ARMY MIL-C-10856 D-1966 CHEMICAL AGENT MUSTARD SIMULATED (MOLASSES RESIDUUM)《模拟芥末化学试剂(糖蜜沉淀)》.pdf

1、MIL-C-10856D 20 September 1966 SUPERSEDING MIL-M-10856C 29 December 1961 IILITARY SPECIFICATION C-CAL AGENT, MUSTARD, SIMILATED (MOLASSES RESIDUUM) This specification is mandatory for use by all De- partments ana Agencies of the Department of Defense. . 1, SCOPE 1.1 This specification c residuum) 2.

2、 APPLICABIaDoCITMENTs 2,l Government documents, The following documents of t effect on date of invitati pert OP this specification SPECIFICATIONS FEDDERAG . PPP-PA20 - P MILITARY srmm MILITARY a-s-129 - MIESTP.173 - Provided by IHSNot for ResaleNo reproduction or networking permitted without license

3、 from IHS-,-,-Unifom Freight Classification (AppljbcatPon for copies of these freight classification ratings rules an regulations should be addressed to Uniform Classification Committee, 202 Union Station, 516 West Jackson Boulevard, Chicago, Illinois 6606, ) At4EFiPCAN SOCIBTX FOR TESTING AND MA“ER

4、sAIs (ASTM) (AppL%ea%baPI for copies of the above pdblication should be cdcressed Lo Lhe American Society for Testing and Materials, 19.16 Race Street, h3hdeipha, Pennsylvania 19103. ) 3. REQUIREMEIJTS 3.1 Material. The molasses residuum shall be a concentrate of st91.1- age from fementat2on of mola

5、sses treated to prevent further fermentation. $he material shall not produce gas when tested as specified in 4.5.1 (see 6.4). 3.2 Chemical anil physical requirements. The molasses residuum shail conform to the physical and chemical requireiments of table I. .i Provided by IHSNot for ResaleNo reprodu

6、ction or networking permitted without license from IHS-,-,-flIL-C-1085bD 13 U 777770b 0273275 1 - _ - MIL-C-108 56D Table I. Chemical and physical requirements Property Density at 1.5.6 (min) Evaporation loss, percent Ash content, percent (max) Acidity calculated as sulfur dioxide, percent (mu) (-)

7、Requir ment 1.20 60 25 3.5 Test method 4.5.2 4.5.3 4.5.4 4.5.5 4. QUALITY ASCURANCE PROVISIONS 4.1 Responsibility for fnspection. Unless otherwise specified in- the contract or purchase order, the supplier is responsible for the perform- ance of all inspection requirements as specified herein. other

8、wise specified, the supplier may utilize his own or any other in- spection facilities and services acceptable to the Gaverment Government reserves the right to perform any of the inspectio forth in the specification where such inspections are de to insure that supplies and services conform to prescr

9、 4.1.1 Objective evidence. The supplier shall provide Except as dence acceptable to the contracting officer that the re and section 5 and for other requirements for which specific inspection procedures have not been given are satisfied. for acceptance at one time, which has been produced by one niar

10、rufacturer under essentially the same manufacturing in materials provided the operation is cont . the process is a batch operation, each batc (See 6.3.) . 4.2 Lotting. A lot shall consist of Che molasses residuum offered 4,3 Sampling. 4.3.1 For examination. Sempling shall be With MILSTD-105 - f Prov

11、ided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-C-1085bD 13 799790b 0293297 5 m I MTT.,P!, 4.5.3 Evaporation loss. Tare to Ehe nearest milligram (mg) a

12、flat- I bottom dish containing a short glass stirring rod and 6 to 7 Q of pure- reviously digested witn concentrated hydrochloric acid, washed, dried, ignited, cooled, and stored in a desiccator). approxwately 3.5000 g of specimen into the tared dich, stir into the at 105O 2 5OC for 8 to 10 hours. 5

13、OC for 1 hour, cool, and reweigh. Weigh Stir, reheat Ett 10SO + Repeat heating and weighing until- I oss in weight in 1 hour is no greater than 3 mg. Calculate the per- l where: A = weight of dish, rod, and sand, in grams, B = weight of specimen, in qrams, and C = weight of ish, rod, canti, and resi

14、due, in grams. I - 4.5.4 - Ash. and heat in a SO- or 100-ml platinum dish until ail water is expelld. a few drops of pure olive oil and heat slowly over a flame until swelling ceases. Treat the residue with approximately 5 ml of a 10-percent ammonium carbonate solution, orate and heat in the muffle

15、furnace at approximately 450% to constant Weigh, to the nearest mg, approximately 5 g of the sample Place the ich in a muffle furnace and heat at Epprox- Reevap- .I I 5OO0C unt5.l a white ash is obtained. B I where: A grams of residue, and 4.5.5 Acidity. Weigh, to the nearest mg, approximately 4 of

16、the , sample into a suitable container. and determine the acidity by titrating electrornetrically with 0.1N (so2) as follows: Dilute to about 2Q0 ml with water odium wroxide (fJaOH). Calculate the acidity as sulfur dioxide i.I where : N = normality of EaOh sclution, milliliters of HaOlI solution, an

17、d i+ = grams of specimen. I Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-5.?2 Marking. contract or order, all shipping containers shall be marked in accordance with MIL-STD-129. Containers should bear a caution label to show that this material con

18、tains cresol and should not be swallowed. In adition to any special marking required by the 6. 30TES 6.1 Intended use. Tie molasses residuum covered by this specification is intended for use in training as a simulant for mustard gas (H) . 6.2 Ordering data, Procurenient documents should specify the

19、title, number, and date of this specification. 6.3. Batch. A batch is efine as tnat quantity of material which has been subjected to some unit chemical or some physical nixing operation intended to make the final product sustantially unif orni. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-User interest : US. GOVERNMENT PRINTING QPFICE 117-251-520/0583 . Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-