ARMY A-A-59279-1998 SODIUM SULFATE ANHYDROUS TECHNICAL (FOR AMMUNITION USE) [Superseded ARMY MIL-S-50004 A CANC NOTICE 2 ARMY MIL-S-50004 A VALID NOTICE 1 ARMY MIL-S-50004 A ARMY M.pdf

1、 9018054 0001985 548 INCH- POUND A-A-59279 13 Julv 1998 SUPERSEDING MIL-S-50004A(AR) 24 June 1968 COMMERCIAL ITEM DESCRIPTION SODIUM SULFATE, ANHYDROUS, TECHNICAL (FOR AMMUNITION USE) The General Services Administration has authorized the use of this commercial item description, for all federal agen

2、cies. 1. SCOPE. This CID covers the general requirements for anhydrous sodium sulfate used for the manufacturing of propellants used in ammunition. 2. SALIENT CHARACTERISTICS. 2.1 Materials. The anhydrous sodium sulfate shall be in the form of a white powder when visually examined and shall be free

3、from lumps, caking, and visual impurities. specified in the contract or order (see 6.2). The anhydrous sodium sulfate shall be provided in the quantity 2.2 Loss on isnition. sulfate shall not exceed 0.5 pezcent when tested in accardance with American Chemical Society (ACS) publication, “Reagent Chem

4、icals“. would include the moisture content (H2O) and other volatiles or trace impurities. The moistu,re content (H20)of the anhydrous sodium Loss on ignition 2.3 Assay. pure when tested in accordance with American Chemical Society (ACS) Specifications, “Reagent Chemicals“. The anhydrous sodium sulfa

5、te shall not be less than 98.0 percent 2.4 Neutrality. The acidity shall be not more than 0.005 percent calculated as sulfuric acid, or the alkalinity shall be not more than 0.5 percent calculated as sodium carbonate when tested in accordance with paragraph 4.2. Beneficial comments (recommendations,

6、 additions, deletions) and any pertinent data which may be of use in improving this document should be addressed to: Commander, US Army TACOM-ARDEC, Attn.: AMSTA-AR-EDE-S, Bldg 12, Picatinny Arsenal, NJ 07806-5000 by using the Standardization Document Improvement Proposal (DD Form 1426) appearing at

7、 the end of this document or by letter. AMSC N/A FSC 6810 DISTRIBUTION STATEMENT A. Approved for public release; distribution is unlimited. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-9018054 000198b 484 A-A- 59279 2.5 Chlorides. when tested in a

8、ccordance with American Chemical Society (ACSI Specifications, “Reagent Chemicals II . The chloride content shall not exceed 0.7 percent by weight 2.6 Insoluble matter. The insoluble matter shall not exceed 0.1 percent by weight when tested in accordance with American Chemical Society (ACS) Specific

9、ations, “Reagent Chemicals“ . 3. REGULATORY REQUIREMENTS. The offeror/contractor is encouraged to use recovered materials to the maximum extent practicable, in accordance with paragraph 23.403 of the Federal Acquisition Regulation (FAR). 4. QUALITY ASSURANCE PROVISIONS. 4.1 Product Conformance. The

10、products provided shall meet the salient characteristics of this CID, conform to the producers own drawings, specifications, standards, and quality assurance practices, and be the same product offered for sale in the commercial market. The government reserves the right to require proof of such confo

11、rmance. 4.2 Neutralitv test. Dissolve a 10.00 gm. sample in 200 ml. of carbon dioxide free water and add methyl red indicator. If the solution is acid, titrate to a change in color with 0.01 N sodium hydroxide solution and calculate the acidity as follows (see 2.4): Percent sodium sulfuric acid = 4.

12、9 NV Where: N = normality of sodium hydroxide solution W V = volume of sodium hydroxide solution W = weight of sample, gm. If the solution is basic, titrate with 0.01 N hydrochloric acid and calculate the alkalinity as follows: ,. Percent sodium carbonate = 5.3 NV Where: N = normality of hydrochlori

13、c acid V = volume of hydrochloric acid W = weight of sample, gm. W 5. PACKAGING. Preservation, packing, and marking shall be as specified in the contract or order. 6. NOTES. 6.1 Source of documents. 6.1.1 The Code of Federal Regulations (CFR) is available by mail order from the Superintendent of Doc

14、uments, ATTN: New Order, P.O. Box 371954, Pittsburgh, PA 15250-7954. 6.1.2 ACS Specifications publication is available from American Chemical Society, Publications Support Services, 1155 Sixteenth Street, NW, Washington, DC 20036. Provided by IHSNot for ResaleNo reproduction or networking permitted

15、without license from IHS-,-,- = 9018054 0001987 310 A- A- 5 92 7 9 6.2 Orderins data. Procurement documents should specify the following: a. Title, number, and date of this CID. b. Quantity required (see 2.1). c. Packaging and marking requirements (see 5). 6.3 Material Safetv Data Sheets. CID may be

16、 subject to the requirements of 29 CFR 1910.1200 and FED-STD-313 for Material Safety Data Sheets (MSDS). Products meeting the requirements of this 6.4 TranSDOrtatiOn. Anhydrous sodium sulfate is subject to therequirements of 49 CFR 100-185 regarding the transportation of hazardous materials. 6.5 Keywords. Chemical Propellant MILITARY INTEREST: Custodian Army-AR Review Activities: ArV-AV, MD1 DLA- GS CIVIL AGENCY COORDINATING ACTIVITY: GSA- FSS Preparing Activity: Army-AR Pro j ect 6810- 16 07 3 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-