DB12 T 795-2018 生活饮用水中5种人工合成甜味剂的测定 液相色谱-串联质谱法.pdf

1、ICS DB12 DBDetermination of five kinds of artificial sweeteners in drinking water liquid chromatography-tandem mass spectrometry method 20010001 CXA A B B 100n g /mLT i m e0 .2 5 0 .5 0 0 .7 5 1 .0 0 1 .2 5 1 .5 0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .5 0 4

2、.7 5%010020160501s td16 M RM o f 8 Ch a n n e l s ES - T IC1 .6 7 e 51 . 3 31 . 9 61 . 5 71 . 4 51 . 8 83 . 8 1100n g /mLT i m e0 .2 0 0 .4 0 0 .6 0 0 .8 0 1 .0 0 1 .2 0 1 .4 0 1 .6 0 1 .8 0 2 .0 0 2 .2 0 2 .4 0 2 .6 0 2 .8 0 3 .0 0 3 .2 0 3 .4 0 3 .6 0 3 .8 0 4 .0 0 4 .2 0 4 .4 0 4 .6 0 4 .8 0%0100

3、0 .2 0 0 .4 0 0 .6 0 0 .8 0 1 .0 0 1 .2 0 1 .4 0 1 .6 0 1 .8 0 2 .0 0 2 .2 0 2 .4 0 2 .6 0 2 .8 0 3 .0 0 3 .2 0 3 .4 0 3 .6 0 3 .8 0 4 .0 0 4 .2 0 4 .4 0 4 .6 0 4 .8 0%01000 .2 0 0 .4 0 0 .6 0 0 .8 0 1 .0 0 1 .2 0 1 .4 0 1 .6 0 1 .8 0 2 .0 0 2 .2 0 2 .4 0 2 .6 0 2 .8 0 3 .0 0 3 .2 0 3 .4 0 3 .6 0 3

4、.8 0 4 .0 0 4 .2 0 4 .4 0 4 .6 0 4 .8 0%01000 .2 0 0 .4 0 0 .6 0 0 .8 0 1 .0 0 1 .2 0 1 .4 0 1 .6 0 1 .8 0 2 .0 0 2 .2 0 2 .4 0 2 .6 0 2 .8 0 3 .0 0 3 .2 0 3 .4 0 3 .6 0 3 .8 0 4 .0 0 4 .2 0 4 .4 0 4 .6 0 4 .8 0%01000 .2 0 0 .4 0 0 .6 0 0 .8 0 1 .0 0 1 .2 0 1 .4 0 1 .6 0 1 .8 0 2 .0 0 2 .2 0 2 .4 0

5、2 .6 0 2 .8 0 3 .0 0 3 .2 0 3 .4 0 3 .6 0 3 .8 0 4 .0 0 4 .2 0 4 .4 0 4 .6 0 4 .8 0%01000 .2 0 0 .4 0 0 .6 0 0 .8 0 1 .0 0 1 .2 0 1 .4 0 1 .6 0 1 .8 0 2 .0 0 2 .2 0 2 .4 0 2 .6 0 2 .8 0 3 .0 0 3 .2 0 3 .4 0 3 .6 0 3 .8 0 4 .0 0 4 .2 0 4 .4 0 4 .6 0 4 .8 0%01000 .2 0 0 .4 0 0 .6 0 0 .8 0 1 .0 0 1 .2

6、0 1 .4 0 1 .6 0 1 .8 0 2 .0 0 2 .2 0 2 .4 0 2 .6 0 2 .8 0 3 .0 0 3 .2 0 3 .4 0 3 .6 0 3 .8 0 4 .0 0 4 .2 0 4 .4 0 4 .6 0 4 .8 0%01000 .2 0 0 .4 0 0 .6 0 0 .8 0 1 .0 0 1 .2 0 1 .4 0 1 .6 0 1 .8 0 2 .0 0 2 .2 0 2 .4 0 2 .6 0 2 .8 0 3 .0 0 3 .2 0 3 .4 0 3 .6 0 3 .8 0 4 .0 0 4 .2 0 4 .4 0 4 .6 0 4 .8 0%

7、010020160502T 3s td1- 6 M RM o f 8 Ch a n n e l s ES- 3 9 5 3 9 5 (s a n l v z h e ta n g )1 .1 8 e 51 .9 53 .7 73 .7 63 .5 020160502T 3s td1- 6 M RM o f 8 Ch a n n e l s ES- 2 9 2 .9 2 6 0 .9 (a s i b a ti a n )5 .7 0 e 41 .8 620160502T 3s td1- 6 M RM o f 8 Ch a n n e l s ES- 2 9 2 .9 2 0 0 .1 (a s

8、 i b a ti a n )2 .6 8 e 41 .8 520160502T 3s td1- 6 M RM o f 8 Ch a n n e l s ES- 1 8 1 .9 1 0 5 .9 ( ta n g j i n n a )2 .7 7 e 41 .4 520160502T 3s td1- 6 M RM o f 8 Ch a n n e l s ES- 1 8 1 .9 4 2 ( ta n g j i n n a )2 .4 4 e 41 .4 520160502T 3s td1- 6 M RM o f 8 Ch a n n e l s ES- 1 7 7 .9 7 9 .9

9、(t i a n m i s u )1 .2 3 e 51 .5 720160502T 3s td1- 6 M RM o f 8 Ch a n n e l s ES- 1 6 1 .8 8 2 (a n s a i m i )1 .4 9 e 51 .3 21 .1 71 .3 320160502T 3s td1- 6 M RM o f 8 Ch a n n e l s ES- 1 6 1 .8 7 7 .9 (a n s a i m i )1 .7 2 e 41 .3 31 .1 85n g /mLT i m e0 .2 5 0 .5 0 0 .7 5 1 .0 0 1 .2 5 1 .5

10、0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .5 0 4 .7 5%010020160501s td12 M RM o f 8 Ch a n n e l s ES - T IC9 .2 6 e 31 . 3 31 . 2 00 . 8 50 . 2 90 . 0 9 0 . 4 70 . 8 01 . 1 63 . 8 23 . 8 13 . 7 81 . 9 61 . 8 91 . 5 91 . 4 6 1 . 6 21 . 6 93 . 6 03 . 5 13 . 4 43

11、 . 2 83 . 1 73 . 0 12 . 8 11 . 9 9 2 . 7 92 . 6 92 . 5 12 . 9 53 . 8 63 . 8 73 . 9 03 . 9 84 . 0 5 4 . 0 94 . 2 04 . 2 24 . 2 34 . 7 74 . 2 7 4 . 4 24 . 5 44 . 8 85n g /mLT i m e0 .2 5 0 .5 0 0 .7 5 1 .0 0 1 .2 5 1 .5 0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .

12、5 0 4 .7 5%01000 .2 5 0 .5 0 0 .7 5 1 .0 0 1 .2 5 1 .5 0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .5 0 4 .7 5%01000 .2 5 0 .5 0 0 .7 5 1 .0 0 1 .2 5 1 .5 0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .5 0 4 .7 5%01000 .2 5 0 .5

13、 0 0 .7 5 1 .0 0 1 .2 5 1 .5 0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .5 0 4 .7 5%01000 .2 5 0 .5 0 0 .7 5 1 .0 0 1 .2 5 1 .5 0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .5 0 4 .7 5%01000 .2 5 0 .5 0 0 .7 5 1 .0 0 1 .2 5 1

14、.5 0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .5 0 4 .7 5%01000 .2 5 0 .5 0 0 .7 5 1 .0 0 1 .2 5 1 .5 0 1 .7 5 2 .0 0 2 .2 5 2 .5 0 2 .7 5 3 .0 0 3 .2 5 3 .5 0 3 .7 5 4 .0 0 4 .2 5 4 .5 0 4 .7 5%010020160501s td12 M RM o f 8 Ch a n n e l s ES - 3 9 5 3 9 5 (s a

15、n l v z h e ta n g )8 .2 0 e 33 . 8 23 . 7 81 . 9 61 . 8 91 . 5 11 . 4 91 . 3 30 . 8 50 . 2 90 . 0 9 0 . 4 70 . 6 2 1 . 2 03 . 6 03 . 4 43 . 2 83 . 0 12 . 8 11 . 9 92 . 7 32 . 5 13 . 8 64 . 0 5 4 . 2 04 . 7 74 . 4 24 . 5 420160501s td12 M RM o f 8 Ch a n n e l s ES - 2 9 2 .9 2 6 0 .9 (a s i b a ti

16、a n )2 .3 4 e 31 . 9 01 . 9 23 . 4 720160501s td12 M RM o f 8 Ch a n n e l s ES - 2 9 2 .9 2 0 0 .1 (a s i b a ti a n )1 .1 9 e 31 . 8 91 . 9 13 . 9 82 . 0 820160501s td12 M RM o f 8 Ch a n n e l s ES - 1 8 1 .9 1 0 5 .9 ( ta n g j i n n a )9171 . 4 61 . 2 40 . 3 01 . 4 82 . 8 42 . 3 61 . 7 2 4 . 2

17、33 . 8 83 . 0 1 4 . 8 620160501s td12 M RM o f 8 Ch a n n e l s ES - 1 8 1 .9 4 2 ( ta n g j i n n a )6311 . 4 71 . 4 41 . 0 90 . 7 50 . 2 10 . 1 50 . 4 7 0 . 9 23 . 8 23 . 7 12 . 1 52 . 0 11 . 8 71 . 7 52 . 8 72 . 5 52 . 4 9 2 . 6 0 3 . 6 02 . 9 93 . 1 8 4 . 5 14 . 0 1 4 . 9 84 . 7 620160501s td12 M RM o f 8 Ch a n n e l s ES - 1 7 7 .9 7 9 .9 (t i a n m i s u )3 .7 1 e 31 . 5 91 . 6 220160501s td12 M RM o f 8 Ch a n n e l s ES - 1 6 1 .8 8 2 (a n s a i m i )7 .6 3 e 31 . 3 31 . 2 6_