1、Designation: C1181 00 (Reapproved 2012)C1181/C1181M 17Standard Test Methods forCompressive Creep of Chemical-Resistant PolymerMachinery Grouts1This standard is issued under the fixed designation C1181;C1181/C1181M; the number immediately following the designation indicatesthe year of original adopti
2、on or, in the case of revision, the year of last revision. A number in parentheses indicates the year of lastreapproval. A superscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope Scope*1.1 These test methods cover a quantitative, comparative test for compr
3、essive creep of chemical-resistant grouting materialsunder a sustained load at a test temperature. Constant load is maintained using a bolt and spring washers. Measurements are madeat laboratory temperature after exposure periods at the selected test temperature.1.2 Test Method A outlines the moldin
4、g techniques for an unbonded test specimen. Test Method B covers the moldingtechniques for a bonded test specimen.1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values given inparentheses are mathematical conversions to SI units that are p
5、rovided for information only and are not considered stated in eachsystem may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from thetwo systems may result in non-conformance with the standard.1.4 This standard does not purport to address a
6、ll of the safety concerns, if any, associated with its use. It is the responsibilityof the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine theapplicability of regulatory limitations prior to use.1.5 This international standard was
7、 developed in accordance with internationally recognized principles on standardizationestablished in the Decision on Principles for the Development of International Standards, Guides and Recommendations issuedby the World Trade Organization Technical Barriers to Trade (TBT) Committee.2. Referenced D
8、ocuments2.1 ASTM Standards:2C904 Terminology Relating to Chemical-Resistant Nonmetallic Materials3. Terminology3.1 DefinitionsFor definitions of terms used in these test methods, see Terminology C904.4. Significance and Use4.1 These test methods provide a means of measuring the total compressive def
9、lection of chemical-resistant, machinery-groutmaterials under a sustained load at the test temperature. Test stress and temperature can be selected to simulate anticipated useconditions. For the purposes of these tests, creep is considered to be the compressive deflection in inches per inch, cm per
10、cminches per inch, which occurs after the initial loading of the specimen at laboratory temperature. The results do not necessarilycorrelate for different specimen thicknesses. No correlation has been established to actual-use conditions.5. Apparatus5.1 Steel Loading PlatesSteel plates, as described
11、, are used for loading the grout during the test. They may, also, be part ofthe mold used to cast the grout specimen.1 These test methods are under the jurisdiction of ASTM Committee C09 on Concrete and Concrete Aggregates and are the direct responsibility of Subcommittee C09.41on Hydraulic Cement G
12、routs.Current edition approved Aug. 1, 2012Dec. 15, 2017. Published September 2012January 2018. Originally approved in 1991. Last previous edition approved in 20052012as C1181 00 (2005).(2012). DOI: 10.1520/C1181-00R12.10.1520/C1181-17.2 For referencedASTM standards, visit theASTM website, www.astm.
13、org, or contactASTM Customer Service at serviceastm.org. For Annual Book of ASTM Standardsvolume information, refer to the standards Document Summary page on the ASTM website.This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what chan
14、ges have been made to the previous version. Becauseit may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versionof the standard as published by ASTM is to be considered the offic
15、ial document.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States15.1.1 Two steel plates are required for each test specimen. The plates shall be 411 to 13 cm 414 to 5 in. (1
16、1 to 13 cm) squareby 1 in. (25 mm)in. square by 25 mm 1 in. thick. A118-in. (30-mm)A30-mm 118-in. diameter hole shall be drilled in the centerof the plates. The edges of the plates and holes shall be deburred.5.1.2 One of the steel plates shall have four 14-in. (6-mm)6-mm 14-in. measuring holes (one
17、 in each corner) with the center13 mm 12 in. (13 mm)in. in from each edge.5.2 Bolt Assembly A 1-in. (24-mm)25-mm 1-in. diameter by 7.5 in. (19 cm)19 cm 7.5 in. long, high-strength steel bolt,and nut, flat washers, and spring washers are used to maintain the test load.5.3 Belleville Spring WashersFou
18、r washers are required for each test. These shall be high carbon steel with dimensions of 12.9by 5.7 cm 118 by 214 in. (5.7 by 6.0 cm) in. outside diameter by 0.159-in. (4.0-mm)4.0-mm 0.159-in. thickness, with 0.039-in.(1.0-mm)1.0-mm 0.039-in. dish. These washers will have an approximate spring rate
19、 of 153 000 lb/in. (27 300 kg/cm)27 300kg/cm 153 000 lb/in. and a rated load of 5793 lb (2630 kg)2630 kg 5793 lb when flattened.5.4 Grout Mold, suitable to cast the 4-in. (10-cm)10-cm 4-in. diameter by 2 5 cm 260.1 in. (5 cm) in. thick grout specimenwith a 12.9-cm 118-in.-in. diameter center hole as
20、 shown in Fig. 1. The faces must be parallel to within 0.030 in. (0.75 mm)0.75mm 0.030 in. over the 4-in. 10 cm 4-in. diameter specimen contact area (see 5.3). The mold may utilize the steel loading plates.5.4.1 For the bonded method, the plates are used as mold end plates.5.5 Compression Machine or
21、 Apparatus , capable of applying the test load to within 62.0 %.5.6 Depth Micrometer, readable to 0.0001 in. (2.5 )2.5 0.0001 in. with adjustable shaft length capable of readingapproximately 3-in. (7.6-cm)7.6-cm 3-in. depth.5.7 Indicating Caliper, readable to 0.001 in. (25 ).25 0.001 in.5.8 Constant
22、 Temperature Oven, capable of maintaining the desired temperature 64F (62C).62C 64F.5.9 Suitable Support Stand, capable of supporting the test assembly when placed under compressive load.6. Specimen Preparation6.1 Temperature Condition all grout components and molds at 7323 6 4F (232C 73 6 2C),4F, f
23、or at least 24 h priorto use.6.2 Test Method A, UnbondedTo prevent bonding, treat all surfaces of the mold with a suitable release agent, which willcontact the material during casting.6.3 Test Method B, Bonded:6.3.1 Prior to assembly, clean to remove foreign matter such as rust, dirt, or scale from
24、the grout contact surfaces of the twobase plates.6.3.2 To prevent bonding, treat all other surfaces of the mold which will contact the material during casting.6.4 Mix the grout according to manufacturers recommendations and pour, or otherwise place, through the fill hole in the mold.The grout may be
25、 consolidated with a rounded-end rod.7. Conditioning7.1 The specimen shall remain in the mold at least 16 h at 7323 6 4F (232C 73 6 2C).4F.7.2 Following the initial conditioning period, disassemble the mold (including the end plates if using Test Method A). Maintainthe specimens at 73 6 4F 23 6 2C 7
26、3 6 4F for a total of seven days, including the time in the mold.FIG. 1 Test SpecimenC1181/C1181M 1728. Test Procedure8.1 Specimen Measurement:8.1.1 Immediately following the conditioning period, measure the outside diameter of the test specimen to the nearest 0.001 in.(25 )25 0.001 in. using an ind
27、icating caliper. Make two measurements at right angles to one another at mid-height. Recordthe diameter as the average of the two measurements.8.1.2 Test Method A Using an indicating caliper, measure the thickness of the specimen in four places around thecircumference to the nearest 0.001 in. 25 0.0
28、01 in. Record the average of the measurements as the specimen thickness. Thevariation in the four measurements shall not exceed 0.060 in. (1.5 mm).1.5 mm 0.060 in.8.1.3 Test Method B Using an indicating caliper, measure the distance between the two plates at four places around thecircumference to th
29、e nearest 0.001 in. 25 0.001 in. Record the average of the measurements as the specimen thickness. Thevariation in the four measurements shall not exceed 0.060 in. (1.5 mm).1.5 mm 0.060 in.8.2 Assemble the testing apparatus as follows:8.2.1 Pass the bolt through the assembly consisting of a flat was
30、her, two nested spring washers, a second flat washer, two morenested spring washers, a third flat washer, the bottom plate, the grout specimen, the top plate, a fourth flat washer, and a nut.8.3 Calculate the load required to produce the test stress on the specimen using the following formula:L5SS p
31、iD24 2ABD (1)where:L = total force required on a specimen, lb (n),S = desired stress, psi (MPa),D = diameter of the grout cylinder, in. (mm), andAB = area of the formed bolt hole (may be taken as 1 in.2(640 mm2).L = total force required on a specimen, N lb,S = desired stress, MPa psi,D = diameter of
32、 the grout cylinder, mm in., andAB = area of the formed bolt hole (may be taken as 640 mm21 in.2).8.4 Place the assembly on the support stand in the compression machine or apparatus such that the load is applied directly tothe bolt head and the opposite plate, leaving the nut accessible for tighteni
33、ng (see Fig. 2).8.4.1 Apply and maintain the test load.8.4.2 Tighten the nut hand-tight.8.4.3 Release the load and remove the test fixture from the compression machine.8.5 Immediately after removing the test apparatus from the compression machine, measure the distance between the top facesof the pla
34、tes. Make the measurements to 0.0001 in. 2.5 0.0001 in. through the four corner holes, using the depth micrometer.Record the individual readings and the average of all four.8.6 Place the specimen in the controlled temperature oven at selected temperature for the designated exposure period, thenremov
35、e and allow to cool at 732364F (232C 7362C)4F for at least 24 h. Reload the specimen as in 8.4; take new readingsto 0.0001 in. 2.5 0.0001 in. and record, and then place specimen in the oven for the next exposure period.8.7 Total exposure periods are shown in Table 1.8.8 Suggested schedule for a five
36、-day work week is presented in Table 2.9. Report9.1 Report the following information:9.1.1 Manufacturers product trade name or designation of the material, or both, and type and batch, or lot number, if available,9.1.2 Conditioning procedure including temperature and time,9.1.3 Test temperature,9.1.
37、4 Load and stress applied to the grout specimen,9.1.5 Individual data including the initial micrometer readings along with all the individual exposed readings and averages withtime and date of readings, and9.1.6 A graph showing the total creep in in./in. cm/cm in./in. as a function of time in the ov
38、en.C1181/C1181M 173FIG. 2 Typical Arrangement to Apply the Compression Load and Hand Tighten the NutC1181/C1181M 17410. Precision and Bias10.1 Precision and bias have not been established for these test methods. It is suggested that duplicate tests be run to verifyreproducibility of test results.11.
39、 Keywords11.1 chemical-resistant; compressive creep; compressive deflection; creep; polymer machinery grouts; stressSUMMARY OF CHANGESCommittee C09 has identified the location of selected changes to this standard since the last issue(C118100(2012) that may impact the use of this standard. (Approved
40、Dec. 15, 2017.)(1) Converted to a combined SI/inch pound standard.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any s
41、uch patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn.Your comments are invit
42、ed either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a
43、 fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this
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45、ive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 Total Exposure PeriodsTotal OvenExposure Cycle No.Cooling, minTime inOvenTime at7323 4F2C73 4F24 2 h 1 24 h 24 h48 4 h 2 24 h 24 h120 6 h 3 72 h 24 h7 d 6 h 4 48 h 24 h14 d 6 h 5 7 days 24 h28 d 12 h 6 14 days 24 hTABLE 2 Suggested Schedule, Five
46、-day Work WeekCycle Place inOven Remove fromOven Measure andReload1 Monday (1)A Tuesday (2) Wednesday (3)2 Wednesday (3) Thursday (4) Friday (5)3 Friday (5) Monday (8) Tuesday (9)4 Tuesday (9) Thursday (11) Friday (12)5 Friday (12) Friday (19) Monday (22)6 Monday (22) Monday (36) Tuesday (37)A Denotes calendar days from start of the test.C1181/C1181M 175
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