IEC 60556-2006 Gyromagnetic materials intended for application at microwave frequencies - Measuring methods for properties《用于微波频率的旋磁材料.性能的测量方法》.pdf

1、 IEC 60556 Edition 2.0 2006-04 INTERNATIONAL STANDARD NORME INTERNATIONALE Gyromagnetic materials intended for application at microwave frequencies Measuring methods for properties Matriaux gyromagntiques destins des applications hyperfrquences Mthodes de mesure des proprits IEC 60556:2006 THIS PUBL

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16、ntactez-nous: Email: csciec.ch Tl.: +41 22 919 02 11 Fax: +41 22 919 03 00 IEC 60556 Edition 2.0 2006-04 INTERNATIONAL STANDARD NORME INTERNATIONALE Gyromagnetic materials intended for application at microwave frequencies Measuring methods for properties Matriaux gyromagntiques destins des applicati

17、ons hyperfrquences Mthodes de mesure des proprits INTERNATIONAL ELECTROTECHNICAL COMMISSION COMMISSION ELECTROTECHNIQUE INTERNATIONALE XA ICS 29.100.10 PRICE CODE CODE PRIX ISBN 978-2-88912-595-1 Registered trademark of the International Electrotechnical Commission Marque dpose de la Commission Elec

18、trotechnique Internationale 2 60556 IEC:2006 CONTENTS FOREWORD . 5 1 Scope . 7 2 Normative references . 7 3 Terms and definitions . 7 4 Saturation magnetization M s7 4.1 General . 7 4.2 Object . 8 4.3 Theory . 8 4.4 Test sample 9 4.5 Measuring apparatus for the vibrating coil method (VCM) 9 4.6 Meas

19、uring apparatus for the vibrating sample method (VSM) 12 4.7 Calibration . 15 4.8 Measuring procedure . 16 4.9 Calculation 17 4.10 Accuracy . 17 4.11 Data presentation 18 5 Magnetization (at specified field strength) M H. 18 5.1 General . 18 5.2 Object . 18 5.3 Theory . 18 5.4 Test specimen . 20 5.5

20、 Measuring apparatus . 21 5.6 Calibration . 23 5.7 Measuring procedure . 24 5.8 Calculation 24 5.9 Accuracy . 24 5.10 Data presentation 24 6 Gyromagnetic resonance linewidth H and effective Land factor g eff(general) . 25 6.1 General . 25 6.2 Object . 25 6.3 Theory . 25 6.4 Test specimens and caviti

21、es 26 6.5 Measuring apparatus . 29 6.6 Measuring procedure . 29 6.7 Calculation 31 6.8 Accuracy . 31 6.9 Data presentation 31 7 Gyromagnetic resonance linewidth H 10and effective Land factor g 10(at 10 GHz) . 31 7.1 General . 31 7.2 Object . 31 7.3 Theory . 31 7.4 Test specimen and cavity 32 7.5 Mea

22、suring apparatus . 33 7.6 Measuring procedure . 33 7.7 Calculation 34 7.8 Accuracy . 34 60556 IEC:2006 3 7.9 Data presentation 35 8 Spin-wave resonance linewidth H k35 8.1 General . 35 8.2 Object . 35 8.3 Theory . 35 8.4 Test specimen and cavity 38 8.5 Measuring apparatus . 39 8.6 Calibration . 39 8

23、.7 Measuring procedure . 39 8.8 Calculation 40 8.9 Accuracy . 40 8.10 Data presentation 40 9 Effective linewidth H eff40 9.1 General . 40 9.2 Object . 40 9.3 Theory . 41 9.4 Test specimen and cavity 43 9.5 Measuring apparatus . 43 9.6 Calibration . 44 9.7 Apparatus adjustment 44 9.8 Measuring proced

24、ure . 45 9.9 Calculation 46 9.10 Accuracy . 46 9.11 Data presentation 46 10 Complex permittivity r. 47 10.1 General . 47 10.2 Object . 47 10.3 Theory . 47 10.4 Test specimen and cavity 50 10.5 Measuring apparatus . 50 10.6 Measurement procedure 51 10.7 Calculation 51 10.8 Accuracy . 52 10.9 Data pre

25、sentation 52 11 Apparent density app. 52 11.1 General . 52 11.2 Apparent density (by mensuration) 52 11.3 Apparent density (by water densitometry) 54 Bibliography 56 Figure 1 Vibrating coil method Sample and coils arrangement 9 Figure 2 Magnetic field configuration . 10 Figure 3 Measuring apparatus

26、(VCM) . 12 Figure 4 Vibrating sample method Sample and coil arrangement 13 Figure 5 Measuring apparatus (VSM) . 14 Figure 6 Hysteresis curves for a magnetic material: B(H) curve, M(H) curve 19 Figure 7 Test sample with compensation unit . 20 4 60556 IEC:2006 Figure 8 Test specimen 21 Figure 9 Measur

27、ing circuit for determining magnetization (at specified field strength) M H . 22 Figure 10 Miller integrator 23 Figure 11 Cavity for measurement of gyromagnetic resonance linewidth and effective Land factor . 27 Figure 12 Stripline resonator for measurement of gyromagnetic resonance linewidth and ef

28、fective Land factor at low frequency 28 Figure 13 Schematic diagram of the equipment required for measurement of gyromagnetic resonance linewidth and effective Land factor . 30 Figure 14 Schematic diagram of the equipment required for measurement of gyromagnetic resonance linewidth and effective Lan

29、d factor at 10 GHz 34 Figure 15 Subsidiary absorption and saturation of the normal resonance . 36 Figure 16 Pulse deterioration at onset of subsidiary resonance 36 Figure 17 Measured critical r.f. field strength as a function of pulse duration t d37 Figure 18 Typical TE 104cavity for the measurement

30、 of spin-wave resonance linewidth at about 9,3 GHz . 38 Figure 19 Block diagram of spin-wave resonance linewidth test equipment 39 Figure 20 Sectional view of the cavity with specimen . 42 Figure 21 Dimensions of a cavity designed for resonance at a frequency of 9,1 GHz . 42 Figure 22 Schematic diag

31、ram of equipment for measuring effective linewidth H eff44 Figure 23 Determination of Q 0. 46 Figure 24 Ideal resonant cavity with specimen, used for theoretical calculation (sectional view) . 48 Figure 25 Dimensions of the resonant cavity with specimen . 50 Figure 26 Schematic diagram of equipment

32、required for the measurement of complex dielectric constant . 51 60556 IEC:2006 5 INTERNATIONAL ELECTROTECHNICAL COMMISSION _ GYROMAGNETIC MATERIALS INTENDED FOR APPLICATION AT MICROWAVE FREQUENCIES MEASURING METHODS FOR PROPERTIES FOREWORD 1) The International Electrotechnical Commission (IEC) is a

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43、bject of patent rights. IEC shall not be held responsible for identifying any or all such patent rights. International Standard IEC 60556 has been prepared by IEC technical committee 51: Magnetic components and ferrite materials. This second edition cancels and replaces the first edition, published

44、in 1982, its amendment 1 (1997) and amendment 2 (2004). This edition constitutes a technical revision. This second edition is a consolidation of the first edition and its amendments 1 and 2. It includes editorial improvements as well as improvements to the figures. This standard is to be read in con

45、junction with IEC 60392. This bilingual version (2011-07) replaces the English version. 6 60556 IEC:2006 The text of this standard is based on the following documents: FDIS Report on voting 51/850/FDIS 51/859/RVD Full information on the voting for the approval of this standard can be found in the re

46、port on voting indicated in the above table. The French version of this standard has not been voted upon. This publication has been drafted in accordance with the ISO/IEC Directives, Part 2. The committee has decided that the contents of this publication will remain unchanged until the stability dat

47、e indicated on the IEC web site under “http:/webstore.iec.ch“ in the data related to the specific publication. At this date, the publication will be reconfirmed, withdrawn, replaced by a revised edition, or amended. 60556 IEC:2006 7 GYROMAGNETIC MATERIALS INTENDED FOR APPLICATION AT MICROWAVE FREQUE

48、NCIES MEASURING METHODS FOR PROPERTIES 1 Scope This International Standard describes methods of measuring the properties used to specify polycrystalline microwave ferrites in accordance with IEC 60392 and for general use in ferrite technology. These measuring methods are intended for the investigati

49、on of materials, generally referred to as ferrites, for application at microwave frequencies. Single crystals and thin films generally fall outside the scope of this standard. NOTE 1 For the purposes of this standard, the words “ferrite” and “microwave” are used in a broad sense: by “ferrites” is meant not only magneto-dielectric chemical component