ANSI ASTM D3138-2004 Standard Specification for Solvent Cements for Transition Joints Between Acrylonitrile- Butadiene-Styrene (ABS) and Poly(Vinyl Chloride) (PVC) Non-Pressure Pip.pdf

1、Designation: D3138 04 (Reapproved 2016) An American National StandardStandard Specification forSolvent Cements for Transition Joints Between Acrylonitrile-Butadiene-Styrene (ABS) and Poly(Vinyl Chloride) (PVC)Non-Pressure Piping Components1This standard is issued under the fixed designation D3138; t

2、he number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.Th

3、is standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope1.1 This specification provides general requirements forsolvent cements used in joining acrylonitrile-butadiene-styrene(ABS) plastic pipe or fittings to poly(vinyl chloride) (PVC)plastic pipe or fittings.1.2

4、These cements are intended for use in cementing tran-sition joints between ABS and PVC materials in non-pressureapplications only (25 psi (170 kPa) or less).NOTE 1This specification was developed to provide a means forjoining an ABS non-pressure piping system using a solvent-cementedtransition joint

5、, for example, joining ABS building drain to a PVC sewersystem. The intention was not to create a specification for an all purposeABS-PVC solvent cement that would be used for mixing ofABS and PVCpiping materials nor to specify a cement that could generally be used foreither material. Specific cemen

6、ts for ABS or PVC components should beused (see 1.3).1.3 Solvent cements used for joining PVC pipe and fittingsare specified in Specification D2564. Solvent cements used forjoining ABS pipe and fittings are specified in SpecificationD2235.1.4 Arecommended procedure for joiningABS to PVC pipeand fitt

7、ings for non-pressure applications is given in theappendix.1.5 The values stated in inch-pound units are to be regardedas standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.6 The following safety h

8、azards caveat pertains only to thetest methods portion, Section 6, of this specification: Thisstandard does not purport to address all of the safety concerns,if any, associated with its use. It is the responsibility of the userof this standard to establish appropriate safety and healthpractices and

9、determine the applicability of regulatory limita-tions prior to use.2. Referenced Documents2.1 ASTM Standards:2D1084 Test Methods for Viscosity of AdhesivesD1600 Terminology forAbbreviated Terms Relating to Plas-ticsD1784 Specification for Rigid Poly(Vinyl Chloride) (PVC)Compounds and Chlorinated Po

10、ly(Vinyl Chloride)(CPVC) CompoundsD2235 Specification for Solvent Cement for Acrylonitrile-Butadiene-Styrene (ABS) Plastic Pipe and FittingsD2564 Specification for Solvent Cements for Poly(VinylChloride) (PVC) Plastic Piping SystemsD2661 Specification for Acrylonitrile-Butadiene-Styrene(ABS) Schedul

11、e 40 Plastic Drain, Waste, and Vent Pipeand FittingsD2665 Specification for Poly(Vinyl Chloride) (PVC) PlasticDrain, Waste, and Vent Pipe and FittingsF402 Practice for Safe Handling of Solvent Cements,Primers, and Cleaners Used for Joining ThermoplasticPipe and FittingsF412 Terminology Relating to P

12、lastic Piping SystemsF493 Specification for Solvent Cements for ChlorinatedPoly(Vinyl Chloride) (CPVC) Plastic Pipe and Fittings3. Terminology3.1 DefinitionsDefinitions are in accordance with Termi-nology F412, and abbreviations are in accordance with Termi-nology D1600, unless otherwise specified.4

13、. Materials and Manufacture4.1 The solvent cement shall be a solution of Class12454-B, unplasticized poly(vinyl chloride) molding or extru-sion compound as classified in Specification D1784, or equiva-lent PVC resin.1This specification is under the jurisdiction of ASTM Committee F17 on PlasticPiping

14、 Systems and is the direct responsibility of Subcommittee F17.20 on Joining.Current edition approved Nov. 1, 2016. Published November 2016. Originallyapproved in 1972. Last previous edition approved in 2011 as D3138 04(2011).DOI: 10.1520/D3138-04R16.2For referenced ASTM standards, visit the ASTM web

15、site, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United Stat

16、esThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Tra

17、de (TBT) Committee.14.2 Either virgin or clean rework material may be used,provided that the rework material is generated from the solventcement manufacturers own production, is compatible withvirgin material, and will produce a cement that meets therequirements of this specification.4.3 The cement

18、shall be free-flowing and shall not containlumps, macroscopic undissolved particles, or any foreignmatter that will adversely affect the ultimate joint strength orchemical resistance of the cement.4.4 The cement shall show no gelation. It shall show nostratification or separation that cannot be remo

19、ved by stirringor shaking.4.5 Inert fillers may be added, provided the resulting cementmeets all requirements of this specification.4.6 The solvents used in the formulation of this solventcement shall consist of tetrahydrofuran (THF) in combinationwith cyclohexanone or methyl ethyl ketone (MEK), or

20、both.NOTE 2It is recommended that solvent cements made to this speci-fication not be orange since that color is recommended for use with CPVCsolvent cement under Specification F493.5. Other Requirements5.1 Resin ContentThe PVC resin content shall be 10 %minimum when tested in accordance with 6.1.5.2

21、 DissolutionThe cement shall be capable of dissolvingan additional 3 weight % of Class 12454-B, PVC compound orthe equivalent PVC resin at 73.4 6 3.6F (23 6 2C) withoutevidence of gelation.5.3 ViscosityThe minimum viscosity at room temperatureshall be 90 cP (90 mPas) when tested in accordance with 6

22、.2.NOTE 3Cements approaching the minimum viscosity requirement ofthis specification generally are not recommended for noninterference-typefit (where a gap exists between the pipe and fitting socket).5.4 Lap Shear StrengthThe minimum average lap shearstrength when tested in accordance with 6.3.2 shal

23、l be 600 psi(4.1 MPa) after a 72-h curing time.5.5 Hydrostatic Burst StrengthThe minimum average hy-drostatic burst strength when tested in accordance with 6.3.3shall be 200 psi (1.4 MPa) after a 72-h curing time.6. Test Methods6.1 Solids Content:6.1.1 Apparatus:6.1.1.1 Ointment Tins (Style No. 12,

24、1-oz (30-mL), allmetal).6.1.1.2 Vacuum Oven.6.1.1.3 Analytical Balance.6.1.1.4 Centrifuge.6.1.2 Procedure:6.1.2.1 Stir the sample thoroughly with a spatula beforeweighing (Note 4). Weight 3.0 6 0.5 g of the sample to thenearest 1 mg into a tared ointment tin. Place the tin into thevacuum oven (Note

25、5), and heat at 248F (120C) for 45 min+ 15, 0 min. Discard specimens left in for more than 1 h. Thevacuum must be continually in operation to draw off flammablesolvents. Absolute pressure should not exceed 15 mm Hg.Remove the tin from the oven and place in a desiccator untilcooled to room temperatur

26、e. Weigh the tin and dried sample tothe nearest 1 mg.NOTE 4This material is usually nonhomogeneous and shall bethoroughly stirred before weighing. The weighing shall also be accom-plished quickly to avoid loss of solvent by volatilization. Some vacuumovens require a longer period of time than 15 min

27、 to reach 248F (120C)even after preheating. It is recommended that the operator watch closelythe time required to reach 248F (120C) and, by manipulation of the heatcontrol mechanism, minimize the amount of time required to reach 248F(120C) while not exceeding the required temperature.NOTE 5The use o

28、f a vacuum oven is mandatory for drying thespecimen. This oven has neither an exposed heating surface nor an openflame, thus avoiding the danger of flashing. The oven also provides anopen vacuum to exhaust solvent fumes.6.1.2.2 After weighing, dissolve the dried sample in THFand determine quantitati

29、vely any inert fillers by means ofcentrifuging. Deduct the weight of the fillers determined fromthe weight of the dried sample prior to calculating the contentof PVC resin in the cement.NOTE 6Dissolve most of the dried sample by adding 15 mL of THFto the sample in the ointment tin and stirring with

30、a glass rod for 15 min.Dissolve the remainder with a second addition of 15 mL of THF, followedby a third addition of 5 mL of THF to rinse the ointment tin. Centrifugethe entire volume at 20 000 r/min for 15 min. Discard the supernatantliquid. Add 15 mL of THF to the tube, mix thoroughly, and transfe

31、r thetube contents to the ointment tin. Use 2 mL more of THF to wash downthe tube, and pour into the ointment tin. Evaporate off the THF in thevacuum oven at 248F (120C) for 45 min. Cool in desiccator, weigh thetin to the nearest 1 mg, and calculate the percent of inert filler present inthe cement.6

32、.1.3 CalculationCalculate the percentage of PVC resin,R, as follows:R,%5 B 2 A 2 D!/C 2 A!# 3100where:A = weight of ointment tin,B = weight of tin and specimen after drying,C = weight of tin and specimen before drying, andD = weight of inert filler, if present.6.2 ViscosityMeasure the viscosity in a

33、ccordance withMethod B of Test Methods D1084 except that conditioning totemperature equilibrium only is required. For qualificationpurposes use a Model RVF viscometer, a speed of 10 r/min,and the spindle that, by trial, gives the closest reading to centerrange of scale for the cement being tested. O

34、ther speeds may beused for quality control purposes.6.3 Bond Strength:6.3.1 Number of SpecimensA minimum of seven speci-mens shall be tested for the lap shear strength test (see 5.4). Aminimum of five specimens shall be tested for the hydrostaticburst strength test (see5.5).6.3.2 Lap Shear Strength:

35、6.3.2.1 Each test specimen (Fig. 1) shall consist ofa1by1-in. (25 by 25-mm) section cut from a14-in. (6-mm) thickType I rigid ABS sheet anda1by2-in. (25 by 50-mm) sectioncut from a14-in. (6-mm) thick Type I rigid PVC sheet.6.3.2.2 Clean the surfaces to be adhered with a clothdampened with methyl eth

36、yl ketone (MEK).D3138 04 (2016)26.3.2.3 Using a 1-in. (25-mm) natural bristle brush, apply athin layer of cement to the complete surface ofa1by1-in. (25by 25-mm) sheet section and to the center of a 1 by 2-in. (25by 50-mm) sheet section.6.3.2.4 Assemble these sections immediately and rotate the1 by

37、1-in. (25 by 25-mm) section 180 on the 1 by 2-in. (25 by50-mm) section, within 5 s, using light hand pressure (approxi-mately 0.5 lbf (2 N).6.3.2.5 Place the assembled test specimen on a clean, levelsurface using the 1 by 2-in. (25 by 50-mm) section as a base.After 30 s, place a 4.4-lb (2-kg) weight

38、 on the test specimen fora period of 3 min, and then remove.6.3.2.6 Store the assembled test specimens at 73.4 6 3.6F(23 6 2C) for the specified time and test immediately in aholding fixture similar to that shown in Fig. 2. The shear speedshall be 0.05 in. (1.25 mm)/min. Express the results in pound

39、sper square inch (or megapascals).6.3.2.7 Disregard the lowest and highest value for thecalculation of the average lap shear strength.6.3.3 Hydrostatic Burst Strength:6.3.3.1 Use nominal 2-in. PVC pipe meeting the require-ments of Specification D2665 and 2-in. ABS couplings meet-ing the requirements

40、 of Specification D2661.6.3.3.2 Cut the pipe square into 6-in. (152-mm) lengths.6.3.3.3 Deburr the pipe and clean the pipe and fitting with aclean dry rag.6.3.3.4 Check the dry fit of the pipe into the coupling socketfor interference fit. The fit shall be such that the pipe will enterthe socket from

41、13 to23 of the socket depth dry when as-sembled by hand.6.3.3.5 Dip a 1-in. brush into MEK and apply a uniformcoating of MEK on the PVC pipe. Allow to set 30 s.6.3.3.6 Immediately flow on a uniform liberal coat ofcement on the PVC pipe with a 1-in. bristle brush.6.3.3.7 Apply a uniform light coat of

42、 cement to the ABScoupling.6.3.3.8 Apply a second uniform layer of cement to the pipe.6.3.3.9 Assemble immediately while joining surfaces arewet. Hold joint together for 1 min for initial set and wipe offbead of cement at juncture of pipe and fitting.6.3.3.10 Store the cemented specimens at 73.4 6 3

43、.6F (236 2C) and 50 6 5 % relative humidity for 72 h and testimmediately.6.3.3.11 Increase the internal hydrostatic pressure at the rateof 200 psi (1.4 MPa) 6 10 % until failure occurs.7. Retest and Rejection7.1 If the results of any test(s) do not meet the requirementsof this specification, the tes

44、t(s) may be conducted again inaccordance with an agreement between the purchaser and theseller. There shall be no agreement to lower the minimumrequirement of the specification by such means as omittingtests that are a part of the specification, substituting ormodifying a test method, or by changing

45、 the specificationlimits. In retesting, the product requirements of this specifica-tion shall be met, and the test methods designated in thespecification shall be followed. If, upon retest, failure occurs,the quantity of product represented by the test(s) does not meetthe requirements of this specif

46、ication.8. Report8.1 Report the following information:8.1.1 Name of cement manufacturer,8.1.2 Lot number,8.1.3 Total PVC resin, 0/0W,8.1.4 Dissolution, pass or fail,8.1.5 Viscosity,8.1.6 Average lap shear strength at each cure time andcomplete identification of PVC and ABS sheet stock used inthe tes

47、ts,8.1.7 Average hydrostatic burst strength, and8.1.8 Total inert filler, 0/0W.9. Certification9.1 When specified in the purchase order, the manufacturershall certify to the purchaser or to his nominee that the productsin the specified lots meet all the requirements of this specifi-cation and, when

48、requested, shall include a copy of themanufacturers routine quality control tests results to documentthat the specification requirements have been met. Each certi-fication so furnished shall be signed by an authorized agent ofthe manufacturer.10. Container Labeling and Marking10.1 Container labeling

49、 of cement shall include the follow-ing:10.1.1 Manufacturers or suppliers name and address andtradename or trademark.10.1.2 This designation: ASTM D3138.10.1.3 Function of material; for use on transition jointsbetween ABS and PVC non-pressure systems (examples:building drain to building sewer, building sewer to mainsewer).10.1.4 Procedure or instructions for application of the ce-ment.FIG. 1 Compressive Shear SpecimenFIG. 2 Typical Specimen Holding FixtureD3138 04 (2016)310.1.5 Lot number of batch on container (not on closure orlid.)