ARMY MIL-PRF-46010 H-2013 LUBRICANT SOLID FILM HEAT CURED CORROSION INHIBITING NATO CODE - S-1738.pdf

1、 Comments, suggestions, or questions on this document should be addressed to U.S. Army RDECOM, Tank Automotive Research, Development and Engineering Center, ATTN: RDTA-EN/STND/TRANS MS #268, 6501 E. 11 Mile Road, Warren, MI 48397-5000 or emailed to usarmy.detroit.rdecom.mbx.tardec-standardizationmai

2、l.mil. Since contact information can change, you may want to verify the currency of this address information using the ASSIST Online database at https:/assist.dla.mil. AMSC N/A FSC 9150 DISTRIBUTION STATEMENT A. Approved for public release, distribution is unlimited. NOT MEASUREMENT SENSITIVE MIL-PR

3、F-46010H 13 November 2013 SUPERSEDING MIL-PRF-46010G 06 August 2008 PERFORMANCE SPECIFICATION LUBRICANT, SOLID FILM, HEAT CURED, CORROSION INHIBITING NATO CODE S-1738 This specification is approved for use by all Departments and Agencies of the Department of Defense. 1. SCOPE 1.1 Scope. This specifi

4、cation establishes the requirements for a corrosion inhibiting heat cured solid film lubricant that is intended to reduce wear and prevent galling, corrosion, and seizure of metals (see 6.1). For aerospace component applications see 6.9 Notes. 1.2 Classifications. This specification establishes the

5、following colors: Color 1: - Natural product color. Color 2: - Black color. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-46010H 2 1.3 Part or identifying number (PIN). The PIN to be used for lubricants acquired to this specification are cr

6、eated as follows: M - 46010 - X Color (see 1.2.3) 1 = Natural 2 = Black Specification number Prefix for military specification 2. APPLICABLE DOCUMENTS 2.1 General The documents listed in this section are specified in sections 3, 4, or 5 of this specification. This section does not include documents

7、cited in other sections of this specification or recommended for additional information or as examples. While every effort has been made to ensure the completeness of this list, document users are cautioned that they must meet all specified requirements of documents cited in sections 3, 4, or 5 of t

8、his specification, whether or not they are listed. 2.2 Government documents. 2.2.1 Specifications, standards, and handbooks. The following specifications, standards, and handbooks form a part of this document to the extent specified herein. Unless otherwise specified, the issues of these documents a

9、re those cited in the solicitation or contract (see 6.2). FEDERAL SPECIFICATIONS VV-D-1078 - Damping Fluid, Silicone Base (Dimethylpolysiloxane) FEDERAL STANDARDS FED-STD-595/36076 - Gray, Flat or Lusterless FED-STD-595/37038 - Miscellaneous, Flat or Lusterless FED-STD-791 - Testing Method of Lubric

10、ants, Liquid Fuels, and Related Products DEPARTMENT OF DEFENSE SPECIFICATIONS MIL-A-8625 - Anodic Coatings for Aluminum and Aluminum Alloys MIL-DTL-16232 - Phosphate Coatings, Heavy, Manganese or Zinc Base Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-

11、,-,-MIL-PRF-46010H 3 MIL-DTL-83133 - Turbine Fuel, Aviation, Kerosene Type, JP-8 (NATO F-34), NATO F-35, and JP-8+100 (NATO F-37) MIL-PRF-372 - Cleaning Compound, Solvent (For Bore of Small Arms and Automatic Aircraft Weapons) MIL-PRF-14107 - Lubricating Oil, Weapons, Low Temperature MIL-PRF-23699 -

12、 Lubricating Oil, Aircraft Turbine Engine, Synthetic Base, NATO Code Number O-156 MIL-PRF-46170 - Hydraulic Fluid, Rust Inhibited, Fire Resistant, Synthetic Hydrocarbon Base NATO Code Number H-544 MIL-PRF-63460 - Lubricant, Cleaner and Preservative for Weapons and Weapons Systems (Copies of the abov

13、e these documents are available online at http:/quicksearch.dla.mil or from the Standardization Document Order Desk, 700 Robbins Ave, Bldg 4D, Philadelphia, PA 19111-5094.) 2.3 Non-Government publications. The following documents form a part of this document to the extent specified herein. Unless ot

14、herwise specified, the issues of these documents are those cited in the solicitation or contract (see 6.2). ASTM INTERNATIONAL ASTM A108 - Standard Specification for Steel Bar, Carbon and Alloy, Cold-Finished (DoD Adopted) ASTM A167 - Standard Specification for Stainless and Heat-Resisting Chromium-

15、Nickel Steel Plate, Sheet, and Strip (DoD adopted) ASTM B117 - Standard Practice for Operating Salt Spray (Fog) Apparatus (DoD adopted) ASTM B209 - Specification for Aluminum and Aluminum-Alloy Sheet and Plate ASTM B244 - Standard Test Method for Measurement of Thickness of Anodic Coatings on Alumin

16、um and of Other Nonconductive Coatings on Nonmagnetic Basis Metals with Eddy-Current Instruments (DoD adopted) ASTM B499 - Standard Test Method for Measurement of Coating Thicknesses by the Magnetic Method: Nonmagnetic Coatings on Magnetic Basis Metals (DoD adopted) ASTM D1141 - Standard Practice fo

17、r the Preparation of Substitute Ocean Water (DoD adopted) ASTM D1193 - Standard Specification for Reagent Water (DoD adopted) ASTM D1732 - Standard Practices for Preparation of Magnesium Alloy Surfaces for Painting (DoD adopted) Provided by IHSNot for ResaleNo reproduction or networking permitted wi

18、thout license from IHS-,-,-MIL-PRF-46010H 4 ASTM D2510 - Standard Test Method for Adhesion of Solid Film Lubricants (DoD adopted) ASTM D2511 - Standard Test Method for Thermal Shock Sensitivity of Solid Film Lubricants (DoD adopted) ASTM D2625 - Standard Test Method for Endurance (Wear) Life and Loa

19、d-Carrying Capacity of Solid Film Lubricants (Falex Pin and Vee Method) (DoD adopted) ASTM D2649 - Standard Test Method for Corrosion Characteristics of Solid Film Lubricants (DoD adopted) ASTM D2832 - Standard Guide for Determining Volatile and Nonvolatile Content of Paint and Related Coatings ASTM

20、 D3960 - Standard Practice for Determining Volatile Organic Compound (VOC) Content of Paints and Related Coatings (DoD adopted) ASTM D4457 - Standard Test Method for Determination of Dichloromethane and 1,1,1-Trichloromethane in Paints and Coatings by Direct Injection into a Gas Chromatograph ASTM D

21、7091 - Standard Practice for Nondestructive Measurement of Dry Film Thickness of Nonmagnetic Coatings Applied to Ferrous Metals and Nonmagnetic, Nonconductive Coatings Applied to Non-Ferrous Metals (DoD Adopted) ASTM F22 - Standard Test Method for Hydrophobic Surface Films by the Water-Break Test (D

22、oD Adopted) (Copies of these documents are available from www.astm.org or ASTM International, P.O. Box C700, West Conshohocken, PA 19428-2959.) SAE INTERNATIONAL AMS1424 - Deicing/Anti-Icing Fluid, Aircraft SAE Type I (DoD Adopted) (Copies of these documents are available from www.sae.org or SAE Cus

23、tomer Service, 400 Commonwealth Drive, Warrendale, PA 15096-0001.) 2.4 Order of precedence. Unless otherwise noted herein or in the contract, in the event of a conflict between the text of this document and the references cited herein, the text of this document takes precedence. Nothing in this docu

24、ment, however, supersedes applicable laws and regulations unless a specific exemption has been obtained. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-46010H 5 3. REQUIREMENTS 3.1 Qualification. The lubricant furnished under this specificat

25、ion shall be products which are qualified for listing on the applicable qualified products list at the time set for award of bids (see 4.2 and 6.3). Any change in the formulation of a qualified product shall necessitate its requalification. 3.2 Materials. Component materials used in the manufacture

26、of this lubricant shall consist essentially of finely powdered lubricating solids dispersed in a suitable liquid binder. The lubricant shall be effective when applied by brushing, dipping, or spraying. The applied film shall meet all requirements both after being cured for 1 hour at 204 15C and afte

27、r being cured for 2 hours at 150 15C. The curing time shall be counted from the time the part reaches the cure temperature, not when the part is first subjected to heat. The lubricants shall contain no lead or lead-containing compounds, ozone depleting substances, graphite, powdered metals, carbon b

28、lack, charcoal or other forms of inorganic carbon (see 6.5 and 6.10). 3.3 Film appearance and thickness. The bonded solid film lubricant, when examined as specified in 4.5.1, shall appear uniform in color and shall be smooth, free from any cracks, scratches, pinholes, blisters, bubbles, runs, sags,

29、foreign matter, grit, rough particles, or separation of ingredients. The coating thickness shall be between 0.008 mm and 0.013 mm. All readings of the coating thickness shall be not less than 0.005 mm or greater than 0.018 mm. 3.4 Film adhesion. A bare metal surface shall not be exposed after liftin

30、g the tape when tested as specified in 4.5. A uniform deposit of powdery material clinging to the tape shall be considered acceptable. 3.5 Resistance to fluids. After immersion in each of the fluids as specified in Table I, no bare metal surface shall be exposed after removing the tape as specified

31、in 4.5. A uniform deposit of powdery material clinging to the tape shall not be considered a failure. Also, the bonded solid film lubricant shall not soften, lift, blister, crack, or peel after exposure to the fluids when tested as specified in section 4.5. 3.6 Thermal stability. When tested as spec

32、ified in 4.5, the solid film lubricant shall not flake, crack, or lift and shall conform to the requirements for film adhesion (see 3.4). 3.7 Endurance life. When tested in four trials in accordance with 4.5, the bonded solid film lubricant shall have an average endurance life at 1000 pounds load (l

33、bf) of 450 minutes. All individual tests shall be not less than 390 minutes. 3.8 Load carrying capacity. When tested in two trials in accordance with 4.5, the bonded solid film lubricant shall have a load capacity of 2500 lbf (11,120 N). All individual tests shall not be less than 2250 lbf (10,000 N

34、). Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-46010H 6 TABLE I. Test fluids. Test Fluid Specification Anti-Icing Fluid SAE AMS1424 Cleaning Compound, Solvent for Bore of Small Arms and Automatic Weapons MIL-PRF-372 Reagent Water ASTM D11

35、93, Type III Substitute Ocean Water ASTM D1141 Hydraulic Fluid, Rust Inhibited, Fire Resistant, Synthetic Hydrocarbon Base MIL-PRF-46170 Turbine Fuel, Aviation, Kerosene Types MIL-DTL-83133, JP-8 Lubricating Oil, Aircraft Turbine Engine, Synthetic Base MIL-PRF-23699 Lubricating Oil, Weapons, Low Tem

36、perature MIL-PRF-14107 Lubricant, Cleaner and Preservative for Weapons and Weapon Systems MIL-PRF-63460 Damping Fluid, Silicone Base (Dimethylpolysiloxane) VV-D-1078 3.9 Aluminum corrosion resistance. When subjected to heat and high humidity conditions as specified in 4.5 on anodized aluminum panels

37、, the bonded solid film lubricant shall not show or cause discoloration, pitting, formation of white deposits, or other evidence of corrosion. 3.10 Sulfurous acid - salt spray. When applied to steel panels and exposed to sulfurous acid - salt spray in accordance with 4.5, there shall be no resultant

38、 pitting, visible corrosion, or staining. 3.11 Salt - spray (fog) test. After being applied to steel panels, the lubricant shall show not more than three rust spots per panel. Any spots shall be not greater than 1.0 mm in diameter, after 100 hours exposure to a 5% salt spray solution in a salt fog c

39、abinet in accordance with 4.5. 3.12 Solids content. The lubricant shall contain not less than 40 percent by weight of solid material when tested in accordance with 4.5.2. 3.13 Storage stability. The fluid lubricant, after a minimum storage period as specified in 4.5.3, shall conform to the requireme

40、nts for endurance life, (see 3.7), the sulfurous acid - salt spray, (see 3.10) and the salt-spray (fog) test (see 3.11) when tested in accordance with 4.5. 3.14 Volatile Organic Content. The lubricant shall contain not more than 250 g/L of volatile organic content when tested as specified in 4.5. 3.

41、15 Toxicity. The lubricant shall have no adverse effects on human health when it is used as intended (see 6.1). Questions on toxicology shall be referred by the procuring activity to the appropriate departmental medical service after consulting the qualifying activity (see 6.3). Provided by IHSNot f

42、or ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-46010H 7 3.16 Color. The lubricant supplied in Color 2 shall closely match color No. 37038 of FED-STD-595, but shall be not lighter than color No. 36076 of FED-STD-595. 3.17 Workmanship. The bonded solid film shall

43、 appear uniform in color, smooth, free from cracks, scratches, blisters, foreign matter, grit, rough particles, bubbles, pin holes, runs, or sags. The lubricant film shall also show no evidence of separation of ingredient materials. 3.18 Recycled, recovered, or environmentally preferable materials.

44、Recycled, recovered or environmentally preferable materials should be used to the maximum extent possible provided that the material meets or exceeds the operational and maintenance requirements, and promotes economically advantageous life-cycle costs. 4. VERIFICATION 4.1 Classification of inspectio

45、ns. The inspections specified herein are classified as follows: a. Qualification inspection (see 4.2). b. Conformance inspection (see 4.3). 4.2 Qualification inspection. The qualification inspection shall consist of the tests in 3.3 through 3.14. 4.3 Conformance inspection. Conformance inspection sh

46、all consist of tests for the following requirements: a. Endurance Life (see 3.7) b. Corrosion Protection (salt-spray) (see 3.11) c. Total Solids (see 3.12) d. Film Adhesion (see 3.4) 4.4 Inspection conditions. 4.4.1 Atmospheric conditions. Unless otherwise specified, all examinations and tests shall

47、 be performed at a temperature of 25 3C and at a relative humidity between 30 and 70 percent. 4.4.2 Preparation of test panels. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-PRF-46010H 8 4.4.2.1 Preparation of and application to test panels for

48、 solid film lubricant (aluminum and corrosion resistant steel). The panels shall be made from: a. aluminum alloy conforming to ASTM B209/5, anodized to conform to MIL-A-8625, type II sulfuric acid anodize, measuring approximately 0.05 cm by 7.6 cm by 15.2 cm (the thickness of the anodize should be b

49、etween .005 and .013mm); and b. corrosion resistant steel conforming to ASTM A167, and measuring approximately 0.09 cm by 7.6 cm by 15.2 cm. The panels shall be pre-cleaned with aliphatic naphtha or any environmentally safe cleaner that sufficiently cleans surfaces to pass ASTM F22. This cleaner shall not cause damage to the surface being cleaned. The corrosion resistant steel