SAE J 1907-1988 Peel Adhesion Test for Glass to Elastomeric Material for Automotive Glass Encapsulation Recommended Practice.pdf

1、SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirelyvoluntary, and its applicability and suitability for any particular use, including any patent infringement arising therefro

2、m, is the sole responsibility of the user.”SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions.QUESTIONS REGARDING THIS DOCUMENT: (724) 772-8512 FAX: (724) 776-0243TO PLACE A DOCUMENT

3、 ORDER; (724) 776-4970 FAX: (724) 776-0790SAE WEB ADDRESS http:/www.sae.orgCopyright 1989 Society of Automotive Engineers, Inc.All rights reserved. Printed in U.S.A.SURFACEVEHICLE400 Commonwealth Drive, Warrendale, PA 15096-0001RECOMMENDEDPRACTICESubmitted for recognition as an American National Sta

4、ndardJ1907ISSUEDOCT88Issued 1989-10PEEL ADHESION TEST FOR GLASS TO ELASTOMERIC MATERIAL FOR AUTOMOTIVE GLASS ENCAPSULATIONForewordThis Document has not changed other than to put it into the new SAE Technical Standards BoardFormat.1. ScopeThis recommended practice defines a procedure for the construc

5、tion and testing of a 180 deg peelspecimen for the purpose of determining the bondability of glass to elastomeric material in automotive modularglass. This test method suggests that elastomeric material of less than 172 mpa modulus be used as theencapsulating material. The present practice of encaps

6、ulating automotive glass is described as molded-in-place elastomeric material onto the outer edge of the glass using thermoplastic or thermosetting material thatquickly sets in the mold. The glass is removed from the mold with the cured elastomeric material bonded tothe perimeter of the glass. This

7、encapsulated glass module can now be bonded with a sealant adhesive intothe body opening of a vehicle.2. References2.1 Applicable PublicationThe following publication forms a part of the specification to the extent specifiedherein.2.1.1 ASTM PUBLICATIONAvailable from ASTM, 100 Barr Harbor Drive, Wes

8、t Conshohocken, PA 19428-2959.ASTM D 10023. Test Substrates3.1 SubstratesThe glass specimens that will be used for testing, or any surface conditioner such as ceramiccoating, should be of the type recommended by automotive engineers.The thermoplastic or thermosetting material should have a modulus o

9、f less than 172 MPa and be of the typeused in automotive glass encapsulation.3.2 DimensionsThe recommended glass sample size should be at least 203 mm (8 in) long and at least3.2 mm (0.125 in) thick and at least 25.4 mm (1 in) wide.3.3 Glass Surface PreparationGlass surface preparation, such as clea

10、ning and priming application, should bein accordance with suppliers or automotive engineers recommendation.SAE J1907 Issued OCT88-2-4. Test Specimen4.1 Glass EncapsulationThe samples for testing should be from glass encapsulated using injection moldingequipment and procedures recommended by automoti

11、ve engineers.4.2 Preparation for SpecimenFor ease of test specimen preparation in 3.5, it is recommended that the glassnot be primed where the elastomeric material is to be cut out.4.3 Encapsulation Dimensions and TolerancesThe elastomeric material should be molded onto the glasssuch that the width

12、dimensions shall be at 6.4 mm (0.25 in) with a tolerance of 0.25 mm (0.01 in). Thethickness dimensions shall be at 3.2 mm (0.125 in) with a tolerance of 0.128 mm (0.005 in). The overalllength of the encapsulation shall be at least 203 mm (8 in) and should not have any flaws or nicks that couldresult

13、 in erroneous test results.FIGURE 1ENCAPSULATED TEST SPECIMEN4.4 Test Specimen Conditioning and AgingThe molded glass should be conditioned according to suppliers orautomotive engineers recommendation.4.5 Test Specimen PreparationAt least 102 mm (4 in) should be cut away from the glass as illustrate

14、d in Figure2 below in order to be used for clamping to the tensile tester.FIGURE 2PREPARATION OF TEST SPECIMEN5. Testing5.1 ApparatusTest apparatus should be a tensile tester described in ASTM D 1002.5.2 Sample ClampingThe top jaw should be clamped to the glass portion and the bottom jaw should becl

15、amped to elastomeric material as described in Figure 3. If necessary, an extender can be attached to theelastomeric material to facilitate clamping.SAE J1907 Issued OCT88-3-FIGURE 3TESTING SPECIMEN ON TENSILE TESTER5.3 Test ConditionsPull specimens at 23 C and 50% relative humidity or as otherwise s

16、pecified.5.4 Test RateTest specimens shall be tested at pull rate of 50.8 mm (2 in) per minute.5.5 Test ObservationsRecord bond values and type of failure every 12.7 mm (0.5 in) for at least 63.5 mm(2.5in).6. Report6.1 Complete identification of glass and elatomeric material used for encapsulation.6

17、.2 Complete identification of material and procedures used for priming and cleaning glass.6.3 Encapsulation conditions used for molding.6.4 Environmental conditions prior to testing.6.5 Peel strength as pounds per linear inch and Newtons per linear centimeter.6.6 Bond values every 12.7 mm (0.5 in) f

18、or ast least 63.5 mm (2.5 in) with an average of these values.SAE J1907 Issued OCT88-4-6.7 Type of failure every 12.7 mm (0.5 in) for at least 63.5 mm (2.5 in) with an average of these values.Abbreviations for type of failure are:CFCohesive failure of elastomeric material.AFAdhesive failure of elast

19、omeric material off primed glass.PFPrimer failure off glass, if it is detectable.PREPARED BY THE SAE STATIONARY GLASS BONDING SUBCOMMITTEE OF THE SAE ADHESIVES AND BODY SEALERS COMMITTEESAE J1907 Issued OCT88RationaleNot applicable.Relationship of SAE Standard to ISO StandardNot applicable.Applicati

20、onThis recommended practice defines a procedure for the construction and testing of a 180 degpeel specimen for the purpose of determining the bondability of glass to elastomeric material inautomotive modular glass. This test method suggests that elastomeric material of less than 172 MPamodulus be us

21、ed as the encapsulating material. The present practice of encapsulating automotive glassis described as molded-in-place elastomeric material onto the outer edge of the glass usingthermoplastic or thermosetting material that quickly sets in the mold. The glass is removed from themold with the cured e

22、lastomeric material bonded to the perimeter of the glass. This encapsulated glassmodule can now be bonded with a sealant adhesive into the body opening of a vehicle.Reference SectionASTM D 1002Developed by the SAE Stationary Glass Bonding SubcommitteeSponsored by the SAE Adhesives And Body Sealers Committee