EN ISO 1716-2018 Reaction to fire tests for products - Determination of the gross heat of combustion (calorific value).pdf

1、BSI Standards PublicationWB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06Reaction to fire tests for products - Determination of the gross heat of combustion (calorific value)BS EN ISO 1716:2018National forewordThis British Standard is the UK implementation of EN ISO 1716:2018. It is identica

2、l to ISO 1716:2018. It supersedes BS EN ISO 1716:2010, which is withdrawn.The UK participation in its preparation was entrusted to Technical Committee FSH/21/-/5, Reaction to fire tests - Heat release and smoke measurement.A list of organizations represented on this committee can be obtained on requ

3、est to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. The British Standards Institution 2018 Published by BSI Standards Limited 2018ISBN 978 0 580 93554 1ICS 91.100.01; 13.220.50Compliance with

4、 a British Standard cannot confer immunity from legal obligations.This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 July 2018.Amendments/corrigenda issued since publicationDate Text affectedBRITISH STANDARDBS EN ISO 1716:2018EUROPEAN STANDAR

5、DNORME EUROPENNEEUROPISCHE NORMEN ISO 1716July 2018ICS 13.220.50; 91.100.01 Supersedes EN ISO 1716:2010EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGCEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2018 CEN Ref. No. EN ISO 1716:2018

6、: EAll rights of exploitation in any form and by any means reserved worldwide for CEN national MembersReaction to fire tests for products - Determination of the gross heat of combustion (calorific value) (ISO 1716:2018)Essais de raction au feu de produits - Dtermination du pouvoir calorifique suprie

7、ur (valeur calorifique) (ISO 1716:2018)Prfungen zum Brandverhalten von Produkten - Bestimmung der Verbrennungswrme (des Brennwerts) (ISO 1716:2018)This European Standard was approved by CEN on 9 May 2018.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the co

8、nditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.This European Standard exis

9、ts in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions.CEN members are the national stan

10、dards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slov

11、akia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.English VersionEN ISO 1716:2018 (E)European forewordThis document (EN ISO 1716:2018) has been prepared by Technical Committee ISO/TC 92 “Fire safety “ in collaboration with Technical Committee CEN/TC 127 “Fire safety in buildings”

12、 the secretariat of which is held by BSI.This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2019, and conflicting national standards shall be withdrawn at the latest by January 2019.Attention

13、 is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights.This document supersedes EN ISO 1716:2010.This document has been prepared under a mandate given to CEN by the E

14、uropean Commission and the European Free Trade Association.According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

15、Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.Endorsement noticeThe

16、 text of ISO 1716:2018 has been approved by CEN as EN ISO 1716:2018 without any modification.iiBS EN ISO 1716:2018ISO 1716:2018Foreword iv1 Scope .12 Normative references 13 Terms and definitions .14 Principle 35 Test apparatus . 36 Reagents and materials .87 Test specimens87.1 General . 87.2 Sampli

17、ng . 97.2.1 General 97.2.2 Loose-fill material . 97.2.3 Liquid-applied products 97.2.4 Thin film products 97.3 Determination of surface density . 97.4 Grinding . 107.5 Type of specimen . 107.6 Conditioning . 107.7 Number of test specimens 107.8 Determination of mass 107.9 Crucible method 117.10 “Cig

18、arette” method . 118 Test procedure .128.1 General 128.2 Calibration procedure 128.2.1 Determination of the water equivalent .128.2.2 Conditions for recalibration 128.3 Standard test procedure 129 Expression of results .149.1 Corrections for manual apparatus 149.2 Corrections for isothermal calorime

19、ter (see Annex C) .149.3 Calculation of the gross heat of combustion of the specimen .159.4 Calculation of the gross heat of combustion of the product .169.4.1 General. 169.4.2 Homogeneous product 179.4.3 Non-homogeneous product . 1710 Test report 1811 Validity of test results .18Annex A (normative)

20、 Calculation of net heat of combustion .20Annex B (informative) Precision of test method .21Annex C (informative) Calculation by graph of the corrective term, c, necessarybecause of the cooling of the calorimeter .24Annex D (informative) Example of determination of the gross heat ofcombustion of a n

21、on-homogeneous product .25Bibliography .30 ISO 2018 All rights reserved iiiContents PageBS EN ISO 1716:2018ISO 1716:2018ForewordISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Sta

22、ndards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also

23、take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In

24、particular the different approval criteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).Attention is drawn to the possibility that some of the elements

25、of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the development of the document will be in the Introduction and/or on the ISO list of patent declarations received (se

26、e www.iso.org/patents).Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement.For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and expressions related to conformity assessment, as well as

27、 information about ISOs adherence to the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following URL: www.iso.org/iso/foreword.html.This document was prepared by Technical Committee ISO/TC 92, Fire safety, Subcommittee SC 1, Fire initiation and growth.Thi

28、s fourth edition cancels and replaces the third edition (ISO 1716:2010), which has been technically revised.iv ISO 2018 All rights reservedBS EN ISO 1716:2018Reaction to fire tests for products - Determination of the gross heat of combustion (calorific value)WARNING The attention of all persons conc

29、erned with managing and carrying out this test is drawn to the fact that fire testing may be hazardous and that there is a possibility that toxic and/or harmful gases may be evolved during the test. Operational hazards may also arise during the testing of specimens, such as the possibility of an exp

30、losion, and during the disposal of test residues.WARNING An assessment of all the potential hazards and risks to health should be made and safety precautions should be identified and provided. Written safety instructions should be issued. Appropriate training should be given to relevant personnel. L

31、aboratory personnel should ensure that they follow written instructions at all times.1 ScopeThis document specifies a method for the determination of the gross heat of combustion (QPCS) of products at constant volume in a bomb calorimeter.This method is intended to be applied to solid products.NOTE

32、Liquids can be tested with similar equipment and using conditions described in ASTM D2401, as described in IEC 610392using ISO 19283test equipment.Annex A specifies the calculation of the net heat of combustion, QPCI, when required.Information on the precision of the test method is given in Annex B.

33、2 Normative referencesThe following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including

34、any amendments) applies.ISO 554, Standard atmospheres for conditioning and/or testing SpecificationsEN 13238, Reaction to fire tests for building products Conditioning procedures and general rules for selection of substrates3 Terms and definitionsFor the purposes of this document, the following term

35、s and definitions apply.ISO and IEC maintain terminological databases for use in standardization at the following addresses: ISO Online browsing platform: available at https:/www.iso.org/obp IEC Electropedia: available at https:/www.electropedia.org/3.1productmaterial, element or component about whi

36、ch information is requiredINTERNATIONAL STANDARD ISO 1716:2018 ISO 2018 All rights reserved 1BS EN ISO 1716:2018ISO 1716:20183.2materialsingle basic substance or uniformly dispersed mixture of substancesEXAMPLE Stone, timber, concrete, mineral wool with a uniformly dispersed binder and polymers.3.3h

37、omogeneous productproduct (3.1) consisting of a single material (3.2) having uniform density and composition throughout the product (3.1)3.4non-homogeneous productproduct (3.1) that does not satisfy the requirements of a homogeneous product (3.3) and which is composed of more than one component, sub

38、stantial or non-substantialNote 1 to entry: If a non-homogeneous product cannot be easily separated into its component parts, the individual components shall be provided separately by the sponsor.3.5non-substantial componentmaterial (3.2) that does not constitute a significant part of a non-homogene

39、ous product (3.4) and that has a layer with a mass/unit area below 1,0 kg/m2and a thickness below 1,0 mmNote 1 to entry: If the non-substantial layers do not comply with the above requirements, together they shall be considered to be substantial.Note 2 to entry: Two or more non-substantial layers th

40、at are adjacent to each other (i.e. with no substantial component(s) in between the layers) are regarded as one non-substantial component when they collectively comply with the requirements for a layer being a non-substantial component.3.6substantial componentmaterial (3.2) that constitutes a signif

41、icant part of a non-homogeneous product (3.4) and that has a layer with a mass/unit area more than or equal to 1,0 kg/m2or a thickness more than or equal to 1,0 mmNote 1 to entry: Two or more non-substantial layers that are adjacent to each other (i.e. with no substantial component(s) in between the

42、 layers) are regarded as one substantial component when they collectively comply with the requirements for a layer being a substantial component.3.7internal non-substantial componentnon-substantial component (3.5) that is covered on both sides by at least one substantial component (3.6)3.8external n

43、on-substantial componentnon-substantial component (3.5) that is not covered on one side by a substantial component (3.6)3.9heat of combustionDEPRECATED: calorific value Qthermal energy produced by combustion of unit mass of a given substanceNote 1 to entry: The heat of combustion is expressed in meg

44、ajoules per kilogram.SOURCE: ISO 13943:2008, 4.174, modified The Note 1 to entry was changed.2 ISO 2018 All rights reservedBS EN ISO 1716:2018ISO 1716:20183.10gross heat of combustionQPCSheat of combustion (3.9) of a substance when the combustion is complete and any produced water is entirely conden

45、sed under specified conditionsNote 1 to entry: The gross heat of combustion is expressed in megajoules per kilogram.Note 2 to entry: The acronym PCS is derived from the French term “pouvoir calorifique suprieur”.3.11net heat of combustionQPCIheat of combustion (3.9) of a substance when the combustio

46、n is complete and any produced water is in the vapour state under specified conditionsNote 1 to entry: The net heat of combustion may be calculated from the gross heat of combustion.Note 2 to entry: The net heat of combustion is expressed in megajoules per kilogram.Note 3 to entry: The acronym PCI i

47、s derived from the French term “pouvoir calorifique infrieur”.3.12latent heat of vaporization of waterqheat which is required to change water from a liquid to a gasNote 1 to entry: The latent heat of vaporization is expressed in megajoules per kilogram.3.13surface densitymass per unit areaNote 1 to

48、entry: The surface density is expressed in kilograms per square metre.4 PrincipleIn this test, a test specimen of specified mass is burned under standardized conditions, at constant volume, in an atmosphere of oxygen, in a bomb calorimeter calibrated by combustion of certified benzoic acid. The heat

49、 of combustion determined under these conditions is calculated on the basis of the observed temperature rise, taking account of heat loss and the latent heat of vaporization of water.This is a test method for determining an absolute value of the heat of combustion for a product and it does not take into account any inherent variability of the product.5 Test apparatusThe test apparatus (bomb calorimeter) shall be as illustrated in Figure 1, and as detailed in 5.1 to 5.4. Additional equipment shall be in accordance with 5.5 to 5.10.Equipment