1、Designation: D5213 12Standard Specification forPolymeric Resin Film for Electrical Insulation and DielectricApplications1This standard is issued under the fixed designation D5213; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the
2、 year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope*1.1 This specification cov
3、ers requirements for the material,dimensions and tolerances, and property values of film, in sheetor strip form, with or without heat-sealable coatings.1.2 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.NOTE 1This document is
4、similar to IEC 60674, Part 3, Sheets 2, 4, 5,6, and 7.2. Referenced Documents2.1 ASTM Standards:2D149 Test Method for Dielectric Breakdown Voltage andDielectric Strength of Solid Electrical Insulating Materialsat Commercial Power FrequenciesD883 Terminology Relating to PlasticsD1711 Terminology Rela
5、ting to Electrical InsulationD2305 Test Methods for Polymeric Films Used for Electri-cal InsulationD3636 Practice for Sampling and Judging Quality of SolidElectrical Insulating MaterialsD4088 Practice for Preparation for Shipment of Solid Elec-trical Insulating Materials (Withdrawn 2003)32.2 IEC Sta
6、ndards:Publication 60674-3 Specification for Electrical Films forElectrical Purposes43. Terminology3.1 DefinitionsDefinitions are in accordance with Termi-nologies D1711 and D883 unless otherwise specified.3.2 Definitions of Terms Specific to This Standard:3.2.1 sheet, nmaterial greater than 75 mm i
7、n width.3.2.2 strip, nmaterial 75 mm or less in width.4. Classification4.1 This specification covers the following:4.1.1 Type IGeneral purpose,4.1.2 Type IIHeat sealable,4.1.2.1 Grade 1One side coated, and4.1.2.2 Grade 2Two sides coated.4.2 Materials:4.2.1 Item APoly(N,N-p,p-oxydiphenylenepyromellit
8、imide),4.2.2 Item BPoly(N,N-p,p-oxydiphenylenebiphenyltetracarboxylimide,4.2.3 Item CPoly(N,N-p-phenylenebiphenyltetracarboxylimide),4.2.4 Item DFEP-fluorocarbon, and4.2.5 Item EPolyethylene terephthalate.4.2.6 Item FPolyethylene naphthalate.4.2.7 Item GPolyetherimide.5. Ordering Information5.1 Orde
9、r the film covered by this specification stating thetype, grade, class, thickness, width, and roll dimensions.6. Materials6.1 Type I material is flexible, unsupported film.6.2 Type II material is film meeting all of the requirementsof Type I, and having a heat-sealable coating on one or bothsides.7.
10、 Requirements7.1 The film covered by this specification shall meet theproperty requirements given in Tables 1-7 and Table 8 whentested by the methods given in Test Methods D2305.1This specification is under the jurisdiction of ASTM Committee D09 onElectrical and Electronic Insulating Materials and i
11、s the direct responsibility ofSubcommittee D09.07 on Flexible and Rigid Insulating Materials.Current edition approved Nov. 1, 2012. Published November 2012. Orginallyapproved in 1991. Last previous edition approved in 2007 as D5213 07. DOI:10.1520/D5213-12.2For referenced ASTM standards, visit the A
12、STM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3The last approved version of this historical standard is referenced onwww.astm.org.4Available from Amer
13、ican National Standards Institute (ANSI), 25 W. 43rd St.,4th Floor, New York, NY 10036, http:/www.ansi.org.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1TABLE 1 Proper
14、ty Values for Type I, Class A Film poly(N,N-p-p-oxydiphenylene pyromellitimide)Average Property ValueNominal Thickness, m (mils)7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)Tensile strength, min MPa (psi),machine direction and transversedirection69(10 000)97(14 000)138(2
15、0 000)138(20 000)138(20 000)138(20 000)138(20 000)138(20 000)Elongation, min percent, machineand transverse direction10 20 35 35 40 45 45 45Shrinkage, max percent, afterexposure to 200 C (392 F),machine and transverse direction. . 0.30 0.30 0.35 0.35 0.35 0.35Moisture absorption, max percent, 100 %
16、RH 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0Dielectric strength, min kV/mm(V/mil), 60 HzA,B120(3000)120(3000)180(4500)180(4500)150(3800)140(3600)100(2500)100(2500)Volume resistivity, min -cm,B ,C10151015101510151015101510151015Permittivity, max at 1 kHzB4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0Dissipation factor, max a
17、t 1 kHzB0.007 0.005 0.005 0.004 0.004 0.004 0.004 0.004AUse Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shall be used for compliance.TABLE 2 Property Values for Type I, Class B Film poly(N,N-p-
18、p-oxydiphenylene biphenyltetracarboxylimide)Average Property ValueNominal Thickness, m (mils)7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 40 (1.6) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)Tensile strength, min MPa (psi),machine direction and transversedirection110(15 000)138(20 000)196(28 000)196(28 000)196(28
19、000)196(28 000)196(28 000)196(28 000)196(28 000)Elongation, min percent, machineand transverse direction24 40 80 80 80 80 80 80 80Shrinkage, max percent, afterexposure to 200 C (392 F),machine and transverse direction. . 0.30 0.30 0.35 0.35 0.35 0.35 0.35Moisture absorption, max percent, 100 % RH 2.
20、0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0Dielectric strength, min kV/mm(V/mil), 60 HzA,B120(3000)120(3000)180(4500)180(4500)150(3800)140(3500)130(3300)100(2500)95(2400)Volume resistivity, min -cm,B ,C101510151015101510151015101510151015Permittivity, max at 1 kHzB4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0Dissipatio
21、n factor, max at 1 kHzB0.007 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005AUse Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shall be used for compliance.TABLE 3 Property Values for Type I, Cla
22、ss C Film poly(N,N-p-phenylene biphenyltetracarboxylimide)Average Property ValueNominal Thickness, m (mils)7.5 (0.3) 13 (0.5) 20 (0.8) 25 (1.0) 40 (1.6) 50 (2.0) 75 (3.0) 100 (4.0) 130 (5.0)Tensile strength, min MPa (psi),machine direction and transversedirection133(19 000)176(25 000)241(34 000)241(
23、34 000)241(34 000)241(34 000)241(34 000)241(34 000)241(34 000)Elongation, min percent, machineand transverse direction25 25 25 25 25 25 25 25 25Shrinkage, max percent, afterexposure to 200 C (392 F),machine and transverse direction. . 0.15 0.15 0.15 0.20 0.20 0.20 0.20Moisture absorption, max percen
24、t, 100 % RH 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8Dielectric strength, min kV/mm(V/mil), 60 HzA,B120(3000)120(3000)180(4500)180(4500)150(3800)140(3500)120(3000)100(2500)95(2400)Volume resistivity, min -cm,B ,C101510151015101510151015101510151015Permittivity, max at 1 kHzB4.0 4.0 4.0 4.0 4.0 4.0 4.0 4.0
25、 4.0Dissipation factor, max at 1 kHzB0.007 0.005 0.005 0.005 0.005 0.005 0.005 0.005 0.005AUse Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shall be used for compliance.D5213 1227.1.1 Type II fi
26、lms, prior to coating, shall meet all of therequirements given in Table 1 for films of the thicknesses givenin Table 9.7.1.2 Type II films, after coating, shall meet all of therequirements given in Table 1 for elongation, before and afterheating, and for shrinkage as given in Table 1 for films of th
27、ethicknesses given in Table 9.7.2 Roll Diameters:7.2.1 The outside diameters of rolls of film shall not varyfrom the value specified on the purchase order by more than6 6 mm (0.25 in.).7.2.2 The inside diameters of cores of standard rolls of filmshall not vary from the value specified on the purchas
28、e order bymore than 6 1.5 mm (0.060 in.).7.3 The widths of film in rolls shall be within the followingtolerances:7.3.1 Twenty-five mm (1 in.) wide or less, 6 0.4 mm (0.015in.).7.3.2 Over 25 to 100 mm (over 1 to 4 in.), 6 0.8 mm (0.030in.).7.3.3 Over 100 mm (4 in.), 6 1.6 mm (0.062 in.).7.4 The numbe
29、r of splices in standard rolls shall not exceedthe values given in Table 10 for Type I film or Table 11 andTable 12 for Type II films.7.5 The thicknesses shall be within the tolerances specifiedin Table 13 for Type I film or Table 3 for Type II film.7.6 The color of the sheet or strip shall be unifo
30、rm within agiven lot, as determined by visual examination.7.7 The film shall be uniform in appearance, as determinedby visual examination. The film shall be clean and free fromcontamination, wrinkles, holes, scratches, and other defectsthat might affect either appearance or serviceability. Theheat-s
31、ealable coating for Type II material shall be uniform inappearance.TABLE 4 Property Values for Type I, Class D Film (FEPFluorocarbon)Average Property ValueNominal Thickness, m (mils)13(0.50)25(1.0)51(2.0)76(3.0)102(4.0)127(5.0)254(10.0)356(14.0)508(20.0)762(30.0)1016(40.0)1524(60.0)2413(95.0)Tensile
32、 strength, min MPa (psi),machine direction and transversedirection13.8(2000)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)17.25(2500)Elongation, min, %, machinedirection and transversedirection175 250 250 250 250 250 250 250
33、250 250 250 250 250Shrinkage, max percent, afterexposure to 200 C (392 F)5.0 5.0 3.0 2.0 2.0 2.0 2.0 2.0 2.0 4.0 4.0 4.0 5.0Moisture absorption, max percent,100 %, RH0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1Dielectric strength, min at 60 HzkV/mm (V/mil)A,B160(4000)160(4000)140(3500)120(300
34、0)110(2750)100(2500)72(1800)64(1600)56(1400). . . .Volume resistivity, min, -cmB ,C1017101710171017101710171017101710171017101710171017Permittivity, max at 1 kHzB2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15 2.15Dissipation factor, max at 1 kHzB0.0003 0.0003 0.0003 0.0003 0.0003 0.0003
35、 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003 0.0003AUse Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shall be used for compliance.TABLE 5 Property Values for Type I, Class E Film (Polyethylene Ter
36、ephthalate)Average Property ValueNominal Thickness, m (mils)12 (0.48) 15 (0.60) 23 (0.92) 36 (1.42) 75 (3.00) 100 (4.00) 190 (7.50) 250 (10.00)19 (0.75) 50 (2.00) 125 (5.00) 225 (9.00) 250Tensile strength, min MPa (psi),machine direction and transversedirection145 (21 000) 145 (21 000) 138 (20 000)
37、138 (20 000) 138 (20 000) 138 (20 000) 138 (20 000) 110(16 000)Elongation, min % machinedirection and transverse direction60 60 65 70 70 70 70 70Shrinkage, max percent afterexposure to 150 C (302 F), 30 min3.5 3.0 3.0 3.0 3.0 3.0 3.0 2.0Moisture absorption, max %, 100 % RH 0.8 0.8 0.8 0.8 0.8 0.8 0.
38、8 0.8Dielectric strength, min at 60 Hz,kV/mm (V/mil)A,B208 (5300) 190 (4800) 174 (4400) 130 (3300) 105 (2700) 80 (2000) 60 (1500) 50 (1300)Volume resistivity, min, -cmB ,C10151015101510151015101510151015Permittivity, max at 1 kHzB3.5 3.5 3.5 3.5 3.5 3.5 3.5 3.5Dissipation factor, max at 1 kHzB0.006
39、0.006 0.006 0.006 0.006 0.006 0.006 0.006AUse Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shall be used for compliance.D5213 1238. Sampling8.1 Sample in accordance with Practice D3636, unlessot
40、herwise agreed upon between the supplier and the purchaser.8.2 For purposes of sampling, an inspection lot for exami-nation shall consist of all film of the same type, grade, class,and nominal thickness submitted for inspection at one time. Ifa single shipment contains film having different lot numb
41、ersassigned by the film manufacturer, sample each lot numberseparately.8.3 The total quantity of material to be taken from each lotshall be approximately twice that estimated to be required forthe tests that are to be made, in order to permit repeat testswithout resampling.8.4 These materials are no
42、rmally made in master rolls ofapproximately 360 kg (800 lb) in weight. Take samples forexamination and testing from the end of the master rolls.9. Number of Tests9.1 Unless otherwise agreed upon by the purchaser and theseller, routine lot inspection tests shall consist of evaluation ofall of the pro
43、perties specified in 7.4 7.7. For these properties,TABLE 6 Property Values for Type I, Class F Film (Polyethylene Naphthalate) Average Property ValueNominal Thickness, m (mils)12 (0.48) 16 (0.65) 25 (1.00) 38 (1.50) 50 (2.00) 75 (3.00) 100 (4.00) - 250 (10.00)Tensile strength, min MPa (psi),machine
44、direction and transversedirection172 (25 000) 172 (25 000) 172 (25 000) 172 (25 000) 172 (25 000) 172 (25 000) 172 (25 000)Elongation, min percent, machineand transverse direction50 50 50 50 50 50 50Shrinkage, max percent, afterexposure to 150 C (302 F), 30 min2.00 2.00 2.00 2.00 2.00 2.00 2.00Moist
45、ure absorption, max %,at 100 % RH0.6 0.6 0.6 0.6 0.6 0.6 0.6Dielectric strength, min at 60 Hz,kV/mm (V/mil)A,B215 (5500) 215 (5500) 195 (5000) 145 (3700) 145 (3700) 120 (3000) 120 (3000)Volume resistivity, min, -cmB ,Cohm-cm1015101510151015101510151015Permittivity, max at 1 kHzB3.4 3.4 3.4 3.4 3.4 3
46、.4 3.4Dissipation factor, max at 1 kHzB0.006 0.006 0.006 0.006 0.006 0.006 0.006AUse Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shall be used for compliance.TABLE 7 Property Values for Type 1,
47、 Class G Film (Polyetherimide)Average Property ValueNominal Thickness, m (mils)25 (1.00) 50 (2.00) 75 (3.00) 100 (4.00) 125 (5.00)Tensile Strength, min Mpa (psi), machine direction andtransverse direction93 (13500) 93 (13500) 93 (13500) 93 (13500) 93 (13500)Elongation, min percent, machine direction
48、 andtransverse direction100.00 100.00 100.00 100.00 100.00Shrinkage, max percent, after exposure to 200 C(392 F)0.60 0.60 0.50 0.40 0.40Moisture Absorption, max percent 100 % RH 1.20 1.20 1.20 1.20 1.20Dielectric strength, min kV/mm (V/mil)A,B284 (7100) 196 (4900) 148 (3700) 124 (3100) 108 (2400)Vol
49、ume Resistivity, min -cmB,C10171017101710171017Permittivity, max at 1kHzB3.40 3.40 3.40 3.40 3.40Dissipation Factor, max at 1kHzB0.0080 0.0080 0.0080 0.0080 0.0080AUse Type 3 electrodes in air of Table 1 of Test Method D149 (opposing 6.4-mm diameter rods).BAt 23 C (73.4 F), 50 % RH.CThe median value of 5 measurements shall be used for compliance.TABLE 8 Additional Property Values for Type II, Class A, B and CFilmsGradeTotal NominalThicknessm (mils)ADielectricStrength, minkV/mm(V/mil)Heat Seal Strength, min at35
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