ARMY FED-STD-141 D-2001 PAINT VARNISH LACQUER AND RELATED MATERIALS METHODS OF INSPECTION SAMPLING AND TESTING《用于检查 取样和测试方法的油漆 清漆 亮漆及相关原料》.pdf

1、FED. TEST METHOD STD. 141DMarch 22, 2001SUPERSEDINGFED. TEST METHOD STD. 141CJanuary 24, 1986FEDERAL TEST METHOD STANDARDPAINT, VARNISH, LACQUER AND RELATED MATERIALS:METHODS OF INSPECTION, SAMPLING AND TESTINGThe General Services Administration has authorized the use of this federal standard, by al

2、l federal agencies.FSC 8010NOT MEASUREMENT SENSITIVEProvided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001FEDERAL TEST METHOD STANDARDPAINT, VARNISH, LACQUER AND RELATED MATERIALS:METHODS OF INSPECTION, SAMPLING AND

3、TESTINGAUTHORITY: This standard is issued pursuant to the Federal Property and AdministrationService Act of 1949, as amended, and its application to the purchase of commodities referred toherein is mandatory on all Federal agencies.SECTION 1SCOPE AND CONTENTS1. SCOPE1.1 Scope. This standard elaborat

4、es the methods used to determine the physical and chemicalproperties of paint, varnish, lacquer, and related materials. The purpose of this standard is to establishstandardized testing methodologies and to eliminate unnecessary or undesirable variations in testresults when evaluating a products adhe

5、rence to specification requirements. If any variation ormodification of the methods established in this standard is required by any specification, the procedureslisted in the specification will take precedence. Any conflict between this standard and any particularspecification will be resolved in fa

6、vor of the specification.2. CONTENTS2.1 Contents. The contents of this standard are arranged in sections as follows:Section1. Scope and Contents.2. Form and Numbering System.3. Alphabetical Index of Test Methods.4. Numerical Index of Test Methods.5. Numerical Index of Canceled Test Methods.6. Numeri

7、cal Index of ASTM methods to be used in place of canceled FTMS 141 Test Methods.7. Notes on the Use of this Standard.8. Reagents, Water, and Ethyl Alcohol.9. Routine and Referee Testing Conditions.1000. Sampling for Inspection and Testing.2000. Preparation of Panels and Application of Test Films.300

8、0. Package Stability Tests.4000. Physical Tests of Coating Materials and Coating Ingredients.6000. Physical and Chemical Tests of Dried Films.FSC 8010Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001iiSECTION 2F

9、ORM AND NUMBERING SYSTEM1. SCOPE1.1 Scope. This section contains a brief description of the form and the system of numberingwithin the individual methods, and also the manner in which new methods are added and oldmethods revised.2. FORM2.1 Revision of existing methods. The binding of this standard p

10、ermits separation forconvenience in adding new methods and revising existing methods.2.1.1 Numbering system used. When a technical change or modification is issued, one willidentify it by adding a decimal point to the basic method number or by incrementing the decimal.2.1.2 Revision precedence. When

11、 a revision is issued on a Standard 141 method, it automaticallysupersedes the previous method. Use the method of the particular revision in force at the time ofinvitation to bid for testing.2.2 New methods. A placement of new methods in this standard is based on the followingcriteria:a. The charact

12、er or purpose of the test method indicates the specific section to which itbelongs.b. A method number is assigned so that the new method is located close to methods of similaror related type.2.3 Use of ASTM test methods. American Society for Testing and Materials (ASTM) methodslisted in section 6 of

13、 this standard have been accepted as substitutes for the applicable canceledFederal test methods and should be used whenever the Fed. Test Method Std. 141 method numberis referenced. When superseded 141 methods are to be cited in the future, the accepted ASTMmethod should be cited directly.3. INDEXE

14、S AND METHOD FORMAT3.1 The indexes.3.1.1 Alphabetical index (section 3). In the alphabetical index, each current method is listedalphabetically by its primary purpose as indicated in its title.3.1.2 Numerical index (section 4). The numerical index lists all current methods in numericalorder.Provided

15、 by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001iii3.1.3 Numerical index of canceled test methods (section 5). An index of canceled, deleted, orsuperseded test methods is listed with cross-reference to the superseding

16、Fed. Test Method Std. 141or accepted ASTM test methods where applicable.3.1.4 Numerical index of accepted ASTM test methods (section 6). The ASTM test methodsaccepted are listed with cross-reference to canceled Fed. Test Method Std. 141 test methods.3.2 Test method format. Whenever possible, the tes

17、t methods contain the first five of thefollowing six paragraphs. Data on precision are included whenever available.3.2.1 Scope. The scope of each test method is given in paragraph 1. It describes the purpose ofthe test method.3.2.2 Apparatus. The apparatus for each test method is listed in paragraph

18、 2. Unusual apparatusis listed, along with standardization techniques and construction requirements, if applicable.3.2.3 Reagents. All reagents required in a test method are listed in paragraph 3. Details are givenfor the preparation of reagents that must be manufactured specifically for a particula

19、r test method.3.2.4 Procedure. The procedure to be followed in each test method is detailed in paragraph 4. Theprocedure generally includes three major sections, preparation of the test specimen, performance ofthe test involved, and calculation of results.3.2.5 Precision. Data on precision for each

20、test method, both within one laboratory and betweendifferent laboratories, are listed in paragraph 5.3.2.6 Notes. Any pertinent notes for each test method are listed in paragraph 6. These notes willinclude caution warnings, comments on variations in results, and similar comments.Provided by IHSNot f

21、or ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001ivSECTION 3ALPHABETICAL INDEX OF TEST METHODS_Title Method No._Adhesion (Wet) Tape Test 6301.3Application of Sprayed Films 2131.2Brushing Properties 4321.3Color Specification from Ph

22、otometric Tristimulus Data 4252.1Condition in Container 3011.3Contractor Inspection Responsibility 1031.1Drying Time 4061.3Infrared Reflectance from Reflectometer 6242.2Infrared Reflectance from Spectrophotometric Data 6241.2Knife Test 6304.2Nonvolatile Vehicle Content 4053.2Reducibility and Dilutio

23、n Stability 4203.2Spraying Properties 4331.2Storage Stability (Filled Container) 3022.2Transparent Liquids, Appearance of 4261.1_Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001vSECTION 4NUMERICAL INDEX OF TEST

24、 METHODS_Title Method No._Contractor Inspection Responsibility 1031.1Application of Sprayed Films 2131.2Condition in Container 3011.3Storage Stability (Filled Container) 3022.2Nonvolatile Vehicle Content 4053.2Drying Time 4061.3Reducibility and Dilution Stability 4203.2Color Specification from Photo

25、metric Tristimulus Data 4252.1Appearance of Transparent Liquids 4261.1Brushing Properties 4321.3Spraying Properties 4331.2Infrared Reflectance from Spectrophotometric Data 6241.2Infrared Reflectance from Reflectometer 6242.2Adhesion (Wet) Tape Test 6301.3Knife Test 6304.2_Provided by IHSNot for Resa

26、leNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001viSECTION 5NUMERICAL INDEX OF CANCELED TEST METHODS_Canceled Use UseTitle of Canceled FTMS 141 FTMS 141 ASTMTest Method Method No. Method No. Method No._Inspection (General) 1011Sampling Ge

27、neral 1021Sampling for Inspection and Testing 1022 D3925Preparation of Steel Panels 2011.2Preparation of Tin Panels 2012.2Preparation of Aluminum Panels 2013.1Preparation of Magnesium Alloy Panels 2015 D1732Preparation of Glass Panels 2021 D3891Preparation of Wood Panels 2031 D358Preparation of Fabr

28、ic Panels 2041Preparation of Concrete Panels 2051Preparation Gypsum Wallboard Panels 2081Preparation of Cast Films 2111Application by Roller 2112Application of Dipped Films 2121 D823, Practice BApplication of Brushed Films 2141.1Application of Flowed Films 2151Application of Film with Film Applicato

29、r 2161(Magnetic Chuck)Application of Film with Film Applicator 2162(Suction Panel Holder)Freeze-Thaw Resistance of Latex 3012 D2243and Emulsion PaintsPackage Stability of Latex Paints 3018 D1849Storage Stability at Thermal Extremes 3019.1Skinning (Partially Filled Container) 3021.1Ease of Reincorpor

30、ation 3027Pigment Content (Ordinary Centrifuge) 4021.1 D2371Pigment Content (Supercentrifuge) 4022 D2698Pigment Content of Cellulosic Lacquer 4023Nonvolatile Vehicle Isolation (Ordinary Centrifuge) 4031Vehicle Isolation (Supercentrifuge) 4032 D2698Volatile and Nonvolatile Content 4041.1 D2369(Ordina

31、ry Laboratory Oven)Volatile and Nonvolatile Content (Vacuum Oven) 4042.1 D2369Volatile (Moisture) Content of Celluloses 4043Nonvolatile Content of Dopes and Lacquers 4044Nonvolatile Matter in Solvents and Diluents 4045 D1353Volatile Matter in Hard Resins 4046Vehicle Solids (Ordinary Centrifuge) 4051

32、.1Vehicle Solids (Super Centrifuge) 4052Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001viiSECTION 5NUMERICAL INDEX OF CANCELED TEST METHODS_Canceled Use UseTitle of Canceled FTMS 141 FTMS 141 ASTMTest Method M

33、ethod No. Method No. Method No._Drying Time (Oil-Base Paints) 4062 4061.3Drying Time (Drying Oils and Resin Solutions) 4063 4061.3Moisture and Other Volatile Matter in Pigments 4071 D280Moisture and Other Volatile Matter in Pigments that 4072Decompose at 110CWater in Paints and Varnishes 4082.1 D136

34、4(Karl Fisher Titration Method)Water in Solvents and Thinners by Turbidity Method 4083 D1476Coarse Particles and Skins in Oil-Base Paints and Pastes 4091.1Coarse Particles and Skins in Synthetic Vehicles 4092.1 D185Coarse Particles in Dry Pigments (Ordinary Form) 4101 D185Coarse Particles in Dry Pig

35、ments (Pellet Form) 4102Wet Hiding Power of Paint (B/W Checkerboard) 4111Wet Hiding Power of Paints (Impervious Chart) 4112Drying Opacity 4121.1Hiding Power (Contrast Ratio) 4122.2 D2805Wet Opacity 4131Stability to Temperature Cycle 4144Kauri Reduction Test 4151 D1642Test Method BRosin-Pentaerythrit

36、ol Ester Reduction Test 4152 D1642Test Method AGas Test (Bell Jar) 4161Gas Test (Oven) 4162Draft Test 4171Specific Gravity of Pigments (Vacuum Method) 4181 D153Test Method A,Sections 4-9Specific Gravity of Pigment (Centrifuge Method) 4182Specific Gravity of Solvents and Thinners 4183 D891Weight per

37、Gallon 4184.1 D1475Specific Gravity of Solid Resins 4185Oil Absorption (Rub Out) 4191 D281Oil Absorption (Gardner-Coleman) 4192Miscibility Tests for Pastes-in-Oil 4201.1Mixing Properties of Aluminum Mixing Varnishes 4202Provided by IHSNot for ResaleNo reproduction or networking permitted without lic

38、ense from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001viiiSECTION 5NUMERICAL INDEX OF CANCELED TEST METHODS_Canceled Use UseTitle of Canceled FTMS 141 FTMS 141 ASTMTest Method Method No. Method No. Method No._Dilution Ratio (Lacquer Ingredients) 4204.1 D1720Bronzing Test of Cellulose 4205Compati

39、bility with Basic Pigment 4206Compatibility with Zinc Oxide 4207Evaluating Degree of Settling of Paint 4208 D869Miscibility and Compatibility 4209Mass Color of Pigments and Pastes-in-Oil 4220.1 D387Exclude Section 6Tinting Strength and Character of Tint of 4221 D387,Color Pigments Sections 2, 4, 6,

40、7Color Pigments (Dry) and Pastes-in-Oil Tinting 4222Strength of White PigmentsColor of Transparent Liquids 4241.1(Acid-Potassium Dichromate)Color of Transparent Liquids (Hellige Scale) 4242Color of Transparent Liquids (Platinum-Cobalt Scale) 4243.1 D1209Color of Transparent Liquids (Barrett Scale) 4

41、244Color of Transparent Liquids (Lovibond Scale) 4245Color of Transparent Liquids (Saybolt Scale) 4246 D156Color of Transparent Liquids 4247(Water-Potassium Dichromate)Color of Transparent Liquids (Gardner Color Std. 1953) 4248 D1544Color Differences of Opaque Materials 4249.1 D1729Visual Evaluation

42、Color of Pigmented Coatings 4250.1 D1729Color Specification from Spectrophotometric Data 4251Color Examination of Resins 4253Color of Lac Resin and Shellac by Comparison of Sols. 4254.1Color of Lac Resin and Shellac by Comparison of 4255 D29Dried FilmsAppearance of Pigmented Materials 4262 3011.3Vis

43、cosity of Transparent Liquids (Gardner Tubes) 4271 D1545Viscosity of Cellulose Derivatives by Ball Drop Method 4272.1 D1343Penetration (Needle) 4273 D5Penetration (Cone) 4273 D937Consistency of Pigmented Materials (Krebs-Stormer) 4281 D562Viscosity of Pigmented Materials (Ford Cup) 4282 D1200Provide

44、d by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. 141DMarch 22, 2001ixSECTION 5NUMERICAL INDEX OF CANCELED TEST METHODS_Canceled Use UseTitle of Canceled FTMS 141 FTMS 141 ASTMTest Method Method No. Method No. Method No._Consistency of Pigmented Materials 4283(Gardner Mobilometer)Viscosity of Pigmented Materials (ASTM Cups) 4284Viscosity (Saybolt Viscosimeter) 4285 D88Viscosity (Brookfield) 4287 D2196Test Method AFlash Point of Volatile Materials (Tag Closed Tester) 4291