AECMA PREN 2565-1993 Aerospace Series Preparation of Carbon Fibre Reinforced Resin Panels for Test Purposes Edition P 2《航空航天系列.碳纤维增强塑料准备测试用 P 2》.pdf

1、CEN PREN+iSbS 93 3404589 0045599 171 Edition approved for publication 1993-05-10 AECMA STANDARD NORME AECMA AECMA NORM Comments should be sent within six months after the date of publication to AECMA Technopolis - 175, rue Jean-Jacques Rousseau 921 38 Issy-les-Moulineaux Cedex - FRANCE prEN 2565 Edi

2、tion P 2 May 1993 UDC : EDITE PAR LASSOCIATION EUROPEENNE DES CONSTRUCTEURS DE MATERIEL AEROSPATIAL Technopolis - 175, rue Jean-Jacques Rousseau - F-92138 Issy-les-Moulineaux Cedex - Tl. (1) 47.36.98.76 Key words : ENGLISH VERSION Aerospace series Preparation of carbon fibre reinforced resin panels

3、for test purposes Srie arospatiale Prparation de panneaux base de rsine et fibres de carbone destins llaboration dprouvettes Supersedes issue P 1 June 1987 Luft- und Raumfahrt Herstellen von CFK- Prf platten This “Aerospace Series “ Prestandard has been drawn up under the responsibility of AECMA (As

4、sociation Europenne des Constructeurs de Matriel Arospatial). It is published on green paper for the neds of AECMA-Members. It has been technically approved by the experts of the concerned Technical Committee following comment by the Member countries. Subsequent to the publication of this prestandar

5、d, the technical content shall not be changed to an extent that interchangeability is affected, physically or functionally, without re-identification of the standard. After examination and signature of the AECMA Standard Checking Centre (NPS) and formal agreement of the Official Services of the Memb

6、er countries it will be submitted as a draft European Standard to CEN (European Committee for Standardization) for formal vote. Nota - Extra copies can be supplied by B.N.A.E. - Technopoli 54 - 199, rue Jean-Jacques Rousseau - 921 38 ISSY-LESMOULINEAUX CEDEX C7 Chairman M. Bezaud I I 0 aecma 19C - C

7、opyright Association Europeene des Constructeurs de Materiel Aerospatial Provided by IHS under license with AECMANot for ResaleNo reproduction or networking permitted without license from IHS-,-,-CEN PRENu25b5 93 m 3404589 0045b00 713 m prEN 2565 Page 2 - Contents 1 Scope 2 Principle 3 References 4

8、Equipment and mate for the preparation of 5 Working procedure -6 Report of preparation of test panel . : ., , . . _. . Copyright Association Europeene des Constructeurs de Materiel Aerospatial Provided by IHS under license with AECMANot for ResaleNo reproduction or networking permitted without licen

9、se from IHS-,-,-CEN PRENx25b5 93 m 3404589 0045bOL b5T m prEN 2565 Page 3 1 Scope This standard describes the preparation of panels with any desired fibre orientation of unidirectional orientated carbon fibre or fabric with thermosetting resins. The purpose of this standard is to describe recommende

10、d processes for the preparation of the panels from which test specimens subsequently are machined. Standard specimens prepared in this manner may be used either for evaluating the components .e. the carbon reinforcement, finishes, resins, catalysts, curing agents, etc. or for verifying the overall q

11、uality of the finished products. 2 Principle Preparation of the laminates or panels by one of the following methods : 2.1 The carbon fibre reinforcement impregnated with liquid resin containing a suitable catalyst or curing agent is moulded under conditions of temperature and pressure appropriate fo

12、r the resin and curing system. Method A (wet lay-up technique) 2.2 Method B (prepreg) The carbon fibre reinforcement impregnated with resin (prepreg) is moulded under conditions of temperature higher than room temperature and pressures appropriate for the resin system. 3 Normative references EN 2564

13、 Aerospace series - Carbon fibre laminates - Test method for the determination of the fibre and resin fractions and porosity content EN 2743 Aerospace series - Reinforced plastics - Standard procedures for conditioning prior to testing 4 Equipment and materials recommended for the preparation of pan

14、els by methods A and B 4.1 Equipment 4.1 .I Press of any hydraulic or mechanical type, with the following requirements a) Temperature measuring and controlling devices to maintain the curing temperature between the specified limits. b) Moulding force with an accuracy of 5 % over the period of time r

15、equired for curing of the resin. ci The pressing tool 1 (see figure 1) consists of frame il), ram (2) and base (3). The height of the frame shall be large enough to provide a moulding chamber where the reactive resin composition can be put in place in one operation. By means of appropriately constru

16、cted guides, e.g. centering pins (41, a gap between the ram and the frame of 0.20 mm minimum shall be ensured. 1) Published as AECMA Prestandard at the date of publication of this standard - Copyright Association Europeene des Constructeurs de Materiel Aerospatial Provided by IHS under license with

17、AECMANot for ResaleNo reproduction or networking permitted without license from IHS-,-,-CEN PRENt2565 93 m 3404589 0045602 59b m prEN 2565 Page 4 d) The tool 2 (see figure 2) consists of two flat plates, which shall be guided only at the four corners (open pressing tool). By placing distance pieces

18、between the guides, a specific thickness of the test panel can be obtained. 4.1.2 Autoclave of any dry heat type with the following requirements : a) as 4.1.1 (a). b) a heat up speed of at least 3 OC/min. c) capable of maintaining the required pressure to an accuracy of 10 kPa over the period of tim

19、e required for curing of the resin. d) vacuum pumps capable of applying a vacuum equal to at least 80 kPa. 4.1.3 Ruler for measuring length and width to an accuracy of 0,5 mm 4.1.4 Micrometer screw type with an accuracy of 0,Ol mm for measuring the thickness 4.1.5 Balance With an accuracy of 0,Ol g

20、4.1.6 Cutting device such as a knife with a sharp blade 4.2 Materials 4.2.1 between the parties concerned. Metal lay-up plate of 500 mm x 500 mm x 7 mm or any other suitable dimensions agreed upon 4.2.2 When necessary, metal cover plate of 300 mm x 300 mm x 7 mm or any other suitable dimensions agre

21、ed upon between the parties concerned. 4.2.3 Where required, rubber pressure retaining rings resistant to a temperature at least 20 OC higher than the actual curing temperature. 4.2.4 Release film resistant to a temperature at least 20 OC higher than the actual curing temperature, such as polyvinylf

22、luoride (PVF), polytetrafluoroethylene (PTFE) or PTFE coated fabric. 4.2.5 When necessary, perforated release film resistant to a temperature at least 20 OC higher than the actual curing temperature, such as PTFE or PTFE coated fabric. 4.2.6 Pressure blanket material with the capacity of formability

23、, resistant to polymerisation products and resistant to a temperature at least 20 OC higher than the actual curing temperature, such as PVF, PTFE or PTFE coated fabric. 4.2.7 Breather material such as aluminium gauze and glass fabric. 4.2.8 Absorption material for absorption of excess resin. Example

24、s are : 1) Woven glass fibre fabric having a surface mass of 100 g/mz capable of absorbing approximately 60 g/m2 resin, 2) Woven glass fibre fabric having a surface mass of 300 g/mz capable of absorbing approximately 115 g/m2 resin, 3) Polyamid fibre fabric having a surface mass of 60 g/m2 capable o

25、f absorbing approximately 40 g/m2 resin. - li- Copyright Association Europeene des Constructeurs de Materiel Aerospatial Provided by IHS under license with AECMANot for ResaleNo reproduction or networking permitted without license from IHS-,-,-CEN PREN*:2565 93 w 3404589 O045603 422 W prEN 2565 Page

26、 5 4.2.9 Metal edge surrounding material strips or other suitable material with a length of 300 mm and a width of 15 mm, or any other dimensions agreed upon between the parties concerned. The thickness depends on thickness of plate or panel to be produced. 4.2.10 Sealing tape resistant to a temperat

27、ure at least 20 OC higher than the actual curing temperature. 5 Working procedure The materials to be used for preparing the test panels, including the material from which the test panels have to be made, shall be conditioned at a temperature of (23 f 2) OC and a relative humidity of (50 k 5) % as s

28、pecified in EN 2743 for at least 2 h. 5.1 5.1.1 The carbon fibre or carbon fibre fabric shall be conditioned during 6 h to the standard atmosphere as specified in EN 2743 and then impregnated with the required resin containing a suitable catalyst or curing agent. Method A (wet lay-up technique) 5.1.

29、2 The resin content of the impregnated carbon fibre assembly shall not be in excess of 45 % by weight. 5.1.3 From the prepared impregnated carbon fibre assembly the required number of layers to produce the final cured thickness of panel (see note in 5.1.5) are cut to the width and length required an

30、d placed on the lay-up plate (4.2.1) to produce a panel of the required dimensions. 5.1.4 Unless otherwise specified in the materials data sheet, not more than 50 % of the gel time of the resin at the temperature of the impregnation may elapse before the start of the cure cycle. 5.1.5 The assembly l

31、aminated on the metal lay-up plate (4.2.1) shall be made ready for curing as presented in figure 1 or figure 2 for pressing tools and figure 3 or figure 4 for bladder press method or autoclave method. The total number of absorption layer material (4.2.8) for excess resin absorption depends on the ac

32、tual resin content required for the cured laminate or panel (see figure 5 as an example). The laminate or panel thickness and resin content are also a function of pressure, temperature and other factors, depending upon the properties of the carbon fibre and of the resin system (see note). NOTE : It

33、will be necessary, before marking the number of panels required for preparing the test specimens, to determine by experiment the number of layers from the prepared resin impregnated carbon fibre tape or sheet and number of absorption layers for excess resin combined with the pressure necesSan/ to ob

34、tain panels of the required cured thickness and resin content. 5.1.6 The temperature, pressure and time of curing are stipulated by agreement or specified in the material data sheet, depending on the type of resin, catalyst or curing agent. The temperature stipulated shall be maintained during the c

35、uring cycle such that the temperature values indicated by the temperature measuring device will remain within the ranges required for the particular resin system (see figure 6). The temperature of any point on the active surface of the plate or panel shall not differ by more than f 2 OC from the val

36、ue indicated by the temperature measuring device (4.1.1.(a) and 4.1.2 (a). 5.1.7 After completion of the curing process the test panel has to be taken from the press or autoclave and cooled if necessary in such a way that any deformation, damage, etc. is avoided. 5.1.8 The carbon fibre orientation(s

37、) relative to the length direction of the panel shall be indicated on a pressure sensitive paper tag or other suitable means agreed upon and applied to the panel. Copyright Association Europeene des Constructeurs de Materiel Aerospatial Provided by IHS under license with AECMANot for ResaleNo reprod

38、uction or networking permitted without license from IHS-,-,-CEN PRENx25b5 93 3404589 0045b04 369 prEN 2565 Page 6 5.1.9 Where no other treatment is specified the panels may be used, in this condition, to produce test specimens. If not specified in the relevant standard on testing the types, sizes an

39、d orientations of the specimens with respect to the orientation of the carbon fibre reinforcement within the panel shall be stipulated by separate agreement. The margins of the panels up to at least 10 mm from its edges shall be discarded. 5.2 Method B (prepreg) 5.2.1 If the material is stored at te

40、mperature lower than the standard specified temperature of EN 2743, it shall be retained in an airtight bag to prevent moisture pick-up. The required material shall be conditioned at a temperature of (23 k 2)OC and relative humidity of (50 f 5) % as specified in EN 2743. After conditioning the mater

41、ial required for the preparation of the test panels shall be cured within 6 h, unless otherwise specified. 5.2.2 The carbon fibre prepreg is cut to the width and length required to prepare a laminate of the required dimensions. 5.2.3 A lay-up to produce a cured test panel shall be prepared as descri

42、bed in clause 5.1.3 through clause 5.1.9. 5.3 5.3.1 Measure the length (4.1.3) of each of the four sides to an accuracy of 0,5 mm after having trimmed at least 10 mm from its edges (5.1.8). Calculate the arithmetic mean of the four measurements rounded off to the nearest mm. Determination of the qua

43、lity of the panels 5.3.2 Measure the thickness (4.1.4) at each of the four corners but not closer than 25 mm to the edges and in the centre to an accuracy of 0,05 mm. Calculate the arithmetic mean of the five measurements rounded off to the nearest 0,l mm. 5.3.3 If required, take a test specimen fro

44、m two diagonally opposite corners with the dimensions of 20 mm x 10 mm at the thickness of the panel. From both test specimens the carbon fibre content by volume and weight shall be determined by resin digestion in accordance with EN 2564-A. 5.3.4 Determine the porosity and other defects by means of

45、 ultrasonic inspection method using the procedure agreed between the parties concerned. 6 Report of preparation of test panel The report of preparation of the test panel shall include the following : 6.1 Place and date of production of test panel. 6.2 Details of number of plies, stacking sequence an

46、d ply orientation. 6.3 Description of materials including batch, roll numbers used for preparing the test panel (nature and type of resin, catalyst, curing agent or other additives including the amounts used, nature and type of carbon fibre, nature of finish, etc.). Copyright Association Europeene d

47、es Constructeurs de Materiel Aerospatial Provided by IHS under license with AECMANot for ResaleNo reproduction or networking permitted without license from IHS-,-,-CEN PRENr25b5 93 D 3404589 O045605 2T5 D prEN 2565 Page 2 6.4 temperatures and pressures, etc.). Description of production equipment (ty

48、pe of press, autoclave, mould, method of checking 6.5 force), temperature, curing-time, post-curing, etc.). Working procedure (designation of method as given in this standard, moulding pressure (or 6.6 Length and width of panel (individual measurements and average value in mm). 6.7 Thickness of pane

49、l (individual measurements and average value in mm). 6.8 percent by volume and by weight. Fibre content of panel (when measured) - individual measurements and average value in 6.9 Porosity level shown by ultrasonic scan picture (when measured) 6.10 Special notes Copyright Association Europeene des Constructeurs de Materiel Aerospatial Provided by IHS under license with AECMANot for ResaleNo reproduction or networking permitted without license from