API RP 10B-3-2016 Testing of Well Cements Used in Deepwater Well Construction (SECOND EDITION) .pdf

1、Testing of Well Cements Used in Deepwater Well Construction API RECOMMENDED PRACTICE 10B-3 SECOND EDITION, JANUARY 2016Special NotesAPI publications necessarily address problems of a general nature. With respect to particular circumstances, local,state, and federal laws and regulations should be rev

2、iewed.Neither API nor any of APIs employees, subcontractors, consultants, committees, or other assignees make anywarranty or representation, either express or implied, with respect to the accuracy, completeness, or usefulness of theinformation contained herein, or assume any liability or responsibil

3、ity for any use, or the results of such use, of anyinformation or process disclosed in this publication. Neither API nor any of APIs employees, subcontractors,consultants, or other assignees represent that use of this publication would not infringe upon privately owned rights.API publications may be

4、 used by anyone desiring to do so. Every effort has been made by the Institute to assure theaccuracy and reliability of the data contained in them; however, the Institute makes no representation, warranty, orguarantee in connection with this publication and hereby expressly disclaims any liability o

5、r responsibility for loss ordamage resulting from its use or for the violation of any authorities having jurisdiction with which this publication mayconflict.API publications are published to facilitate the broad availability of proven, sound engineering and operatingpractices. These publications ar

6、e not intended to obviate the need for applying sound engineering judgmentregarding when and where these publications should be utilized. The formulation and publication of API publicationsis not intended in any way to inhibit anyone from using any other practices.Any manufacturer marking equipment

7、or materials in conformance with the marking requirements of an API standardis solely responsible for complying with all the applicable requirements of that standard. API does not represent,warrant, or guarantee that such products do in fact conform to the applicable API standard.Users of this Recom

8、mended Practice should not rely exclusively on the information contained in this document.Sound business, scientific, engineering, and safety judgment should be used in employing the information containedherein. All rights reserved. No part of this work may be reproduced, translated, stored in a ret

9、rieval system, or transmitted by any means, electronic, mechanical, photocopying, recording, or otherwise, without prior written permission from the publisher. Contact the Publisher, API Publishing Services, 1220 L Street, NW, Washington, DC 20005.Copyright 2016 American Petroleum InstituteForewordN

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11、liability for infringement of letters patent.The verbal forms used to express the provisions in this recommended practice are as follows: the term “shall” denotes a minimum requirement in order to conform to the recommended practice; the term “should” denotes a recommendation or that which is advise

12、d but not required in order to conform to therecommended practice; the term “may” is used to express permission or a provision that is optional; and the term “can” is used to express possibility or capability.Informative elements: As used in a standard, “informative” denotes elements that: identify

13、the document, introduce itscontent and explain its background, development, and its relationship with other documents; or provide additionalinformation intended to assist the understanding or use of the document.Normative elements: As used in a standard, “normative” denotes elements that describe th

14、e scope of the document,and which set out provisions that are required to implement the standard.This document was produced under API standardization procedures that ensure appropriate notification andparticipation in the developmental process and is designated as an API standard. Questions concerni

15、ng theinterpretation of the content of this publication or comments and questions concerning the procedures under whichthis publication was developed should be directed in writing to the Director of Standards, American PetroleumInstitute, 1220 L Street, NW, Washington, DC 20005. Requests for permiss

16、ion to reproduce or translate all or any partof the material published herein should also be addressed to the director.Generally, API standards are reviewed and revised, reaffirmed, or withdrawn at least every five years. A one-timeextension of up to two years may be added to this review cycle. Stat

17、us of the publication can be ascertained from theAPI Standards Department, telephone (202) 682-8000. A catalog of API publications and materials is publishedannually by API, 1220 L Street, NW, Washington, DC 20005.Suggested revisions are invited and should be submitted to the Standards Department, A

18、PI, 1220 L Street, NW,Washington, DC 20005, standardsapi.org.iiiContentsPage1 Scope . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11.1 General . . . . . . . . . . . . . . . . . . . .

19、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11.2 Applicability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12 N

20、ormative References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 Terms and Definitions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

21、. . . . . . . . . 14 Sampling. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45 Preparation of Slurry. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

22、 . . . . . . . . . . . . . . . . . . . . . . . . . . 55.1 Preparation of Conventional Cement Slurry . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55.2 Preparation of Specialty Cement Slurry . . . . . . . . . . . . . . . . . . . . . . . . . . . .

23、. . . . . . . . . . . . . . . . . . . . . . . . . . 56 Determination of Temperature and Pressure Schedules for Conditioning and Testing. . . . . . . . . . . . . . . 56.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

24、. . . . . . . . . . . . . . . . . . . . 56.2 Slurry Conditioning Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77 Deepwater Well-simulation Strength Testing. . . . . . . . . . . . . . . . . . . . . . . . . . . . .

25、 . . . . . . . . . . . . . . . . . . . . 117.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 117.2 Sampling Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

26、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 117.3 Preparation of Slurry. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 117.4 Non-destructive Sonic Compressive Strength Determi

27、nation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 127.5 Destructive Method for Determination of Compressive Strength . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 157.6 Compressive Strength Determination . . . . . . . . . . . . . . . . . . . . . . . . . .

28、. . . . . . . . . . . . . . . . . . . . . . . . . . . . 208 Deepwater Well-simulation Thickening-time Tests . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 218.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

29、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 218.2 Sampling. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 218.3 Apparatus. . . . . . . . . . . . . . . . . . . . . .

30、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 218.4 Thickening-time Schedule Determination and Testing Method. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 219 Static Fluid Loss Testing . . . . . . . . . . . . .

31、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 289.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 289.2 Sampling. . . .

32、. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 289.3 Slurry Preparation for Fluid Loss Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

33、299.4 Testing Temperature Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 299.5 Conditioning the Slurry for Fluid Loss Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

34、99.6 Temperature and Pressure Testing Schedule Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 299.7 Fluid Loss Testing Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 299.8 Flui

35、d Loss Results and Reporting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2910 Well-simulation Slurry Stability Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2910

36、.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2910.2 Sampling Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

37、. . . . . . . . . . . . . . . . . . 2910.3 Slurry Preparation for Slurry Stability Testing. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2910.4 Testing Temperature Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

38、 . . . . . . . . . . . . . . . . . . . 2910.5 Conditioning the Slurry for Stability Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3010.6 Temperature and Pressure Testing Schedule Determination . . . . . . . . . . . . . . . . . . . . . . . .

39、 . . . . . . . . . . . 3010.7 Slurry Stability Testing Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3011 Determination of Rheological Properties and Gel-strength using a Rotational Viscometer . . . . . . . . . . 3011.1

40、General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3011.2 Sampling Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

41、 . . . . . . . . . . . . . . . . 30vContentsPage11.3 Slurry Preparation for Rheological and Gel-strength Property Determination . . . . . . . . . . . . . . . . . . . . . 3011.4 Testing Temperature Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

42、 . . . . . . . . . . . 3011.5 Conditioning the Slurry for Rheological and Gel-strength Testing. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3011.6 Temperature and Pressure Testing Schedule Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3011.7 Rheo

43、logical Property and Gel-strength Determination Testing Methods. . . . . . . . . . . . . . . . . . . . . . . . . . 3011.8 Reporting and Characterization of Rheological Behavior . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3012 Compatibility of Wellbore Fluids . . . . .

44、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3112.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3112.2 Sampling

45、Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3112.3 Preparation of Test Fluids Used in Compatibility Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3112.5 Cond

46、itioning of the Fluids Used in Compatibility Testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3112.6 Temperature and Pressure Testing Schedule Determination . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3112.7 Compatibility Determination Tes

47、ting Methods. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3112.8 Interpretation of Compatibility Testing and Spacer Surfactant Screening Test Results . . . . . . . . . . . . . 31Bibliography . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

48、 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32Tables1 Temperature and Pressure Schedule: Pressurized Consistometer Conditioning Method, Testing Location Shallower than Wellbore Hotspot Location . . . . . . . . . . . . . . . . . . . . . . . . .

49、 . . . . . . . . . . . 92 Temperature and Pressure Schedule: Pressurized Consistometer Conditioning Method, Testing Location Deeper than Wellbore Hotspot Location . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93 Temperature and Pressure Schedule: Well-simulation Thickening-time for Casing or Liner without a Liner-top Packer / Non-expandable Liner Hanger System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 224 Temperature and Pressure Schedule: Well-simulation Thickening-time for Casing or Liner with a Liner-top Packer/Non-expanda