ARMY MIL-PRF-3150 E-2008 LUBRICATING OIL PRESERVATIVE MEDIUM《防锈润滑油 中油》.pdf

1、Beneficial comments (recommendations, additions, deletions) and any pertinent data which may be of use in improving this document should be addressed to: U.S. Army Tank-automotive and Armaments Command, ATTN: AMSRD-TAR-E/268, MS-268, Warren, MI 48397-5000 by letter or emailed to dami_standardization

2、conus.army.mil. Since contact information can change, you may want to verify the currency of this address information using the ASSIST Online database at http:/assist.daps.dla.mil AMSC N/A FSC 9150 NOT MEASUREMENT SENSITIVE MIL-PRF-3150E 7 August 2008 SUPERSEDING MIL-PRF-3150D 6 February 1997 PERFOR

3、MANCE SPECIFICATION LUBRICATING OIL, PRESERVATIVE, MEDIUM This specification is approved for use by all Departments and Agencies of the Department of Defense. 1. SCOPE. 1.1 Scope. This specification covers one grade of preservative lubricating oil. 1.2 Identification. This lubricant is identified by

4、 Military Symbol PL-M and North Atlantic Treaty Organization (NATO) Code Number O-192 (see 6.9). 1.3 National stock numbers (NSNs). The following is a list of NSNs which correspond to the lubricating oil container sizes: Table I. NSN and corresponding minimum container size Size designation National

5、 Stock Number (NSN) Container size 01 9150-00-271-8427 4 ounces 02 9150-00-231-2361 1 quart 03 9150-00-231-2356 5 gallons 04 9150-00-231-2357 55 gallons Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-3150E 1.4 Part identifying number (PIN).

6、PINs to be used for procuring lubricating oil prescribed by this specification are created as follows: M3150 01- PL-M 2. APPLICABLE DOCUMENTS. PL-M is Military Symbol Dash number from Table I indicating container size “M” prefix and specification number 2.1 General. The documents listed in this sect

7、ion are specified in sections 3 and 4 of this specification. This section does not include documents cited in other sections of this specification or recommended for additional information or as examples. While every effort has been made to ensure the completeness of this list, document users are ca

8、utioned that they must meet all specified requirements in documents cited in sections 3 and 4 of this specification, whether or not they are listed. 2.2 Government documents. 2.2.1 Specifications, standards and handbooks. The following specifications, standards, and handbooks form a part of this doc

9、ument to the extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the solicitation or contract. FEDERAL STANDARDS FED-STD-791 - Testing Method of Lubricants, Liquid Fuels, and Related Products DEPARTMENT OF DEFENSE SPECIFICATIONS MIL-PRF-680 - Degreas

10、ing Solvent (Unless otherwise indicated, copies of these documents are available from the Standardization Document Order Desk, 700 Robbins Avenue, Building 4D, Philadelphia, PA 19111-5094, or online at http:/assist.daps.dla.mil/quicksearch/ ) 2.2.2 Other Government documents, drawings, and publicati

11、ons. The following other Government documents, drawings, and publications form a part of this document to the extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the solicitation or contract. 2 Provided by IHSNot for ResaleNo reproduction or networki

12、ng permitted without license from IHS-,-,-MIL-PRF-3150E CODE OF FEDERAL REGULATIONS (CFR) Title 29 Labor (Copies of this document is available from U.S. Government Printing Office, P.O.Box 979050, St. Louis, MO 63197-9000 or by calling (866) 512-1800, (if in DC area, call (202) 512-1800, or online a

13、t www.gpo.access.gov ). 2.3 Non-Government publications. The following documents form a part of this document to the extent specified herein. Unless otherwise specified, the issues of these documents are those cited in the solicitation or contract. AMERICAN CONFERENCE OF GOVERNMENTAL INDUSTRIAL HYGI

14、ENISTS (ACGIH) ACGIH Threshold Limit Values (TLV) and Biological Exposure Indices (BEI). (Copies of the above document may be ordered from American Conference of Governmental Industrial Hygienists, 1330 Kemper Meadow Drive, Cincinnati, Ohio 45240, 513-742-2020, or online at www.acgih.org.) ASTM INTE

15、RNATIONAL (ASTM), American Society for Testing and Materials ASTM B117 - Standard Practice for Operating Salt Spray (Fog) Apparatus ASTM D97 - Standard Test Method for Pour Point of Petroleum Products ASTM D130 - Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Stri

16、p Test ASTM D445 - Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and calculation of Dynamic Viscosity) ASTM D446 - Standard Specifications and Operating Instructions for Glass Capillary Kinematic Viscometers ASTM D972 - Standard Test Method for Evaporation Loss of L

17、ubricating Greases and Oils ASTM D1152 - Standard Specification for Methanol (Methyl Alcohol) ASTM D1748 - Standard Test Method for Rust Protection by Metal Preservatives in the Humidity Cabinet 3 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-P

18、RF-3150E (Copies of these documents may be obtained from the ASTM International, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, or ordered online at www.astm.org). 2.4 Order of precedence. In the event of a conflict between the text of this document and the references cited herein, the tex

19、t of this document takes precedence. Nothing in this document, however, supersedes applicable laws and regulations unless a specific exemption has been obtained. 3. REQUIREMENTS. 3.1 Qualification. Lubricants furnished under this specification shall be products that are authorized by the qualifying

20、activity for listing in the applicable qualified products database (QPD) before contract award (see 4.1.1 and 6.3). 3.1.1 Conformance inspection. When specified by the qualifying authority and/or the purchasing requisition, a sample of this oil shall be subjected to a qualification conformance inspe

21、ction (see 4.1.2 and TABLE III). Any change in the formulation of a qualified product shall necessitate its requalification. 3.2 Materials. The contractor shall formulate the oil that fully meets the support and ownership, interface, environmental, and operational requirements as specified herein (s

22、ee 3.3, 3.4, 3.5,and 3.6). 3.2.1 Recycled, recovered, or environmentally preferable materials. Recycled, recovered, or environmentally preferable materials should be used to the maximum extent possible, provided that the material meets or exceeds the operational and maintenance requirements, and pro

23、motes economically advantageous life cycle costs (see 4.2.1). 3.3 Support and ownership requirements. 3.3.1 Tolerances. The finished oil properties shall fall within permissible tolerances assigned by the qualifying activity to the product receiving qualification (see 4.3.1). 3.3.2 Toxicity. The lub

24、ricating oil shall have no adverse effects on human health when it is used as intended (see 4.3.3). 3.3.2.1 Toxicity warning label. Marking shall be in accordance with the requirements and specified herein. However, each unit, intermediate and exterior container, shall be marked in such a manner as

25、to warn against use in food-processing or food-handling equipment, on surfaces that may contact food, and contaminating foodstuffs (see 4.3.2.1). 3.3.3 Workmanship. The oil shall be uniform in appearance and free from suspended matter, grit, or other foreign matter when examined visually through a 4

26、0 lumen transmitted light (see 4.3.3). 4 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-3150E 3.4 Interface requirements. 3.4.1 Copper strip corrosion. The oil shall not tarnish the copper strip exceeding the value of 2a on the ASTM Copper S

27、trip Corrosion Standards incorporated in ASTM D130 Standard Test Method for Corrosiveness to Copper From Petroleum Products by Copper Strip Test (see 4.4.1). 3.4.2 Removability. When tested as specified in paragraph 4.4.2, the oil shall leave no visual evidence of oil residue, stain or discoloration

28、 on test panels after testing. 3.5 Environmental requirements. 3.5.1 Humidity protection. When tested as specified in paragragh 4.5.1, the oil shall provide protection against corrosion such that not more than three corrosion dots, of which, the lengths, widths, or diameters shall not be greater tha

29、n one millimeter shall be evident on the test panels after 30 days (720 hours) exposure in the humidity cabinet. The total of such corrosion dots on all three test panels shall not exceed three. Corrosion on the outer 6 mm of the panels shall not be cause for rejection (see 4.5.1). 3.5.2 Salt-spray

30、resistance. When tested as specified in paragragh 4.5.2, the oil, when applied to three test panels, shall provide salt-spray resistance so that not more than three corrosion dots, of which, the lengths, widths, or diameters are not greater than one millimeter after 48 hours exposure to a spray of 5

31、% salt solution or the oil fails to pass. The total of such corrosion dots on all three test panels shall not exceed nine or the oil fails to pass. Corrosion on the outer 6 mm of the panels shall not be cause for rejection (see 4.5.2). 3.5.3 Accelerated stability. When tested as specified in paragra

32、gh 4.5.3, the oil shall flow freely to its new level within 5 seconds and the viscosity shall not change more than 5% from the original viscosity (see 4.5.3 and TABLE IV). 3.5.4 Low temperature stability. When tested as specified in paragragh 4.5.4, the oil shall flow freely to its new level within

33、5 seconds and the viscosity shall not change more than 5% from the original viscosity (see 4.5.4 and TABLE V). 3.5.5 Storage stability. When tested as specified in paragragh 4.5.5, the oil shall meet all of the requirements specified in Table II, 3.3.3, 3.4.1, 3.4.2, 3.5.1, 3.5.2, 3.5.3, and 3.5.4 a

34、fter completion of the 6-month storage stability test (see 4.5.5 and TABLE VI). 3.6 Operating requirements. 3.6.1 Physical properties. The kinematic viscosity of the oil shall be as specified in Table II. 5 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS

35、-,-,-MIL-PRF-3150E TABLE II. Requirements PHYSICAL PROPERTIES METHOD VALUES Viscosity 40C, Kinematic, (mm2/s) ASTM D445 95 to 125 Pour Point, C, max. ASTM D97 -6 Evaporation loss at 100C, max. ASTM D972 5% 3.6.2 Pour point. The maximum pour point of the oil shall be no greater than 6C (see TABLE II

36、and 4.5.2). 3.6.3 Evaporation loss. The maximum mass percent evaporation loss of the oil shall not be greater than 5% (see TABLE II and 4.5.3). 4. VERIFICATION. 4.1 Classification of inspections. The inspection requirements as specified herein are classified as follows. a. Qualification inspection (

37、see 4.1.1). b. Conformance inspection (see 4.1.2). TABLE III. Requirements/verification cross-reference matrix Property Section 3 RequirementSection 4 Verification QualificationTesting Conformance Inspection Materials 3.2 4.2 Recycled, recovered, or environmentally preferable materials 3.2.1 4.2.1 T

38、olerances 3.3.1 4.3.1 X Toxicity 3.3.2 4.3.2 Toxicity warning label 3.3.2.1 4.3.2.1 X Workmanship 3.3.3 4.3.3 Copper strip corrosion 3.4.1 4.4.1 X X Removability 3.4.2 4.4.2 Humidity protection 3.5.1 4.5.1 X Salt-spray resistance 3.5.2 4.5.2 X Accelerated stability 3.5.3 4.5.3 X Low temperature stab

39、ility 3.5.4 4.5.4 X Storage stability 3.5.5 4.5.5 X Viscosity, kinetic 40C TABLE II 4.6.2 X X Pour point TABLE II 4.6.3 X X Evaporation loss TABLE II 4.6.4 X X 6 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-3150E 4.1.1 Qualification inspec

40、tion. Qualification inspection shall consist of tests for all of the requirements as specified in Table III and may be conducted in any plant or laboratory approved by the qualifying activity (see 6.3). 4.1.2 Conformance inspection. Conformance inspection shall consist of tests for all of the requir

41、ements as specified in Table III and may be conducted in any plant or laboratory approved by the qualifying activity. 4.2 Materials. To determine conformance to 3.2, the lubricating oil shall be examined and tested in accordance with sections 4.3, 4.4, 4.5, and 4.6. 4.2.1 Recycled, recovered, or env

42、ironmentally preferable materials. The Environmental Protection Agency (EPA) maintains an online list of toxic chemicals and hazardous substances at www.epa.gov/ebtpages/pollutants.html that shall be consulted to verify section 3.2.1. 4.3 Support and ownership verification. 4.3.1 Tolerances. Examine

43、 test data against assigned tolerances of the tests in Table II. If test values are outside the tolerance ranges, the material shall be rejected. 4.3.2 Toxicity. To determine conformance to 3.3.2, components of the oils formulation shall be compared with the toxic limits established by 29 CFR 1910.1

44、200 and ACGIH Threshold Limit Values (TLV) and Biological Exposure Indices (BEI). Oils with components exceeding the toxic limits shall be disqualified. Methods of quantitative determination shall be selected at the discretion of both the qualifying activity and the manufacture/blender. The EPA main

45、tains an online list of toxic chemicals and hazardous substances at www.epa.gov/ebtpages/pollutants.html and this list shall be used as guidance. 4.3.2.1 Toxicity warning label. Upon inspection container markings shall convey the following information: WARNING! Do not use this oil in food-processing

46、 or food-handling equipment on surfaces that may contact food. Do not allow the oil to contaminate foodstuffs. 4.3.3 Workmanship. Place the oil in a 4-oz. translucent container and shake the container and contents for ten seconds. Allow the contents to settle for thirty seconds. Then, examine the co

47、ntainer by holding it up to a 40 lumen transmitted light source. No residue shall be visible in the oil. 4.4 Interface verification. 4.4.1 Copper strip corrosion. To determine conformance to 3.4.1, the oil shall be tested in accordance with (IAW) ASTM D130 for 3 hours at 100C. The copper strips shal

48、l exhibit a value not more than 2a IAW the ASTM Copper Strip Corrosion Standards. 7 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-3150E 4.4.2 Removability. To determine conformance to 3.4.2, the oil shall be tested by completely immersing the three oil-coated test panels used for the humidity protection test (see 4.5.1) in a breaker containing degreasing solvent IAW MIL-PRF-680, Type II at 25C and agitating the solvent slightly for not more than one minute. Then, repeat this process with methanol IAW ASTM D1152. After removal from