SAE CMH-17-5A-2017 Composite Materials Handbook Volume 5 (Ceramic Matrix Composites).pdf

1、 NOT MEASUREMENT SENSITIVE CMH-17-5A Volume 5 of 6 1 JUNE 2017 Superseding MIL-HDBK-17-5 17 JUNE 2002 COMPOSITE MATERIALS HANDBOOK VOLUME 5. CERAMIC MATRIX COMPOSITES Copyright 2017 - Composite Materials Handbook 17 (CMH-17). All rights reserved. Un-authorized duplication or distribution may violate

2、 the Copyright Laws of the United States and of other jurisdictions Published by SAE International on behalf of CMH-17, a division of Wichita State University CMH-17-5A Volume 5, Foreword / Table of Contents ii FOREWORD The Composite Materials Handbook, CMH-17, provides information and guidance nece

3、ssary to design and fabricate structural components from composite materials. Its primary purposes are a) the standardization of engineering data development methodologies related to testing, data reduction, and data reporting of property data for current and emerging composite materials, b) guidanc

4、e on material and process specifi-cations and procedures for utilization of the material data presented in the handbook, and c) methodologies for the design, analysis, certification, manufacture, and field support of composite structures. In support of these objectives, the handbook includes composi

5、te materials properties that meet specific data require-ments. The Handbook therefore constitutes an overview of the field of composites technology and engi-neering, an area that is advancing and changing rapidly. As a result, the document will be continually revised as sections are added or modifie

6、d to reflect advances in the state-of-the-art. CMH-17 Mission The Composite Materials Handbook organization creates, publishes and maintains proven, reliable engi-neering information and standards, subjected to thorough technical review, to support the development and use of composite materials and

7、structures. CMH-17 Vision The Composite Materials Handbook will be the authoritative worldwide focal point for technical information on composite materials and structures. Goals and Objectives to Support CMH-17 Mission x To periodically meet with experts from the field to discuss critical technical

8、issues for composite structural applications, with an emphasis on increasing overall product efficiency, quality and safety. x To provide comprehensive, practical engineering guidance that has proven reliable for the design, fabrication, characterization, test and maintenance of composite materials

9、and structures. x To provide reliable data, linked to control of processes and raw materials, thereby being a compre-hensive source of material property basis values and design information that can be shared within the industry. x To provide a resource for composite material and structure education

10、with examples, applications and references to supporting engineering work. x To establish guidelines for use of information in the Handbook, identifying the limitations of the data and methods. x To provide guidance on references to proven standards and engineering practices. x To provide for period

11、ic updates to maintain the all-inclusive nature of the information. x To provide information in formats best-suited for user needs. x To serve the needs of the international composites community through meetings and dialogue be-tween member industries, which use teamwork and the diverse member engin

12、eering skills to pro-vide information for the handbook. CMH-17-5A Volume 5, Foreword / Table of Contents iii Notes 1. Every effort has been made to reflect the latest information on polymer (organic), metal, and ce-ramic composites. The handbook is continually reviewed and revised to ensure it is co

13、mplete and current. 2. CMH-17 provides guidelines and material properties for polymer (organic), metal, and ceramic ma-trix composite materials. The first three volumes of this handbook currently focus on, but are not limited to, polymeric composites intended for aircraft and aerospace vehicles. Met

14、al matrix com-posites (MMC), ceramic matrix composites (CMC), and sandwich composites are covered in Vol-umes 4, 5, and 6, respectively. 3. The information contained in this handbook was obtained from materials producers, industry com-panies and experts, reports on Government sponsored research, the

15、 open literature, and by con-tract with research laboratories and those who participate in the CMH-17 coordination activity. The information in this handbook has undergone vigorous technical review and was subject to mem-bership vote. 4. Beneficial comments (recommendations, additions, deletions) an

16、d any pertinent data which may be of use in improving this document should be addressed to: CMH-17 Secretariat, Wichita State University, 1845 Fairmount, Wichita, KS 67260, by letter or email, infocmh17.org. ACKNOWLEDGEMENT Volunteer committee members from government, industry, and academia develop,

17、 coordinate and review all the information provided in this handbook. The time and effort of the volunteers and the support of their respective departments, companies, and universities make it possible to insure the handbook reflects com-pleteness, accuracy, and state-of-the-art composite technology

18、 Support necessary for the development and maintenance of the Composite Materials Handbook (CMH-17) are provided by the handbook Secretariat, Wichita State University. The primary source of funding for the current Secretariat contract is the Federal Aviation Administration. CMH-17-5A Volume 5, Fore

19、word / Table of Contents iv CONTENTS PART A. INTRODUCTION AND GUIDELINES PART B. DESIGN AND SUPPORTABILITY PART C. TESTING PART D. DATA REQUIREMENTS AND DATA SETS APPENDIX A. DERIVATION OF THE RESIDUAL STRENGTH REDUCTION EXPRESSIONS FOR LCF AND RUPTURE LOADINGS Page PART A. INTRODUCTION AND GUIDELIN

20、ES . 1 1 CMH-17 GUIDELINES AND PROCEDURES 1 1.1 INTRODUCTION TO THE HANDBOOK 1 1.2 OVERVIEW OF HANDBOOK CONTENT 1 1.3 INTRODUCTION TO VOLUME 5 2 1.3.1 Objectives of Ceramic Matrix Composite (CMC) Working Groups . 3 1.3.1.1 Objectives and tasks for Data Review Working Group 3 1.3.1.2 Vision, goals an

21、d objectives for Materials and Processes Working Group . 4 1.3.1.3 Vision, goals and objectives for Design and Analysis Working Group . 4 1.3.1.4 Vision, goals and objectives for Testing Working Group 5 1.4 PURPOSE 5 1.5 SCOPE . 6 1.5.1 Part A: Introduction and Guidelines 7 1.5.2 Part B: Design and

22、Supportability 7 1.5.3 Part C: Testing 7 1.5.4 Part D: Data Requirements and Data Sets 7 1.6 USE OF THE DOCUMENT AND LIMITATIONS 8 1.6.1 Source of information 8 1.6.2 Use of data and guidelines in applications 8 1.6.3 Strength properties and allowables terminology . 9 1.6.4 Use of References . 9 1.6

23、5 Use of tradenames and product names 9 1.6.6 Toxicity, health hazards, and safety . 9 1.6.7 Ozone depleting chemicals . 9 1.7 APPROVAL PROCEDURES 9 1.8 SYMBOLS, ABBREVIATIONS, AND SYSTEMS OF UNITS . 10 1.8.1 Symbols and abbreviations . 10 1.8.1.1 Constituent properties 15 1.8.1.2 Laminae and lamin

24、ates 16 1.8.1.3 Subscripts 17 1.8.1.4 Superscripts . 18 1.8.1.5 Acronyms . 18 1.8.2 System of units 23 1.9 DEFINITIONS 24 2 CHAPTER 2 INTRODUCTION, HISTORY AND OVERVIEW 47 2.1 BACKGROUND . 47 2.2 CMC STRUCTURAL FUNDAMENTALS 48 2.3 HANDBOOK OBJECTIVES . 50 CMH-17-5A Volume 5, Foreword / Table of Cont

25、ents v 3 PROCESSING, CHARACTERIZATION, AND MANUFACTURING 56 3.1 CMC SYSTEMS, PROCESSING, PROPERTIES, AND APPLICATIONS . 56 3.1.1 The Application of SiC/SiC and Ox/Ox CMCs in Aircraft Turbine Engine Hot Section and Exhaust Components56 3.1.2 CMC Systems, Processing Methods, and Properties . 58 3.1.3

26、SiC/SiC CMCs . 59 3.1.3.1 Chemical Vapor Infiltration (CVI) SiC/SiC CMCs . 59 3.1.3.1.1 CVI fabrication technique . 59 3.1.3.1.2 Typical properties for CVI SiC/SiC CMCs 61 3.1.3.2 Polymer Infiltration such data are needed by material suppliers, design engineering personnel, manufacturing or-ganizati

27、ons, and structure end-users alike. In addition, reliable, proven design and analysis methods are essential to the efficient development and application of composite structures. This handbook is intended to provide these through standardization of: 1. Methods used to develop, analyze, and publish pr

28、operty data for composite materials. 2. Statistically-based, material property datasets for composite materials. 3. General procedures for designing, analyzing, testing, and supporting composite structures that uti-lize the property data published in this handbook. In many cases, this standardizatio

29、n is intended to address the requirements of regulatory agencies, while providing efficient engineering practices for developing structures that meet the needs of customer organizations. Composites is an evolving and growing technical field, and the Handbook Coordinating Committee is continuously wo

30、rking to incorporate new information and new material properties data as it becomes avail-able and is proven acceptable. While the source and context for much of this information has come from experience with aerospace applications, all industries utilizing composite materials and structures, whethe

31、r commercial or military, will find the handbook useful. This latest revision includes information related to broader applications from non-aerospace industries, and incorporation of non-aerospace data will increase as development of the handbook continues. Composite Materials Handbook-17 (CMH-17) h

32、as been developed and is maintained as a joint effort of the Department of Defense and the Federal Aviation Administration, with considerable participation and input from industry, academia, and other government agencies. Although initial structural applications of composites tended to be military,

33、recent development trends have seen increasing use of these materials in commercial applications. In part because of these trends, the formal administration of the handbook passed from the Department of Defense to the Federal Aviation Administration in 2006 and the handbook title was changed from Mi

34、litary Handbook-17 to Composite Materials Handbook-17. The organization of the Coordinating Committee and the purpose of the handbook did not change. This handbook documents engineering methodologies for the development of standardized, statisti-cally-based material property data for ceramic matrix

35、composite materials. Also provided are data summar-ies for a number of relevant composite material systems for which available data meet specific CMH-17 requirements for publication. Additionally, supporting engineering and manufacturing technologies and common practices related to composite materia

36、ls are summarized. 1.2 OVERVIEW OF HANDBOOK CONTENT Composite Materials Handbook-17 is composed of a series of six volumes. Volume 1: Polymer Matrix Composites - Guidelines for Characterization of Structural Materials Volume 1 contains guidelines for determining the properties of polymer matrix comp

37、osite material sys-tems and their constituents, as well as the properties of generic structural elements, including test planning, test matrices, sampling, conditioning, test procedure selection, data reporting, data reduction, statistical analysis, and other related topics. Special attention is giv

38、en to the statistical treatment and analysis of data. CMH-17-5A Volume 5, Part A Introduction and Guidelines 2 Volume 1 contains guidelines for general development of material characterization data as well as specific requirements for publication of material data in CMH-17. Volume 2: Polymer Matrix

39、Composites - Material Properties Volume 2 contains statistically-based data for polymer matrix composites that meets specific CMH-17 population sampling and data documentation requirements, covering material systems of general interest. As of the publication of Revision G, data published in Volume 2

40、 are under the jurisdiction of the Data Review Working Group and are approved by the overall CMH-17 Coordinating Committee. New material systems will be included and additional material data for existing systems will be added as data becomes available and are approved. Selected historical data from

41、previous versions of the handbook that do not meet current data sampling, test methodology, or documentation requirements, but that still are of potential interest to industry are also included in this Volume. Volume 3: Polymer Matrix Composites - Materials Usage, Design, and Analysis Volume 3 provi

42、des methodologies and lessons learned for the design, analysis, manufacture, and field support of fiber-reinforced, polymeric-matrix composite structures. It also provides guidance on material and process specifications and procedures for utilization of the data presented in Volume 2. The infor-mati

43、on provided is consistent with the guidance provided in Volume 1, and is an extensive compilation of the current knowledge and experiences of the engineers and scientists who are active in composites from industry, government, and academia. Volume 4: Metal Matrix Composites Volume 4 publishes proper

44、ties on metal matrix composite material systems for which data meeting the specific requirements of the handbook are available. In addition, it provides selected guidance on other technical topics related to this class of composites, including material selection, material specification, pro-cessing,

45、 characterization testing, data reduction, design, analysis, quality control, and repair of typical metal matrix composite materials. Volume 5: Ceramic Matrix Composites Volume 5 publishes properties on ceramic matrix composite material systems for which data meeting the specific requirements of the

46、 handbook are available. In addition, it provides selected guidance on other technical topics related to this class of composites, including material selection, material specification, pro-cessing, characterization testing, data reduction, design, analysis, quality control, and repair of typical ce-

47、ramic matrix composite materials. Volume 6: Structural Sandwich Composites Volume 6 is an update to the cancelled Military Handbook 23, which was prepared for use in the design of structural sandwich polymer composites, primarily for flight vehicles. The information presented includes test methods,

48、material properties, design and analysis techniques, fabrication methods, quality control and inspection procedures, and repair techniques for sandwich structures in both military and commercial vehi-cles. 1.3 INTRODUCTION TO VOLUME 5 It is generally understood that standardized, statistically-based

49、 material property data are essential to an efficient engineering development process; such data are needed by material suppliers, engineering users, and system end-users alike. Since the inherent properties of materials are independent of specific applications, data development methodologies and material property data are applicable to a wide variety of industries. They also form much of the technical basis for establishment of statistically-based design values acceptable to procuring or