SAE AS 6449C-2017 Solid Film Lubricant.pdf

1、_ SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising there

2、from, is the sole responsibility of the user.” SAE reviews each technical report at least every five years at which time it may be revised, reaffirmed, stabilized, or cancelled. SAE invites your written comments and suggestions. Copyright 2017 SAE International All rights reserved. No part of this p

3、ublication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-497

4、0 (outside USA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your input. To provide feedback on this Technical Report, please visit http:/standards.sae.org/AS6449C AEROSPACE STANDARD AS6449 REV. C Issued 2011-07 Revised 2017-07 Superseding AS6449B Sol

5、id Film Lubricant RATIONALE The document has been revised to change shelf life requirement into 12 months from date of manufacture, odor test temperature has been clarified, thickness requirements were made consistent, and aluminum alloy temper/specification have been clarified. 1. SCOPE This docume

6、nt establishes the requirements for a dry film lubricant AS6449 lubricant for use on breathing oxygen system and potable water system components, for a temperature range of -90 to +300 F. This document also establishes the Non-Destructive Test (NDT) procedures and criteria for coated production part

7、s. This document requires qualified products and product applicators. 1.1 Application For applications where temperatures may range from -90 to 300 F (-68 to 149 C), except Type IV may be used up to 400 F (204 C). 1.2 Type This specification establishes the following types: 1.2.1 For Use in Oxygen a

8、nd Potable Water Systems AS6449 Type I: A lubricant for use on oxygen and potable water system fittings AS6449 Type II: A lubricant for use on potable water fittings 1.2.2 Unleaded lubricant for hydraulic and other systems AS6449 Type III: Unleaded Lubricant in compliance with AS5272 Type I as liste

9、d in PRI-QPL-AS5272 AS6449 Type IV: Unleaded Lubricant in compliance with AS5272 Type II as listed in PRI-QPL-AS5272 NOTE: Types III and IV are lead free materials that are qualified to AS5272 as Types I and II respectively and are listed with other lead bearing materials in PRI-QPL-AS5272. These qu

10、alified lead free materials have been selected for inclusion in this document as AS6449 Types III and IV. SAE INTERNATIONAL AS6449C Page 2 of 11 1.3 Safety Hazardous Materials While the materials, methods, applications, and processes described or referenced in this specification may involve use of h

11、azardous materials, this specification does not address the hazards which may be involved is such use. The product manufacturer shall prepare Materials Safety Data Sheets (MSDS) in accordance with ANSI Z400 and abide by MSDS requirements to ensure familiarity with the safe and proper handling of haz

12、ardous materials used and take necessary precautionary measures to ensure the health and safety of all personnel involved. 2. REFERENCES 2.1 Applicable Documents The following publications form a part of this document to the extent specified herein. The latest issue of SAE publications shall apply.

13、The applicable issue of other publications shall be the issue in effect on the date of the purchase order. In the event of conflict between the text of this document and references cited herein, the text of this document takes precedence. Nothing in this document, however, supersedes applicable laws

14、 and regulations unless a specific exemption has been obtained. 2.1.1 SAE Publications Available from SAE International, 400 Commonwealth Drive, Warrendale, PA 15096-0001, Tel: 877-606-7323 (inside USA and Canada) or +1 724-776-4970 (outside USA), www.sae.org. AMS4083 Aluminum Alloy Tubing, Hydrauli

15、c, Seamless, Drawn, Round 1.0Mg - 0.60Si - 0.28Cu - 0.20Cr (6061-T6) Solution and Precipitation Heat Treated AMS5513 Steel, Corrosion-Resistant, Sheet, Strip, and Plate 19Cr - 9.2Ni (SAE 30304) Solution Heat Treated AMS5901 Steel, Corrosion-Resistant, Sheet, Strip, and Plate 18Cr - 8Ni (SAE 30301) S

16、olution Heat Treated AMS-M-7866 Molybdenum Disulfide, Technical, Lubrication Grade AMS-QQ-A-250/12 Aluminum Alloy 7075, Plate and Sheet AMS-QQ-A-250/4 Aluminum Alloy 2024, Plate and Sheet AMS-STD-595 Colors Used in Government Procurement AS1241 Fire Resistant Phosphate Ester Hydraulic Fluid for Airc

17、raft AS2094 Test Methods for Tube-Fitting Assemblies AS5234 Nut, Coupling Flareless AS5272 Lubricant, Solid Film, Heat Cured, Corrosion Inhibiting, Procurement Specification AS5528 Lubricant Application, Solid Film, Heat Cured, Corrosion Inhibiting AS5529 Sleeve, Flareless Tube Fitting, Internally S

18、waged AS6450 Lubricant Application, Solid Film, Heat Cured, Potable Water, Hydraulic, and Other Fluid Systems AS9100 Quality Management Systems - Requirements for Aviation, Space and Defense Organizations SAE INTERNATIONAL AS6449C Page 3 of 11 2.1.2 AlA Publications Available from Aerospace Industri

19、es Association, 1000 Wilson Boulevard, Suite 1700, Arlington, VA 22209-3928, Tel: 703-358-1000, www.aia-aerospace.org. NAS850 General Packaging Standard NAS854 Hazardous Material Packaging and Safety Data Sheet Preparation 2.2 ANSI Accredited Publications Copies of these documents are available onli

20、ne at http:/webstore.ansi.org/. ANSI Z400 Material Safety Data Sheets 2.3 ASTM Publications Available from ASTM International, 100 Barr Harbor Drive, P.O. Box C700, West Conshohocken, PA 19428-2959, Tel: 610-832-9585, www.astm.org. ASTM B117 Standard Practice for Operating Salt Spray (Fog) Test Appa

21、ratus ASTM A967 Standard Specification for Chemical Passivation Treatments for Stainless Steel Parts ASTM D1655 Standard Specification for Aviation Turbine Fuels ASTM D2247 Standard Practice for Testing Water Resistance of Coatings in 100% Relative Humidity ASTM D2510 Standard Test Method for Adhesi

22、on of Solid Film Lubricants ASTM D2512 Standard Test Method for Compatibility of Materials with Liquid Oxygen (Impact Sensitivity Threshold and Pass-Fail Techniques) ASTM D2625 Standard Test Method for Endurance (Wear) Life and Load-Carrying Capacity of Solid Film Lubricants (Falex Pin and Vee Metho

23、d) ASTM D4080 Standard Specification for Trichloroethylene, Technical and Vapor-Degreasing Grade 2.4 ISO Publications Available at http:/webstore.ansi.org/. ISO/IEC 17025 General Requirements for the Competence of Testing and Calibration Laboratories 2.5 PRI Publications Available from Performance R

24、eview Institute, 161 Thorn Hill Road, Warrendale, PA 15086-7527, Tel: 724-772-1616, www.pri-network.org. PD2101 Aerospace Quality Assurance, Product Standards, Qualification Procedure, - Fluid Distribution Systems PRI-QPL-AS5272 Qualified Products List (QPL) of Products Qualified Under SAE Aerospace

25、 Specification AS5272 - Lubricant, Solid Film, Heat Cured, Corrosion Inhibiting PRI-QPL-AS6449 Qualified Products List (QPL) of Products Qualified Under SAE Aerospace Specification AS6449 - Solid Film Lubricant for Fluid Fittings in Oxygen, Potable Water, Hydraulic, and Other Systems SAE INTERNATION

26、AL AS6449C Page 4 of 11 2.6 U.S. Government Publications Copies of these documents are available online at http:/quicksearch.dla.mil. MIL-A-8625 Anodic Coatings for Aluminum and Aluminum Alloys MIL-PRF-83282 Hydraulic Fluid, Fire Resistant, Synthetic Hydrocarbon Base MIL-PRF-27210 Oxygen, Aviators B

27、reathing, Liquid and Gas TT-N-95 Naphta, Aliphatic 2.7 Other Government Publications Not Available under ASSIST Available from United States Environmental Protection Agency (EPA), Web: www.epa.gov, Email: nscepEbps-, Phone: 1-800-490-9198, Mail: U.S. EPA/NSCEP, P.O. Box 42419, Cincinnati, OH 45242-0

28、419. OSHA 1910.1200 Hazard Communication Standard Available from www.epa.gov. RE-ADD-030 Hazard Communication Program Available from https:/www.acquisition.gov/far/, Email: acquisitioncentralgsa.gov, Mail: GSA/VIR, Attn: Regulatory Secretariat, 1800F Street, NW, Washington, DC 20405. Title 29 CFR Co

29、de of Federal Regulations (CFP) 1910 3. REQUIREMENTS 3.1 Qualification The lubricants furnished under this specification shall be products which are listed or approved on the applicable qualified product list, Types I and II in PRI-QPL-AS6449 and Types III and IV as lead-free in PRI-QPL-AS5272. The

30、QPL requirement for AS6449 Types I and II may be in effect for purchase orders within 18 months following initial AS6449 release. Suppliers seeking listing on the initial QPL should contact PRI. Until the QPL is in effect, users of this standard are advised to control source approvals. No change in

31、product formulation, raw material, basic methods of manufacturing or plant site shall be made without notification and prior approval from the Performance Review Institute (PRI). Requalification or testing and revised supplier designation may be required. 3.1.1 Manufacturer Qualification A manufactu

32、rer producing a product in conformance to this procurement specification shall be accredited in accordance with AS9100. 3.1.2 Product Qualification All lubricants Type I and Type II shall conform to the requirements of this specification and shall be approved in accordance with the requirements of P

33、D2001, for listing in a PRI Qualified Products List (QPL) PRI-QPL-AS6449. 3.1.3 Qualification Testing All qualification testing shall be conducted by a laboratory which is accredited per ISO/IEC 17025 with a relevant scope. If qualification tests are performed at the manufacturers facility or at a t

34、est facility without ISO/IEC 17025 accreditation with a relevant scope, test shall be witnessed by a QPG member, designated QPG representative, PRI Auditor, or verified by OEM qualification test. SAE INTERNATIONAL AS6449C Page 5 of 11 3.2 Material Requirements 3.2.1 General Requirements The lubrican

35、t, applied in accordance with AS6450, shall meet the following requirements. The material shall meet all the requirements of this specification at any time within 12 months from the date of manufacture when material is stored from 40 to 100 F (4 to 38 C). The cured coating when applied to oxygen and

36、 potable water fittings shall not transfer to hands, packaging material or oxygen and potable water tubes under normal handling conditions. 3.2.2 Bonded Solid Film Requirements Type I and Type II lubricants applied in accordance with AS6450, shall meet the requirements in 3.2 and 3.3, except Type II

37、 lubricant is not required to meet the requirements of 3.3.1. Type III and Type IV lubricants applied in accordance with AS5528 shall meet the requirements of AS5272 Type I and Type II respectively. 3.2.3 Film Appearance and Thickness The cured dry lubricant film shall have a uniform appearance and

38、complete coverage. No voids or buildups in excess of the film thickness tolerances of AS6450 will be permitted on contact (bearing) surfaces. The average thickness, based on six readings minimum, of the cured film of all Types shall be between 0.0003 inch (0.008 mm) and 0.0005 inch (0.013 mm). Film

39、thickness shall be controlled on both external and internal threads by the process and by fit-check, i.e., when installed on appropriate thread gage the coated threads shall permit three quarter turn of free rotation, threads shall not exceed AS8879 MMC (Maximum Material Condition) during gage check

40、. 3.2.4 Composition The dry lubricant shall be composed of molybdenum disulfide, in accordance with AMS-M-7866, combined with suitable bonding agents to meet the requirements of this document. The requirements of AMS-M-7866 for molybdenum disulfide particle size shall not apply. The material manufac

41、ture shall select a grade/particle size of molybdenum disulfide that is suitable for meeting all performance requirements and material characteristics of this specification, and shall not change grade/particle size for production lots from that which was qualified. Manufacturing processes shall also

42、 be controlled to ensure the final particle size of molybdenum disulfide contained within material production lots remains consistent with that of the materials submitted for qualification. The product shall not contain lead, chrome, mercury, cadmium, antimony, or their compounds. The dry lubricant

43、shall not contain any compounds that have a residual high vapor pressure after the cure cycle or are leachable by common industrial solvents. 3.2.5 Toxic Products, Formulations, and Health Hazard Evaluation The dry film lubricant shall have no known adverse effect on the health of personnel when use

44、d for intended purpose. The dry film lubricant shall contain no components which produce harmful vapors during or after installation. Health hazard evaluation shall be performed for each new material qualified to this specification in accordance with RE-ADD-030 to establish its usage precautions. A

45、Material Safety Data Sheet shall be submitted in accordance with 1.3. 3.3 Performance Requirements 3.3.1 Liquid Oxygen (LOX) and Gaseous Oxygen Compatibility (Type I Oxygen Components only) The supplier shall submit written evidence that the cured lubricant does not react in liquid or gaseous oxygen

46、 when subjected to 98 J (72 feet-pound) impact test conducted in accordance with ASTM D2512. NOTE: Required for Type I only, not for Type II. 3.3.2 Low Temperature Stability The cured lubricant shall not flake, crack, or otherwise show loss of adhesion when tested in accordance with 4.6.2. SAE INTER

47、NATIONAL AS6449C Page 6 of 11 3.3.3 Fluid Resistance When tested according to 4.6.3, the immersed portion of the test panels shall show no evidence of softening, lifting, blistering, peeling, cracking, or loss of adhesion. After performing the tape adhesion test, there shall be no deposit or transfe

48、r of any coating material to the tape when viewed by the unaided eye. Exposing the substrate also indicates unsatisfactory adhesion. Test specimens shall be as shown in Table 1. 3.3.4 Corrosion Resistance When tested according to 4.6.4, the test specimens or anodized aluminum panels shall not show d

49、iscoloration, pitting, formation of white deposits, or other evidence of corrosion. Test specimens shall be as shown in Table 1. 3.3.5 Odor The cured lubricant shall contain no materials which have an objectionable odor or which will produce an objectionable odor when in contact with oxygen at 160 F 10 F for a minimum of 24 hours. A decision that the odor is objectionable to one or more of the observers, when test