ASTM C150 C150M-2016e1 Standard Specification for Portland Cement《硅酸盐水泥的标准规格》.pdf

1、Designation: C150/C150M 161Standard Specification forPortland Cement1This standard is issued under the fixed designation C150/C150M; the number immediately following the designation indicates the yearof original adoption or, in the case of revision, the year of last revision. A number in parentheses

2、 indicates the year of last reapproval.A superscript epsilon () indicates an editorial change since the last revision or reapproval.1NOTERevised editorially to remove an erroneous reference in 9.1.7 in July 2016.1. Scope*1.1 This specification covers ten types of portland cement,as follows (see Note

3、 2):1.1.1 Type IFor use when the special properties specifiedfor any other type are not required.1.1.2 Type IAAir-entraining cement for the same uses asType I, where air-entrainment is desired.1.1.3 Type IIFor general use, more especially when mod-erate sulfate resistance is desired.1.1.4 Type IIAAi

4、r-entraining cement for the same uses asType II, where air-entrainment is desired.1.1.5 Type II(MH)For general use, more especially whenmoderate heat of hydration and moderate sulfate resistance aredesired.1.1.6 Type II(MH)AAir-entraining cement for the sameuses as Type II(MH), where air-entrainment

5、 is desired.1.1.7 Type IIIFor use when high early strength is desired.1.1.8 Type IIIAAir-entraining cement for the same use asType III, where air-entrainment is desired.1.1.9 Type IVFor use when a low heat of hydration isdesired.1.1.10 Type VFor use when high sulfate resistance isdesired.NOTE 1Some

6、cements are designated with a combined typeclassification, such as Type I/II, indicating that the cement meets therequirements of the indicated types and is being offered as suitable for usewhen either type is desired.NOTE 2Cement conforming to the requirements for all types are notcarried in stock

7、in some areas. In advance of specifying the use of cementother than Type I, determine whether the proposed type of cement is, orcan be made, available.1.2 The values stated in either SI units or inch-pound unitsare to be regarded separately as standard. The values stated ineach system may not be exa

8、ct equivalents; therefore, eachsystem shall be used independently of the other. Combiningvalues from the two systems may result in non-conformancewith the standard. Values in SI units or inch-pound units shallbe obtained by measurement in SI units or inch-pound unitsor by appropriate conversion, usi

9、ng the Rules for Conversionand Rounding given in IEEE/ASTM SI 10, of measurementsmade in other units or SI units. Values are stated in only SIunits when inch-pound units are not used in practice.1.3 The text of this standard references notes and footnoteswhich provide explanatory material. These not

10、es and footnotes(excluding those in tables and figures) shall not be consideredas requirements of the standard.2. Referenced Documents2.1 ASTM Standards:2C33 Specification for Concrete AggregatesC51 Terminology Relating to Lime and Limestone (as usedby the Industry)C109/C109M Test Method for Compres

11、sive Strength ofHydraulic Cement Mortars (Using 2-in. or 50-mm CubeSpecimens)C114 Test Methods for Chemical Analysis of HydraulicCementC115 Test Method for Fineness of Portland Cement by theTurbidimeterC151 Test Method for Autoclave Expansion of HydraulicCementC183 Practice for Sampling and the Amou

12、nt of Testing ofHydraulic CementC185 Test Method for Air Content of Hydraulic CementMortarC186 Test Method for Heat of Hydration of HydraulicCementC191 Test Methods for Time of Setting of Hydraulic Cementby Vicat NeedleC204 Test Methods for Fineness of Hydraulic Cement byAir-Permeability ApparatusC2

13、19 Terminology Relating to Hydraulic CementC226 Specification for Air-Entraining Additions for Use inthe Manufacture of Air-Entraining Hydraulic Cement1This specification is under the jurisdiction of ASTM Committee C01 onCement and is the direct responsibility of Subcommittee C01.10 on HydraulicCeme

14、nts for General Concrete Construction.Current edition approved March 15, 2016. Published April 2016. Originallyapproved in 1940. Last previous edition approved in 2015 as C150/C150M 15.DOI: 10.1520/C0150_C0150M-16E01.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact AST

15、M Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshoho

16、cken, PA 19428-2959. United States1C266 Test Method for Time of Setting of Hydraulic-CementPaste by Gillmore NeedlesC451 Test Method for Early Stiffening of Hydraulic Cement(Paste Method)C452 Test Method for Potential Expansion of Portland-Cement Mortars Exposed to SulfateC465 Specification for Proc

17、essing Additions for Use in theManufacture of Hydraulic CementsC563 Test Method for Approximation of Optimum SO3inHydraulic Cement Using Compressive StrengthC1038 Test Method for Expansion of Hydraulic CementMortar Bars Stored in WaterC1702 Test Method for Measurement of Heat of Hydrationof Hydrauli

18、c Cementitious Materials Using IsothermalConduction CalorimetryE29 Practice for Using Significant Digits in Test Data toDetermine Conformance with SpecificationsIEEE/ASTM SI 10 American National Standard for Use ofthe International System of Units (SI): The Modern MetricSystem3. Terminology3.1 Defin

19、itionsSee Terminology C219.4. Ordering Information4.1 Orders for material under this specification shall includethe following:4.1.1 This specification number and date,4.1.2 Type or types allowable. If no type is specified,Type I shall be supplied,4.1.3 Any optional chemical requirements from Table 2

20、,ifdesired, and4.1.4 Any optional physical requirements from Table 4,ifdesired.5. Ingredients5.1 The cement covered by this specification shall containno ingredients except as follows:5.1.1 Portland cement clinker.5.1.2 Water or calcium sulfate, or both. The amounts shallbe such that the limits show

21、n in Table 1 for sulfur trioxide andloss-on-ignition are not exceeded.5.1.3 Limestone. The amount shall not be more than 5.0 %by mass such that the chemical and physical requirements ofthis standard are met (see Note 3). The limestone, defined inTerminology C51, shall be naturally occurring and cons

22、ist of atleast 70 % by mass of one or more of the mineral forms ofcalcium carbonate. If limestone is used, the manufacturer shallreport the amount used, expressed as a percentage of cementmass, as determined using Annex A2, along with the oxidecomposition of the limestone.NOTE 3The standard permits

23、up to 5 % by mass of the final cementproduct to be naturally occurring, finely ground limestone, but does notrequire that limestone be added to the cement. Cement without groundlimestone can be specified in the contract or order.5.1.4 Inorganic processing additions. The amount shall benot more than

24、5.0 % by mass of cement. Not more than oneinorganic processing addition shall be used at a time. Foramounts greater than 1.0 %, they shall have been shown tomeet the requirements of Specification C465 for the inorganicTABLE 1 Standard Composition RequirementsCement TypeAApplicableTestMethodI andIAII

25、 andIIAII(MH)andII(MH)AIII andIIIAIV VAluminum oxide (Al2O3), max, % C114 . 6.0 6.0 . . .Ferric oxide (Fe2O3), max, % C114 . 6.0B6.0B,C. 6.5 .Magnesium oxide (MgO), max, % C114 6.0 6.0 6.0 6.0 6.0 6.0Sulfur trioxide (SO3),Dmax, % C114When (C3A)Eis 8 % or less 3.0 3.0 3.0 3.5 2.3 2.3When (C3A)Eis mor

26、e than 8 % 3.5FF4.5FFLoss on ignition, max, % C114When limestone is not an ingredient 3.0 3.0 3.0 3.0 2.5 3.0When limestone is an ingredient 3.5 3.5 3.5 3.5 3.5 3.5Insoluble residue, max, % C114 1.5 1.5 1.5 1.5 1.5 1.5Tricalcium silicate (C3S)E, max, % See Annex A1 . . . . 35C.Dicalcium silicate (C2

27、S)E, min, % See Annex A1 . . . . 40C.Tricalcium aluminate (C3A)E, max, % See Annex A1 . 8 8 15 7C5BSum of C3S+4.75C3AG, max, % See Annex A1 . . 100C,H. . .Tetracalcium aluminoferrite plus twice thetricalcium aluminate (C4AF+2(C3A),or solid solution (C4AF+C2F), asapplicable, max, %See Annex A1 . . .

28、. . 25BASee Note 2.BDoes not apply when the sulfate resistance limit in Table 4 is specified.CDoes not apply when the heat of hydration limit in Table 4 is specified.DIt is permissible to exceed the values in the table for SO3content, provided it has been demonstrated by Test Method C1038 that the c

29、ement with the increased SO3will not develop expansion exceeding 0.020 % at 14 days. When the manufacturer supplies cement under this provision, supporting data shall be supplied to the purchaser.See Note 6.ESee Annex A1 for calculation.FNot applicable.GSee Note 5.HIn addition, three-day heat of hyd

30、ration testing by Test Method C1702 shall be conducted at least once every six months. Such testing shall not be used for acceptanceor rejection of the cement, but results shall be reported for informational purposes.C150/C150M 1612processing addition in the amount used or greater. If aninorganic pr

31、ocessing addition is used, the manufacturer shallreport the amount used, expressed as a percentage of cementmass, along with the oxide composition of the processingaddition. See Note 4.NOTE 4These requirements are based on data and recommendationsby Taylor.35.1.5 Organic Processing additions. They s

32、hall have beenshown to meet the requirements of Specification C465 in theamounts used or greater and the total amount of organicprocessing additions used shall not exceed 1.0 % by mass ofcement.5.1.6 Air-entraining addition (for air-entraining portlandcement only). The interground addition shall con

33、form to therequirements of Specification C226.6. Chemical Composition6.1 Portland cement of each of the ten types shown inSection 1 shall conform to the respective standard chemicalrequirements prescribed in Table 1. In addition, optionalchemical requirements are shown in Table 2.NOTE 5The limit on

34、the sum, C3S + 4.75C3A, in Table 1 providescontrol on the heat of hydration of the cement and is consistent with a TestMethod C186 seven-day heat of hydration limit of 335 kJ/kg 80 cal/g, ora Test Method C1702 three-day heat of hydration limit of 315 kJ/kg75 cal g.NOTE 6There are cases where perform

35、ance of a cement is improvedwith SO3in excess of the Table 1 limits in this specification. Test MethodC563 is one of several methods a manufacturer can use to evaluate theeffect of sulfate content on cement characteristics. Whenever SO3contentof a cement exceeds Table 1 limits, Test Method C1038 res

36、ults provideevidence that excessive expansion does not occur at this higher sulfatecontent.7. Physical Properties7.1 Portland cement of each of the ten types shown inSection 1 shall conform to the respective standard physicalrequirements prescribed in Table 3. In addition, optionalphysical requireme

37、nts are shown in Table 4.8. Sampling8.1 When the purchaser desires that the cement be sampledand tested to verify compliance with this specification, performsampling and testing in accordance with Practice C183.8.2 Practice C183 is not designed for manufacturing qualitycontrol and is not required fo

38、r manufacturers certification.9. Test Methods9.1 Determine the applicable properties enumerated in thisspecification in accordance with the following test methods:9.1.1 Chemical AnalysisTest Methods C114.9.1.2 Air Content of MortarTest Method C185.9.1.3 Fineness by Air PermeabilityTest Method C204.9

39、.1.4 Autoclave ExpansionTest Method C151.9.1.5 StrengthTest Method C109/C109M.9.1.6 Time of Setting by Vicat NeedlesTest Method C191.9.1.7 False SetTest Method C451.9.1.8 Heat of HydrationTest Method C186 or C1702.9.1.9 Sulfate ResistanceTest Method C452 (sulfate expan-sion).9.1.10 Time of Setting b

40、y Gillmore NeedlesTest MethodC266.9.1.11 Fineness by TurbidimeterTest Method C115.9.1.12 Calcium Sulfate (Expansion of) MortarTestMethod C1038.10. Inspection10.1 Inspection of the material shall be made as agreed uponbetween the purchaser and the seller as part of the purchasecontract.11. Rejection1

41、1.1 The cement shall be rejected if it fails to meet any ofthe requirements of this specification.11.2 At the option of the purchaser, retest, before using,cement remaining in bulk storage for more than six months orcement in bags in local storage in the custody of a vendor formore than three months

42、 after completion of tests and reject thecement if it fails to conform to any of the requirements of thisspecification. Cement so rejected shall be the responsibility ofthe owner of record at the time of resampling for retest.3Taylor, P., “Specifications and Protocols for Acceptance Tests on Process

43、ingAdditions in Cement Manufacturing,” NCHRP Report 607, Transportation ResearchBoard, Washington, DC 20008, 96 pp. Available at www.trb.org.TABLE 2 Optional Composition RequirementsACement TypeApplicable TestMethodI and IA II and IIAII(MH) andII(MH)AIII and IIIA IV V RemarksTricalcium aluminate(C3A

44、)B, max, %See Annex A1 . . . 8 . .for moderatesulfate resistanceTricalcium aluminate(C3A)B, max, %See Annex A1 . . . 5 . .for high sulfateresistanceEquivalent alkalies(Na2O + 0.658K2O), max, %C114 0.60C0.60C0.60C0.60C0.60C0.60Clow-alkali cementAThese optional requirements apply only when specificall

45、y requested. Verify availability before ordering. See Note 2.BSee Annex A1 for calculation.CSpecify this limit when the cement is to be used in concrete with aggregates that are potentially reactive and no other provisions have been made to protect the concretefrom deleteriously reactive aggregates.

46、 Refer to Specification C33 for information on potential reactivity of aggregates.C150/C150M 1613TABLE3StandardPhysicalRequirementsCementTypeAApplicableTestMethodIIAIIIIAII(MH)II(MH)AIIIIIIAIVVAircontentofmortar,Bvolume%:C185max12221222122212221212min.16.16.16.16.Fineness,specificsurface,m2/kgAirper

47、meabilitytestC204min260260260260260260.260260max.430C430C.430.Autoclaveexpansion,max,%C1510.800.800.800.800.800.800.800.800.800.80Strength,notlessthanthevaluesshownfortheagesindicatedasfollows:DCompressivestrength,MPapsi:C109/ C109M1day.12.0 174010.0 1450.3days12.0 174010.0 145010.0 14508.0 116010.0

48、 1450 7.0E1020E8.0 11606.0E870E24.0 348019.0 2760.8.0 11607days19.0 276016.0 232017.0 247014.0 203017.0 247012.0E1740E14.0 2030 9.0E1310E.7.0 102015.0 218028days.17.0 247021.0 3050Timeofsetting;Vicattest:FC191Timeofsetting,min,notlessthan45454545454545454545Timeofsetting,min,notmorethan3753753753753

49、75375375375375375ASeeNote2.BCompliancewiththerequirementsofthisspecificationdoesnotnecessarilyensurethatthedesiredaircontentwillbeobtainedinconcrete.CMaximumfinenesslimitsdonotapplyifthesumofC3S+4.75C3Aislessthanorequalto90.DThestrengthatanyspecifiedtestageshallbenotlessthanthatattainedatanypreviousspecifiedtestage.EWhentheoptionalheatofhydrationinTable4isspecified.FThetimeofsettingisthatdescribedasinitialsettingtimeinTestMethodC191.C150/C150M 161411.3 Packag