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IEC 61788-17-2013 Superconductivity - Part 17 Electronic characteristic measurements - Local critical current density and its distribution in large-area superco.pdf

1、 IEC 61788-17 Edition 1.0 2013-01 INTERNATIONAL STANDARD NORME INTERNATIONALE Superconductivity Part 17: Electronic characteristic measurements Local critical current density and its distribution in large-area superconducting films Supraconductivit Partie 17: Mesures de caractristiques lectroniques

2、Densit de courant critique local et sa distribution dans les films supraconducteurs de grande surface IEC61788-17:2013 colourinsideTHIS PUBLICATION IS COPYRIGHT PROTECTED Copyright 2013 IEC, Geneva, Switzerland All rights reserved. Unless otherwise specified, no part of this publication may be repro

3、duced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either IEC or IECs member National Committee in the country of the requester. If you have any questions about IEC copyright or have an enquiry about obtai

4、ning additional rights to this publication, please contact the address below or your local IEC member National Committee for further information. Droits de reproduction rservs. Sauf indication contraire, aucune partie de cette publication ne peut tre reproduite ni utilise sous quelque forme que ce s

5、oit et par aucun procd, lectronique ou mcanique, y compris la photocopie et les microfilms, sans laccord crit de la CEI ou du Comit national de la CEI du pays du demandeur. Si vous avez des questions sur le copyright de la CEI ou si vous dsirez obtenir des droits supplmentaires sur cette publication

6、 utilisez les coordonnes ci-aprs ou contactez le Comit national de la CEI de votre pays de rsidence. IEC Central Office Tel.: +41 22 919 02 11 3, rue de Varemb Fax: +41 22 919 03 00 CH-1211 Geneva 20 infoiec.ch Switzerland www.iec.ch About the IEC The International Electrotechnical Commission (IEC)

7、 is the leading global organization that prepares and publishes International Standards for all electrical, electronic and related technologies. About IEC publications The technical content of IEC publications is kept under constant review by the IEC. Please make sure that you have the latest editio

8、n, a corrigenda or an amendment might have been published. Useful links: IEC publications search - www.iec.ch/searchpub The advanced search enables you to find IEC publications by a variety of criteria (reference number, text, technical committee,). It also gives information on projects, replaced an

9、d withdrawn publications. IEC Just Published - webstore.iec.ch/justpublished Stay up to date on all new IEC publications. Just Published details all new publications released. Available on-line and also once a month by email. Electropedia - www.electropedia.org The worlds leading online dictionary o

10、f electronic and electrical terms containing more than 30 000 terms and definitions in English and French, with equivalent terms in additional languages. Also known as the International Electrotechnical Vocabulary (IEV) on-line. Customer Service Centre - webstore.iec.ch/csc If you wish to give us yo

11、ur feedback on this publication or need further assistance, please contact the Customer Service Centre: csciec.ch. A propos de la CEI La Commission Electrotechnique Internationale (CEI) est la premire organisation mondiale qui labore et publie des Normes internationales pour tout ce qui a trait llec

12、tricit, llectronique et aux technologies apparentes. A propos des publications CEI Le contenu technique des publications de la CEI est constamment revu. Veuillez vous assurer que vous possdez ldition la plus rcente, un corrigendum ou amendement peut avoir t publi. Liens utiles: Recherche de publicat

13、ions CEI - www.iec.ch/searchpub La recherche avance vous permet de trouver des publications CEI en utilisant diffrents critres (numro de rfrence, texte, comit dtudes,). Elle donne aussi des informations sur les projets et les publications remplaces ou retires. Just Published CEI - webstore.iec.ch/ju

14、stpublished Restez inform sur les nouvelles publications de la CEI. Just Published dtaille les nouvelles publications parues. Disponible en ligne et aussi une fois par mois par email. Electropedia - www.electropedia.org Le premier dictionnaire en ligne au monde de termes lectroniques et lectriques.

15、Il contient plus de 30 000 termes et dfinitions en anglais et en franais, ainsi que les termes quivalents dans les langues additionnelles. Egalement appel Vocabulaire Electrotechnique International (VEI) en ligne. Service Clients - webstore.iec.ch/csc Si vous dsirez nous donner des commentaires sur

16、cette publication ou si vous avez des questions contactez-nous: csciec.ch. IEC 61788-17 Edition 1.0 2013-01 INTERNATIONAL STANDARD NORME INTERNATIONALE Superconductivity Part 17: Electronic characteristic measurements Local critical current density and its distribution in large-area superconducting

17、films Supraconductivit Partie 17: Mesures de caractristiques lectroniques Densit de courant critique local et sa distribution dans les films supraconducteurs de grande surface INTERNATIONAL ELECTROTECHNICAL COMMISSION COMMISSION ELECTROTECHNIQUE INTERNATIONALE X ICS 17.220.20; 29.050 PRICE CODE CODE

18、 PRIX ISBN 978-2-83220-583-9 Registered trademark of the International Electrotechnical Commission Marque dpose de la Commission Electrotechnique Internationale Warning! Make sure that you obtained this publication from an authorized distributor. Attention! Veuillez vous assurer que vous avez obtenu

19、 cette publication via un distributeur agr. colourinside 2 61788-17 IEC:2013 CONTENTS FOREWORD . 4 INTRODUCTION . 6 1 Scope . 8 2 Normative reference . 8 3 Terms and definitions . 8 4 Requirements . 9 5 Apparatus . 9 5.1 Measurement equipment . 9 5.2 Components for inductive measurements 10 5.2.1 Co

20、ils 10 5.2.2 Spacer film 11 5.2.3 Mechanism for the set-up of the coil 11 5.2.4 Calibration wafer . 11 6 Measurement procedure . 12 6.1 General . 12 6.2 Determination of the experimental coil coefficient 12 6.2.1 Calculation of the theoretical coil coefficient k . 12 6.2.2 Transport measurements of

21、bridges in the calibration wafer 13 6.2.3 U3measurements of the calibration wafer . 13 6.2.4 Calculation of the E-J characteristics from frequency-dependent Ithdata . 13 6.2.5 Determination of the k from Jctand Jc0values for an appropriate E 14 6.3 Measurement of Jcin sample films 15 6.4 Measurement

22、 of Jcwith only one frequency . 15 6.5 Examples of the theoretical and experimental coil coefficients . 16 7 Uncertainty in the test method 17 7.1 Major sources of systematic effects that affect the U3measurement . 17 7.2 Effect of deviation from the prescribed value in the coil-to-film distance 18

23、7.3 Uncertainty of the experimental coil coefficient and the obtained Jc. 18 7.4 Effects of the film edge 19 7.5 Specimen protection 19 8 Test report 19 8.1 Identification of test specimen . 19 8.2 Report of Jcvalues 19 8.3 Report of test conditions 19 Annex A (informative) Additional information re

24、lating to Clauses 1 to 8 20 Annex B (informative) Optional measurement systems . 26 Annex C (informative) Uncertainty considerations 32 Annex D (informative) Evaluation of the uncertainty . 37 Bibliography 43 Figure 1 Diagram for an electric circuit used for inductive Jcmeasurement of HTS films 10 F

25、igure 2 Illustration showing techniques to press the sample coil to HTS films . 11 Figure 3 Example of a calibration wafer used to determine the coil coefficient . 12 61788-17 IEC:2013 3 Figure 4 Illustration for the sample coil and the magnetic field during measurement . 13 Figure 5 E-J characteris

26、tics measured by a transport method and the U3inductive method . 14 Figure 6 Example of the normalized third-harmonic voltages (U3/fI0) measured with various frequencies . 15 Figure 7 Illustration for coils 1 and 3 in Table 1 16 Figure 8 The coil-factor function F(r) = 2H0/I0calculated for the three

27、 coils 17 Figure 9 The coil-to-film distance Z1dependence of the theoretical coil coefficient k 18 Figure A.1 Illustration for the sample coil and the magnetic field during measurement . 22 Figure A.2 (a) U3and (b) U3/I0plotted against I0in a YBCO thin film measured in applied DC magnetic fields, an

28、d the scaling observed when normalized by Ith (insets) 23 Figure B.1 Schematic diagram for the variable-RL-cancel circuit 27 Figure B.2 Diagram for an electrical circuit used for the 2-coil method . 27 Figure B.3 Harmonic noises arising from the power source 28 Figure B.4 Noise reduction using a can

29、cel coil with a superconducting film 28 Figure B.5 Normalized harmonic noises (U3/fI0) arising from the power source . 29 Figure B.6 Normalized noise voltages after the reduction using a cancel coil with a superconducting film . 29 Figure B.7 Normalized noise voltages after the reduction using a can

30、cel coil without a superconducting film 30 Figure B.8 Normalized noise voltages with the 2-coil system shown in Figure B.2 . 30 Figure D.1 Effect of the coil position against a superconducting thin film on the measured Jcvalues 41 Table 1 Specifications and coil coefficients of typical sample coils

31、 16 Table C.1 Output signals from two nominally identical extensometers 33 Table C.2 Mean values of two output signals . 33 Table C.3 Experimental standard deviations of two output signals . 33 Table C.4 Standard uncertainties of two output signals 34 Table C.5 Coefficient of variations of two outp

32、ut signals 34 Table D.1 Uncertainty budget table for the experimental coil coefficient k . 37 Table D.2 Examples of repeated measurements of Jcand n-values . 40 4 61788-17 IEC:2013 INTERNATIONAL ELECTROTECHNICAL COMMISSION _ SUPERCONDUCTIVITY Part 17: Electronic characteristic measurements Local cri

33、tical current density and its distribution in large-area superconducting films FOREWORD 1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising all national electrotechnical committees (IEC National Committees). The object of IEC is to promot

34、e international co-operation on all questions concerning standardization in the electrical and electronic fields. To this end and in addition to other activities, IEC publishes International Standards, Technical Specifications, Technical Reports, Publicly Available Specifications (PAS) and Guides (h

35、ereafter referred to as “IEC Publication(s)”). Their preparation is entrusted to technical committees; any IEC National Committee interested in the subject dealt with may participate in this preparatory work. International, governmental and non-governmental organizations liaising with the IEC also p

36、articipate in this preparation. IEC collaborates closely with the International Organization for Standardization (ISO) in accordance with conditions determined by agreement between the two organizations. 2) The formal decisions or agreements of IEC on technical matters express, as nearly as possible

37、 an international consensus of opinion on the relevant subjects since each technical committee has representation from all interested IEC National Committees. 3) IEC Publications have the form of recommendations for international use and are accepted by IEC National Committees in that sense. While

38、all reasonable efforts are made to ensure that the technical content of IEC Publications is accurate, IEC cannot be held responsible for the way in which they are used or for any misinterpretation by any end user. 4) In order to promote international uniformity, IEC National Committees undertake to

39、apply IEC Publications transparently to the maximum extent possible in their national and regional publications. Any divergence between any IEC Publication and the corresponding national or regional publication shall be clearly indicated in the latter. 5) IEC itself does not provide any attestation

40、of conformity. Independent certification bodies provide conformity assessment services and, in some areas, access to IEC marks of conformity. IEC is not responsible for any services carried out by independent certification bodies. 6) All users should ensure that they have the latest edition of this

41、publication. 7) No liability shall attach to IEC or its directors, employees, servants or agents including individual experts and members of its technical committees and IEC National Committees for any personal injury, property damage or other damage of any nature whatsoever, whether direct or indir

42、ect, or for costs (including legal fees) and expenses arising out of the publication, use of, or reliance upon, this IEC Publication or any other IEC Publications. 8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is indispensable for the

43、 correct application of this publication. International Standard IEC 61788-17 has been prepared by IEC technical committee 90: Superconductivity. The text of this standard is based on the following documents: FDIS Report on voting 90/310/FDIS 90/319/RVD Full information on the voting for the approva

44、l of this standard can be found in the report on voting indicated in the above table. This publication has been drafted in accordance with the ISO/IEC Directives, Part 2. A list of all the parts of the IEC 61788 series, published under the general title Superconductivity, can be found on the IEC web

45、site. 61788-17 IEC:2013 5 The committee has decided that the contents of this publication will remain unchanged until the stability date indicated on the IEC web site under “http:/webstore.iec.ch“ in the data related to the specific publication. At this date, the publication will be reconfirmed, wit

46、hdrawn, replaced by a revised edition, or amended. IMPORTANT The colour inside logo on the cover page of this publication indicates that it contains colours which are considered to be useful for the correct understanding of its contents. Users should therefore print this document using a colour prin

47、ter. 6 61788-17 IEC:2013 INTRODUCTION Over twenty years after their discovery in 1986, high-temperature superconductors are now finding their way into products and technologies that will revolutionize information transmission, transportation, and energy. Among them, high-temperature superconducting

48、HTS) microwave filters, which exploit the extremely low surface resistance of superconductors, have already been commercialized. They have two major advantages over conventional non-superconducting filters, namely: low insertion loss (low noise characteristics) and high frequency selectivity (sharp

49、 cut) 11. These advantages enable a reduced number of base stations, improved speech quality, more efficient use of frequency bandwidths, and reduced unnecessary radio wave noise. Large-area superconducting thin films have been developed for use in microwave devices 2. They are also used for emerging superconducting power devices, such as, resistive-type superconducting fault-curr

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