by weight shown in Table 1, determined by wet chemical meth

15、ods in accordance with ASTM E354, by spectrochemical methods, or by other analytical methods acceptable to purchaser. Table 1 - CompositionElement min maxCarbonManganeseSiliconPhosphorusSulfurChromiumNickelMolybdenumColumbium (Niobium)TitaniumCobaltAluminumIron-19.0059.007.502.751.00-remainder0.030.

16、200.200.0150.01022.0063.009.504.001.601.000.35SAE INTERNATIONAL AMS5854C Page 3 of 73.1.1 Check AnalysisComposition variations shall meet the applicable requirements of AMS2269.3.2 Melting PracticeAlloy shall be produced by multiple melting using consumable electrode practice in the remelt cycle or

17、shall be induction melted under vacuum.3.3 ConditionThe product shall be supplied in the following condition:3.3.1 BarsHot finished and solution heat treated; round bars shall be ground or turned.3.3.2 Bars shall not be cut from plate (see 4.4.2).3.3.3 WireCold drawn and solution heat treated.3.3.4

18、Forgings, Extrusions, and Flash Welded RingsSolution heat treated.3.3.4.1 Flash welded rings shall not be supplied unless specified or permitted on purchasers part drawing. When supplied, rings shall be manufactured in accordance with AMS7490.3.3.5 Stock for Forging or Flash Welded RingsAs ordered b

19、y the forging or flash welded ring manufacturer.3.4 Heat TreatmentBars, forgings, and flash welded rings shall be solution heat treated by heating to a temperature within the range 1,850 to 1,950 F (1,010 to 1,066 C), holding at the selected temperature within 25 F (14 C) for a time commensurate wit

20、h cross-sectional thickness, and cooling at a rate equivalent to air cooling. Pyrometry shall be in accordance with AMS2750.3.5 PropertiesThe product shall conform to the following requirements:3.5.1 Bars, Wire, Forgings, and Flash Welded Rings3.5.1.1 As Solution Heat Treated3.5.1.1.1 Hardness of Ba

21、rs, Forgings, and Flash Welded RingsShall be not higher than 287 HB, or equivalent (see 8.2).3.5.1.1.2 Tensile Strength of WireShall be not higher than 135 ksi (931 MPa), determined in accordance with ASTM E8/E8M.SAE INTERNATIONAL AMS5854C Page 4 of 73.5.1.1.3 Average Grain SizeASTM No. 3 or finer,

22、determined in accordance with ASTM E112, for product with a least cross-section dimension under 2-1/2 inches (63.5 mm).3.5.1.2 After Precipitation Heat TreatmentProduct, 4 inches (102 mm) and under in nominal diameter or least distance between parallel sides, shall meet the requirements of 3.5.1.2.1

23、 and 3.5.1.2.2 after being precipitation heat treated by heating to a temperature within the range 1,325 to 1,375 F (718 to 746 C), holding at the selected temperature within 15 F (8 C) for not less than 8 hours, cooling at a rate of 100 F 15 F (55 C 8 C) degrees per hour to 1,150 F 15 F (621 C 8 C)

24、, holding at 1,150 F 15 F (621 C 8 C) for not less than 8 hours, and cooling at a rate equivalent to air cooling. Instead of the 100 F (55 C) degrees per hour cooling rate to 1,150 F 15 F (621 C 8 C), product may be furnace cooled at any rate provided the time at 1,150 F 15 F (621 C 8 C) is adjusted

25、 to give a total precipitation heat treatment time of not less than 18 hours.3.5.1.2.1 Tensile PropertiesShall be as shown in Table 2, determined in accordance with ASTM E8/E8M on specimens taken from product under 4 inches (102 mm) in least cross-sectional dimension.Table 2 - Minimum tensile proper

26、tiesProperty ValueTensile StrengthYield Strength at 0.2% OffsetElongation in 4DReduction in Area150 ksi (1,034 MPa)115 ksi ( 793 MPa)25%40%3.5.1.2.2 HardnessShall be not lower than 30 HRC, or equivalent (see 8.2), but the product shall not be rejected on basis of hardness if the tensile properties o

27、f 3.5.1.2.1 are acceptable, determined on specimens taken from the same sample as that with nonconforming hardness or from another sample with similar nonconforming hardness.3.5.1.2.3 Mechanical property requirements for product outside of the range covered by 1.1 shall be agreed upon between purcha

28、ser and supplier (see 8.5).3.5.2 Forging StockWhen a sample of stock is forged to a test coupon and heat treated as in 3.4 and 3.5.1.2, specimens taken from the heat treated coupon shall conform to the requirements of 3.5.1.2.1. If specimens taken from the stock after heat treatment as in 3.4 and 3.

29、5.1.2 conform to the requirements of 3.5.1.2.1, the test shall be accepted as equivalent to tests of a forged coupon.3.5.3 Extrusions and Stock for Flash Welded RingsShall be as agreed upon by purchaser and producer.3.6 QualityThe product, as received by purchaser, shall be uniform in quality and co

30、ndition, sound, and free from foreign materials and from imperfections detrimental to usage of the product. 3.6.1 Grain flow of die forgings, except in areas which contain flash-line end grain, shall follow the general contour of the forging showing no evidence of reentrant grain flow.3.7 Tolerances

31、Shall conform to all applicable requirements of AMS2261 for bars and wire.SAE INTERNATIONAL AMS5854C Page 5 of 74. QUALITY ASSURANCE PROVISIONS4.1 Responsibility for InspectionThe producer of the product shall supply all samples for producers tests and shall be responsible for performance of all req

32、uired tests. Purchaser reserves the right to sample and to perform any confirmatory testing deemed necessary to ensure that the product conforms to specified requirements.4.2 Classification of Tests4.2.1 Acceptance TestsThe following requirements are acceptance tests and shall be performed on each h

33、eat or lot as applicable:4.2.1.1 Composition (3.1) of each heat.4.2.1.2 Hardness (3.5.1.1.1), wire tensile properties (3.5.1.1.2), and average grain size (3.5.1.1.3) of each lot solution heat treated.4.2.1.3 Tensile properties (3.5.1.2.1), and hardness (3.5.1.2.2) of each lot after precipitation hea

34、t treatment.4.2.1.4 Tolerances (3.7) of each lot.4.2.2 Periodic TestsTests of forging stock (3.5.2) to demonstrate ability to develop required properties and grain flow of die forgings (3.6.1) are periodic tests and shall be performed at a frequency selected by the producer unless frequency of testi

35、ng is specified by purchaser.4.3 Sampling and Testing4.3.1 Bars, Wire, Flash Welded Rings, Extrusions, and Stock for Forgings and Flash Welded RingsIn accordance with AMS2371.4.3.2 ForgingsIn accordance with AMS2374.4.4 Reports4.4.1 Bars, Wire, Flash Welded Rings and ForgingsThe producer of the prod

36、uct shall furnish with each shipment a report showing the producers name and the country where the metal was melted (e.g., final melt in the case of metal processed by multiple melting operations) and showing the results of tests for composition of each heat (3.1), and for hardness (3.5.1.1.1), wire

37、 tensile properties (3.5.1.1.2), and average grain size (3.5.1.1.3) as solution heat treated, and for tensile properties (3.5.1.2.1) and hardness (3.5.1.2.2), if applicable regarding product size, after precipitation heat treatment of each lot, and stating that the product conforms to the other tech

38、nical requirements. This report shall include the purchase order number, heat and lot numbers, AMS5854C, product form, size, and quantity. If forgings are supplied, the size and source of stock used to make the forgings shall also be included.4.4.2 Report the nominal metallurgically worked cross sec

39、tional size and the cut size, if different (see 3.2.1.1).4.4.3 When the product size is outside the range covered by 1.1, the report shall contain a statement to that effect.SAE INTERNATIONAL AMS5854C Page 6 of 74.4.4 Extrusions and Stock for Forgings and Flash Welded RingsThe producer of extrusions

40、 and stock for forgings and flash welded rings shall furnish with each shipment a report showing the producers name and the country where the metal was melted (e.g., final melt in the case of metal processed by multiple melting operations) and showing the results of tests for composition of each hea

41、t (3.1), and for tensile properties and hardness of forging stock after forging and heat treatment of coupon (3.5.2), if applicable, This report shall include the purchase order number, heat and lot numbers, AMS5854C, product form, size, and quantity.4.5 Resampling and Retesting4.5.1 Bars, Wire, Fla

42、sh Welded Rings, Extrusions, and Stock for Forgings and Flash Welded RingsIn accordance with AMS2371.4.5.2 ForgingsIn accordance with AMS2374.5. PREPARATION FOR DELIVERY5.1 SizesExcept when exact lengths or multiples of exact lengths are ordered, straight bars will be acceptable in mill lengths of 6

43、 to 24feet (1.8 to 7.3 m) but not more than 25% of any shipment shall be supplied in lengths of 6 to 9 feet (1.8 to 2.7 m), except that for bars weighing over 25 pounds per foot (37 kg/m), short lengths down to 2 feet (61 mm) may be supplied.5.2 Identification5.2.1 Bars, Wire, and ExtrusionsIn accor

44、dance with AMS2806.5.2.2 ForgingsIn accordance with AMS2808.5.2.3 Flash Welding Rings and Stock for Forging or Flash Welded RingsAs agreed upon by purchaser and producer.5.3 PackagingThe product shall be prepared for shipment in accordance with commercial practice and in compliance with applicable r

45、ules and regulations pertaining to the handling, packaging, and transportation of the product to ensure carrier acceptance and safe delivery.6. ACKNOWLEDGMENTA producer shall mention this specification number and its revision letter in all quotations and when acknowledging purchase orders.7. REJECTI

46、ONSProduct not conforming to this specification, or to modifications authorized by purchaser, will be subject to rejection.SAE INTERNATIONAL AMS5854C Page 7 of 78. NOTES8.1 Revision IndicatorA change bar (l) located in the left margin is for the convenience of the user in locating areas where techni

47、cal revisions, not editorial changes, have been made to the previous issue of this document. An (R) symbol to the left of the document title indicates a complete revision of the document, including technical revisions. Change bars and (R) are not used in original publications, nor in documents that

48、contain editorial changes only.8.2 Hardness conversion tables for metals are presented in ASTM E140.8.3 Terms used in AMS are clarified in ARP1917.8.4 Dimensions and properties in inch/pound units and the Fahrenheit temperatures are primary; dimensions and properties in SI units and the Celsius temp

49、eratures are shown as the approximate equivalents of the primary units and are presented only for information.8.5 Purchase documents should specify not less than the following:AMS5854CProduct form and size or part number of product desiredProperty and acceptance requirements from the cognizant engineering organization applicable to sizes outside the range listed in 1.1