ASTM D7868-13(2017) Standard Practice for Determining the Dry Fall (Fog) Properties of Protective Coatings.pdf

1、Designation: D7868 13 (Reapproved 2017)Standard Practice forDetermining the Dry Fall (Fog) Properties of ProtectiveCoatings1This standard is issued under the fixed designation D7868; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision,

2、the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice covers a procedure for qualitatively evalu-ating the dry fall properties of coatings. The es

3、tablishment ofthe test environment and the evaluation procedures are de-scribed.1.2 This practice uses panels containing an automotivefinish since these types of surfaces are often the primaryconcern relating to overspray damage. Panels coated with othersystems may be used as collection surfaces whe

4、n they aredeemed to be more representative.1.3 The values stated in inch-pound units are to be regardedas standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.4 This standard does not purport to addr

5、ess all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety, health, and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.5 This international standard was devel

6、oped in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade (TBT) Committee.2. Referenced Docu

7、ments2.1 ASTM Standards:2D610 Practice for Evaluating Degree of Rusting on PaintedSteel SurfacesD5402 Practice for Assessing the Solvent Resistance ofOrganic Coatings Using Solvent Rubs3. Terminology3.1 Definitions:3.1.1 dry/fall/fog coating, nan interior or exterior coatingspecially formulated so t

8、hat the fine particles of overspray dryto a dust or powder during a free fall of a certain distance atspecific temperature and humidity ranges, and will not adhereto surfaces on which the overspray is subsequently deposited.4. Summary of Practice4.1 A structural frame is erected and enclosed. Spray

9、targetsare placed inside the enclosure. Four steel panels coated withan automotive basecoat/clear coat system are placed on theenclosure floor to collect the dry fall. (Panels coated with othersystems or uncoated panels, or both, can be used when they aredeemed to be more representative.) A duplicat

10、e panel set ismaintained at the prevailing air temperature, while the otherduplicate panel set is heated in oven and placed inside theenclosure immediately prior to atomizing the coating. Thecoating is atomized against the targets at each of two distancesand the panels are removed for evaluation. Tw

11、o of the coatedsteel panels remain at laboratory ambient conditions, while the“pre-heated” panels are returned to a laboratory oven. Theheated and ambient coated panels are cleaned and evaluatedafter 24-h for dry fall attachment.5. Significance and Use5.1 Attachment of overspray particles to vehicle

12、s and othersurfaces not intended to be coated can result in propertydamage and insurance claims. Dry fall coatings are formulatedsuch that overspray particles dry as they move through the air,and before they land on horizontal surfaces. These particles canthen be brushed off, vacuumed or washed from

13、 the surfaceswith no damage. This practice can be used to evaluate the dryfall properties of coatings prior to large scale use. The practicecan also be used to evaluate whether the coating(s) possess thesame dry fall properties when the fallout collects on surfaceswith an elevated temperature.6. Rea

14、gents6.1 Commercially available Car Washing Concentrate.6.2 Mineral Spirits.1This practice is under the jurisdiction of ASTM Committee D01 on Paint andRelated Coatings, Materials, and Applications and is the direct responsibility ofSubcommittee D01.46 on Industrial Protective Coatings.Current editio

15、n approved Dec. 1, 2017. Published December 2017. Originallyapproved in 2013. Last previous edition approved in 2013 as D7868 13. DOI:10.1520D7868-13R17.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMSt

16、andards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in accordance with internationally recognized princip

17、les on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.17. Procedure7.1 Construct a frame (enclosure) using steel conduit andcoupling

18、s or other materials of construction. The interior of theenclosure measures approximately 3 ft wide by 4 ft deep and is19 ft high in order to permit a dry fall test distance of 18 ft.3Enclose the frame with plastic sheeting or tarpaulins andsecure, making sure there is access at the base of the encl

19、osureto add and remove the collection surfaces (coated panels). Abase constructed of plywood and protected with paper orplastic sheeting (that can be pushed in/pulled out to load/unload the panels) may be used. This requires the frame to beheightened approximately 2 in. from the floor surface usingw

20、ooden blocks or other methods (see Fig. 1).7.2 Fabricate and suspend (vertically) a spray target con-structed of18 in. by 3 by 3 ft wood or other rigid material ontotwo hanging rods inside the enclosure. Mount troughs alongthe bottom edge of the target (optional) or position thecollection surfaces t

21、o prevent dripping coating on the dry fallcollection surfaces at the base of the enclosure. The spraytargets are positioned at the top of the enclosure to allow a dryfall distance of 18 ft, and are positioned 48 ft and 24 ft from thespray gun tip (see 7.7 and 7.9). The spray targets shall bereplaced

22、 for each test to prevent build-up of wet coating on thetargets and potential dripping onto the dry fall collectionsurfaces at the base of the enclosure (See Fig. 2).7.3 Mix and reduce (thin) the coating material according tothe manufacturers instructions, by the maximum amountpermitted. Record the

23、material temperature. Atomize the coat-ing by airless spray (unless another spray method is mutuallyselected), using the pump pressure, hose diameter and tip sizerecommended by the manufacturer. If the coating manufacturerrecommends a range of pump pressures and tip sizes, use thelowest pump pressur

24、e and the largest tip size (of the rangesrecommended) to create a worse case scenario. Record theactual pressure and tip size used, and the type, batch numberand amount of reducer used.7.4 Record the date and time of day. Measure and record theair temperature, relative humidity and dew point tempera

25、tureinside the enclosure. Testing should be performed when the airtemperature is between 60 and 80F (16 and 27C) and therelative humidity is between 40 and 85 %. The enclosureshould not be mechanically ventilated.7.5 Place duplicate 4 by 6 in. steel panels coated with anautomotive system (basecoat/c

26、lear coat) in the center of theenclosure base. The color of the coating on the panels shall beblack unless another panel color is mutually selected orrequired for contrast to the color of the dry fall product beingevaluated. Record the coating system on the panels as well asthe color of the finish c

27、oat on the panels. The surfacetemperature of the panels shall be measured and recorded.Place a second set of duplicate steel panels (that have beenpre-heated in an oven maintained at 50C until a surfacetemperature of 122F (50C) is attained).4Record the oventemperature. This set of pre-heated panels

28、(designed to repli-cate a hot surface) shall be placed inside the enclosure within10 s of coating atomization to minimize heat loss. Identify theback sides of the panels with the replicate number; (forexample, 1, 2) and the condition (for example, normal and hot).Position the normal temperature and

29、pre-heated (hot) panelsrandomly on the base of the enclosure.7.6 Position the spray target (described in 7.2) at the top ofthe enclosure against the back wall. Orient the target vertically(the middle of the target should be approximately 18 ft fromthe dry fall collection platform at the base of the

30、enclosure).Record the start time, then atomize the coating against thespray target (48 in. from the spray tip) for 45 6 3s.5Monitorthe atomization time using a stopwatch.After the elapsed spraytime, immediately remove the panels from the base of theenclosure.Allow two of the steel panels to remain a

31、t laboratory3Other dry fall distances can be selected as agreed upon between purchaser andseller. The enclosure height may be adjusted to accommodate other dry falldistances.4The use of thicker steel panels (for example, 0.25 in.) will retain heat longerthan thinner steel panels.5Shorter atomization

32、 time (for example, 15 s.) may be invoked when shorter dryfall distances (for example, 10 ft) are employed.FIG. 1 Dry Fall EvaluationEnclosure with Plastic Sheeting(NoteBase is heightened using 1.5 in. wooden blocks.)D7868 13 (2017)2ambient conditions (nominal 77F (25C) and 50 % relativehumidity) fo

33、r approximately 24 h. Immediately place thepre-heated panels back into laboratory oven (maintained at122F (50C) for 24 h. After the 24 h period, proceed to 7.8.7.7 Repeat steps 7.2 7.6 with a new target positionedmidway in the enclosure so that it is 24 in. from the spray tip.To reduce any influence

34、 of residual solvent vapors inside theenclosure, allow a minimum of 30 min between spray trialswith the same product (for example, between 48 and 24 in.spray distances) and a minimum of 1 h between products.67.8 Allow the panels removed from the oven to equilibrateto room temperature, then evaluate

35、the surface of the ambientand oven panels by attempting to remove the dry fall by drybrushing (using a clean, soft bristle dust pan brush). Rate andrecord the degree of attachment after dry brushing (DB) usingFig. 3 (4DB to 1DB).7.9 If dry brushing will not remove the overspray, usemoderate pressure

36、7with a cellulose sponge and standard carwash concentrate, diluted per the manufacturers instructionsin warm (70 to 90F (21 to 32C) water to scrub the surface.Rate and record the degree of attachment after scrubbing thesurface with the car wash (CW) solution using Fig. 3 (4CW to1CW).7.10 If moderate

37、 scrubbing with a cellulose sponge andstandard car wash concentrate in warm water will not removethe overspray, use moderate pressure with cotton cloths andmineral spirits to scrub the surface. Rate and record the degreeof attachment after scrubbing the surface with mineral spirits(MS) using Fig. 3

38、(4MS to 1MS).7.11 Other methods of removal such as pressure washingmay be used.8. Report8.1 The following information shall be documented andreported.8.1.1 Product manufacturer and product number.8.1.2 Batch number of product and reducer.8.1.3 Date and time of testing.8.1.4 Coating system used on dr

39、y fall collection panels.8.1.5 Prevailing temperature and relative humidity condi-tions.8.1.6 Type and amount of reducer added.8.1.7 Application method.8.1.8 Application equipment (pressure, tip size, hose diam-eter).8.1.9 Pre-test oven temperature.8.1.10 Post-test oven temperature.8.1.11 Dry fall d

40、istance (if greater or less than 18 ft).8.1.12 Elapsed time of atomization.8.1.13 Elapsed time from collection to evaluation.8.1.14 Qualitative attachment rating on ambient coatedpanels.6Alternatively, one side of the enclosure may be opened for ventilation betweenspray trials or product trials, or

41、both.7As defined by Section 6.1 of Practice D5402, the pressure exerted onto acellulose sponge or cotton cloth on a laboratory balance required to generate 1000to 2000 g of force shall be considered by this practice to be moderate pressure.FIG. 2 Illustration of Target Suspension Inside Upper Area o

42、f Enclosure(NoteTop is enclosed with plastic or tarpaulins.)D7868 13 (2017)38.1.15 Qualitative attachment rating on post-heated coatedpanels.8.1.16 Procedure(s) used to remove the overspray from thepanels (dry brushing, car washing solution/sponge, mineralspirits/cloth, etc.). If a car washing solut

43、ion is used, report themanufacturer of the car washing solution and the concentrationused.9. Keywords9.1 dry fall; dry fog; oversprayASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standar

44、d are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif

45、not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, whic

46、h you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,Un

47、ited States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 3 Dry Fall (Fog) Attachment RatingsD7868 13 (2017)4