ASTM C1482-2010 Standard Specification for Polyimide Flexible Cellular Thermal and Sound Absorbing Insulation《聚酰亚胺柔性多孔隔热和吸声材料标准规范》.pdf

1、Designation: C1482 10Standard Specification forPolyimide Flexible Cellular Thermal and Sound AbsorbingInsulation1This standard is issued under the fixed designation C1482; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of

2、 last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers the composition and physicalproperties of lightweight, flexible open-cell polyimide foamins

3、ulation intended for use as thermal and sound-absorbinginsulation for temperatures from -328F up to +572F (-200Cand +300C) in commercial and industrial environments.1.1.1 Annex A1 includes faced polyimide foam as specifiedby the U.S. Navy for marine applications.1.1.2 This standard is designed as a

4、material specificationand not a design document. Physical property requirementsvary by application and temperature. No single test is adequatefor estimating either the minimum or maximum use tempera-ture of polyimide foam under all possible conditions. Consultthe manufacturer for specific recommenda

5、tions and physicalproperties for specific applications.1.1.3 The use of an appropriate vapor retarder is required inall applications where condensation could occur and cause adecrease in thermal performance or affect other system prop-erties.1.2 The values stated in inch-pound units are to be regard

6、edas standard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.3 This standard is used to measure and describe theresponse of materials, products, or assemblies to heat and flameunder controlled condition

7、s, but does not by itself incorporateall factors required for fire-hazard or fire-risk assessment of thematerials, products, or assemblies under actual fire conditions.1.4 This standard does not purport to address all of thesafety concerns associated with its use. It is the responsibilityof the user

8、 to establish appropriate safety and health practicesand determine the applicability of regulatory requirementsprior to use.NOTE 1The subject matter of this material specification is not coveredby any other ASTM specification. There is no known ISO standardcovering the subject of this standard.2. Re

9、ferenced Documents2.1 ASTM Standards:2C165 Test Method for Measuring Compressive Propertiesof Thermal InsulationsC168 Terminology Relating to Thermal InsulationC177 Test Method for Steady-State Heat Flux Measure-ments and Thermal Transmission Properties by Means ofthe Guarded-Hot-Plate ApparatusC302

10、 Test Method for Density and Dimensions of Pre-formed Pipe-Covering-Type Thermal InsulationC335 Test Method for Steady-State Heat Transfer Proper-ties of Pipe InsulationC390 Practice for Sampling and Acceptance of ThermalInsulation LotsC411 Test Method for Hot-Surface Performance of High-Temperature

11、 Thermal InsulationC421 Test Method for Tumbling Friability of PreformedBlock-Type and Preformed Pipe-Covering-Type ThermalInsulationC423 Test Method for Sound Absorption and Sound Ab-sorption Coefficients by the Reverberation Room MethodC447 Practice for Estimating the Maximum Use Tempera-ture of T

12、hermal InsulationsC518 Test Method for Steady-State Thermal TransmissionProperties by Means of the Heat Flow Meter ApparatusC634 Terminology Relating to Building and EnvironmentalAcousticsC665 Specification for Mineral-Fiber Blanket Thermal In-sulation for Light Frame Construction and ManufacturedHo

13、usingC1045 Practice for Calculating Thermal Transmission Prop-erties Under Steady-State ConditionsC1058 Practice for Selecting Temperatures for Evaluatingand Reporting Thermal Properties of Thermal InsulationC1114 Test Method for Steady-State Thermal TransmissionProperties by Means of the Thin-Heate

14、r ApparatusC1304 Test Method for Assessing the Odor Emission ofThermal Insulation Materials1This specification is under the jurisdiction of ASTM Committee C16 onThermal Insulation and is the direct responsibility of Subcommittee C16.22 onOrganic and Nonhomogeneous Inorganic Thermal Insulations.Curre

15、nt edition approved Sept. 1, 2010. Published October 2010. Originallyapproved in 2000. Last previous edition approved in 2009 as C1482 10 DOI:10.1520/C1482-10.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of

16、ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.C1338 Test Method for Determining Fungi Resistance ofInsulation Materials and FacingsC1

17、559 Test Method for Determining Wicking of FibrousGlass Blanket Insulation (Aircraft Type)D395 Test Methods for Rubber PropertyCompression SetD543 Practices for Evaluating the Resistance of Plastics toChemical ReagentsD638 Test Method for Tensile Properties of PlasticsD2126 Test Method for Response

18、of Rigid Cellular Plasticsto Thermal and Humid AgingD3574 Test Methods for Flexible Cellular MaterialsSlab,Bonded, and Molded Urethane FoamsD3675 Test Method for Surface Flammability of FlexibleCellular Materials Using a Radiant Heat Energy SourceE84 Test Method for Surface Burning Characteristics o

19、fBuilding MaterialsE96/E96M Test Methods for Water Vapor Transmission ofMaterialsE176 Terminology of Fire StandardsE662 Test Method for Specific Optical Density of SmokeGenerated by Solid MaterialsE795 Practices for Mounting Test Specimens During SoundAbsorption TestsE800 Guide for Measurement of Ga

20、ses Present or Gener-ated During FiresE1354 Test Method for Heat and Visible Smoke ReleaseRates for Materials and Products Using an Oxygen Con-sumption CalorimeterE2231 Practice for Specimen Preparation and Mounting ofPipe and Duct Insulation Materials to Assess SurfaceBurning Characteristics2.2 U.S

21、. Federal Standards:FAR 25.853(a), Appendix F, Part 1, (a) (1) (i) Test Criteriaand Procedures for Showing Compliance with Sec.25.853, or 25.8553FAR 25.856(a), Appendix F, Part VI, Test Method toDetermine the Flammability and Flame Propagation Char-acteristics of Thermal/Acoustic Insulation Material

22、sMIL-C-20079 Cloth, Glass; Tape, Textile Glass; andThread, Glass4MIL-A-3316 Adhesive, Fire-Resistant, Thermal Insulation4DOD-E-24607 Enamel, Interior, Nonflaming (Dry), Chlori-nated Alkyd Resin, Semigloss (Metric)42.3 Private Sector Standards:Boeing BSS 7239 Test Method for Toxic Gas Generation byMa

23、terials on Combustion5TAPPI T 803 Puncture and Stiffness Test of ContainerBoard6TM-232 Vertical Pipe-Chase Test to Determine Flame-Propagation Characteristics of Pipe Covering73. Terminology3.1 DefinitionsTerms used in this specification are definedin Terminology C168, Terminology C634, and Terminol

24、ogyE176. In the case of a conflict, Terminology C168 shall be thedominant authority.3.2 Definitions of Terms Specific to This Standard:3.2.1 flexible cellular producta cellular organic polymericmaterial that will not rupture when a specimen 8 by 1 by 1 in.(200 by 25 by 25 mm) is bent around a 1 in.

25、(25 mm) diametermandrel at a uniform rate of one lap in 5 sec. at a temperaturebetween 64 and 85F (18 and 29C), in accordance with thedescription of a flexible cellular product (currently Subsection3.1.3) in Test Methods D3574.3.2.2 slaba rectangular section, piece, or sheet of foamthat is cut from

26、a bun, or block of foam.3.2.3 polyimide foama flexible cellular product in whichthe bonds formed between monomers during polymerizationare imide or amide bonds. The theoretical mole fraction ofimide bonds must be greater than the theoretical mole fractionof amide bonds.4. Classification4.1 The flexi

27、ble polyimide cellular insulations of this speci-fication are classified into Types I through VI as listed in Tables1 and 2 (Note 2). Type I is further subdivided into two gradesbased on maximum allowable thermal conductivity at 75 F(24 C). The Types II and III are subdivided into classes (Note3).NO

28、TE 2Although all types find application in a wide variety ofmarkets, the current primary market for each type is as follows:Type Imarine and industrial applications.Type IIType II is Type I foam faced and used in specific marineapplications, as specified for the U.S. Navy in Annex A1.Type IIIType II

29、I is Type I foam pipe shaped and used in specificmarine applications, as specified for the U.S. Navy in Annex A1.Types IV and Vaerospace applications depending on density.Type VIapplications requiring improved high temperature and fireperformance.NOTE 3The Type II and Type III designations as well a

30、s thesubdivision of Types into Classes is to maintain uniformity with existingU.S. Navy nomenclature (Annex A1).5. Materials and Manufacture5.1 Polyimide foam shall be manufactured from the appro-priate monomers, and necessary compounding ingredients toconform to 3.2.3. This is not intended to imply

31、 that foamproducts made using different materials are equivalent withrespect to all physical properties.6. Physical Properties6.1 The insulation shall conform to the requirements inTables 1 and 2 for each type, unless specifically stated3Federal Aviation Regulations Part 25 (Airworthiness Standards,

32、 TransportCategory Aircraft, and Section 25.853. Procedure in appendix F, Part I, (a) (1) (i)and (ii). Available from Superintendent of Documents, U.S. Government PrintingOffice P.O. Box 371954, Pittsburgh, PA 15250-7954.4Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,Section D

33、, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:/www.dodssp.daps.mil.5Available from Boeing Commercial Airplane Group, Material Division, P.O.Box 3707, Seattle, WA 98124-2207.6Available from Technical Association of the Pulp and Paper Industry (TAPPI),15 Technology Parkway South, Norcross, GA

34、30092, http:/www.tappi.org.7Available from Armstrong World Industries, Inc., Research and Development,P.O. Box 3511, Lancaster, PA 17604.C1482 102otherwise by agreement between the supplier and the pur-chaser. Tests shall be made in accordance with the methodsspecified in 11.1-11.20.6.1.1 Upper Temp

35、erature LimitUpper temperature limitshall be determined according to 11.4 at the intended maximumuse temperature of the application, or at a temperature deter-mined by agreement between the purchaser and manufacturer.6.1.2 Burning CharacteristicsThe uncoated and unfacedfoam shall conform to the requ

36、irements in Tables 1 and 2 foreach type, when tested in accordance with 11.12-11.20, withoutthe use of flame/smoke or heat suppressant barriers or coatings.6.1.3 Sound Absorbing PerformanceUnless specificallyotherwise agreed to between the supplier and the purchaser, alltests shall be made in accord

37、ance with the methods specified in11.19.TABLE 1 Polyimide Foam Classification (inch-pound)TYPE IGrade 1TYPE IGrade 2TYPE IV TYPE V TYPE VIDensity, max, lb/ft30.48 0.48 0.37 0.55 0.50Maximum Apparent Thermal Conductivity Btu-in./h ft2F238 F 0.14 0.14 0.14 0.14 0.1458 F 0.23 0.22 0.23 0.23 0.2375 F 0.

38、32 0.29 0.34 0.30 0.34212 F 0.51 0.47 0.54 0.47 0.50356 F 0.74 0.70 0.81 0.70 0.74572 F NAANAANAANAA1.15Upper Temperature Limit test temperature for C411, F 400 400 400 400 572High Temperature Stability%ofinitial tensile strength retained after 336 hoursin air oven at 400 F, min, %60 60 NAANAANAAHig

39、h Temperature Stability%ofinitial tensile strength retained after 336 hoursin air oven at 572 F, min, %NAANAANAANAA70Tensile Strength, min, lb/in.28.5 8.5 2.8 8.5 3.9Compressive Strength, min, lb/in.2at 25% deflection 0.5 0.5 NAANAA0.550% Compression Deflection, min, lb/in21.2 1.2 NAANAANAACompressi

40、on Set, max, % NAANAA40 40 NAASteam AgingChange in Tensile Strength, max, %Dimensional and weight changes, max, %25102510NAANAANAANAA2510Corrosiveness pass pass pass pass passChemical Resistance pass pass pass pass passSurface Burning Characteristics, 2 in. thicknessFlame Spread Index, maxSmoke Deve

41、lopment, Index, max10151015152015201015Radiant Panel Surface Flammability, Flame Spread Index, max 55552Vertical BurnBBurn Length, max, in. NAANAA22.4NAAAfter Flame Time, max, sec NAANAA11ATotal heat release (2 min), max, Btu/ft279 79 NAANAANAAMaximum heat release rate, max, Btu/min-ft2106 106 NAANA

42、ANAASpecific Optical Smoke Density, Dm, maxnon-flaming modeflaming mode51051051051055Total Hydrogen Halide (HCl, HBr, and HF) Gases in Smoke, Flaming Exposure,max, ppm (Above background for empty chamber)10 10 10 10 10Toxic Gas Generation: max, ppmCO 300 300 300 300 300HCN 55555HFHCl 10 10 10 10 10H

43、Br 55555SO2NOx 10 10 10 10 10Acoustical Absorption Coefficient 2 in. thickness, min Noise ReductionCoefficient (NRC)0.75 0.70 0.75 0.85 0.70Tumbling Friability600 Revolutions, mass loss, Max % 3.0 3.0 NAANAA3.01200 Revolutions, mass loss Max, % 5.0 5.0 NAANAA5.0Odor Emission Pass Pass Pass Pass Pass

44、Fungi Resistance Pass Pass Pass Pass PassWicking, 48h, distance above water line,max at 72F, in.0.5 0.5 NAANAA0.5ANA = not applicableBThe material shall not melt, drip, or flow when tested as required.C1482 1036.2 The values stated in Tables 1 and 2 are not to be used asdesign values. It is the resp

45、onsibility of the buyer to specifydesign requirements and obtain supporting documentationfrom the material supplier.7. Workmanship and Appearance7.1 The slab offered as saleable material shall be free offoreign materials and defects that will adversely affect itsperformance in service.7.2 Voids and

46、Surface DamageIt is acceptable to repairsurface damage due to handling, and voids that are between0.24 in. (6mm) and 1.4 in. (35mm) in diameter, and extendthrough the entire slab, by gluing, plugging, or cutting andsplicing. Voids greater than 1.4 in. (35mm) in diameter shall because for rejection o

47、f the affected material. It is acceptable toachieve plugging using compression fit or by using adhesives.Adhesives used for repair shall not affect the overall smoke,fire, or acoustic performance required for the material in thisTABLE 2 Polyimide Foam Classification (SI units)TYPE IGrade 1TYPE IGrad

48、e 2TYPE IV TYPE V TYPE VIDensity, max, kg/m37.7 7.7 5.9 8.8 8.0Maximum Apparent Thermal Conductivity W/m-K150 C 0.020 0.020 0.020 0.020 0.02050 C 0.033 0.032 0.033 0.033 0.03324 C 0.046 0.042 0.049 0.043 0.049100 C 0.074 0.068 0.078 0.068 0.072180 C 0.107 0.101 0.117 0.101 0.107300 C NAANAANAANAA0.1

49、66Upper Temperature Limit test temperature for C411, C 204 204 204 204 300High Temperature Stability%ofinitial tensile strength retained after 336 hoursin air oven at 204 C, min, %60 60 NAANAANAAHigh Temperature Stability%ofinitial tensile strength retained after 336 hoursin air oven at 300 C, min, %NAANAANAANAA70Tensile Strength, kPa 60 60 18 60 27Compressive Strength, min, kPa at 25% deflection 3.4 3.4 NAANAA3.450% Compression Deflection, min, kPa 8 8 NAANAANAACompression Set, max, % NAANAA40 40 NAASteam Aging,Change i