ASTM C150-2007 Standard Specification for Portland Cement《硅酸盐水泥的标准规范》.pdf

1、Designation: C 150 07Standard Specification forPortland Cement1This standard is issued under the fixed designation C 150; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates

2、the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope*1.1 This specification covers eight types of portland cement,as follows (see Note 2):1.1

3、.1 Type IFor use when the special properties specifiedfor any other type are not required.1.1.2 Type IAAir-entraining cement for the same uses asType I, where air-entrainment is desired.1.1.3 Type IIFor general use, more especially when mod-erate sulfate resistance or moderate heat of hydration isde

4、sired.1.1.4 Type IIAAir-entraining cement for the same uses asType II, where air-entrainment is desired.1.1.5 Type IIIFor use when high early strength is desired.1.1.6 Type IIIAAir-entraining cement for the same use asType III, where air-entrainment is desired.1.1.7 Type IVFor use when a low heat of

5、 hydration isdesired.1.1.8 Type VFor use when high sulfate resistance isdesired.NOTE 1Some cements are designated with a combined type classifi-cation, such as Type I/II, indicating that the cement meets the require-ments of the indicated types and is being offered as suitable for use wheneither typ

6、e is desired.NOTE 2Cement conforming to the requirements for all types are notcarried in stock in some areas. In advance of specifying the use of cementother than Type I, determine whether the proposed type of cement is, orcan be made, available.1.2 When both SI and inch-pound units are present, the

7、 SIunits are the standard. The inch-pound units are approxima-tions listed for information only.1.3 The text of this standard references notes and footnoteswhich provide explanatory material. These notes and footnotes(excluding those in tables and figures) shall not be consideredas requirements of t

8、he standard.2. Referenced Documents2.1 ASTM Standards:2C33 Specification for Concrete AggregatesC51 Terminology Relating to Lime and Limestone (as usedby the Industry)C 109/C 109M Test Method for Compressive Strength ofHydraulic Cement Mortars(Using 2-in. or 50-mm CubeSpecimens)C114 Test Methods for

9、 Chemical Analysis of HydraulicCementC115 Test Method for Fineness of Portland Cement by theTurbidimeterC 151 Test Method for Autoclave Expansion of HydraulicCementC 183 Practice for Sampling and the Amount of Testing ofHydraulic CementC 185 Test Method for Air Content of Hydraulic CementMortarC 186

10、 Test Method for Heat of Hydration of HydraulicCementC 191 Test Methods for Time of Setting of HydraulicCement by Vicat NeedleC 204 Test Methods for Fineness of Hydraulic Cement byAir-Permeability ApparatusC 219 Terminology Relating to Hydraulic CementC 226 Specification for Air-Entraining Additions

11、 for Use inthe Manufacture of Air-Entraining Hydraulic CementC 266 Test Method for Time of Setting of Hydraulic-Cement Paste by Gillmore NeedlesC 451 Test Method for Early Stiffening of Hydraulic Ce-ment (Paste Method)C 452 Test Method for Potential Expansion of Portland-Cement Mortars Exposed to Su

12、lfateC 465 Specification for Processing Additions for Use in theManufacture of Hydraulic Cements1This specification is under the jurisdiction of ASTM Committee C01 onCement and is the direct responsibility of Subcommittee C01.10 on HydraulicCements for General Concrete Construction.Current edition a

13、pproved May 1, 2007. Published June 2007. Originallyapproved in 1940. Last previous edition approved in 2005 as C 150 05.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refe

14、r to the standards Document Summary page onthe ASTM website.1*A Summary of Changes section appears at the end of this standard.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.C 563 Test Method for Approximation of Optimum SO3inHydraul

15、ic Cement Using Compressive StrengthC 1038 Test Method for Expansion of Hydraulic CementMortar Bars Stored in WaterE29 Practice for Using Significant Digits in Test Data toDetermine Conformance with Specifications3. Terminology3.1 DefinitionsSee Terminology C 219.4. Ordering Information4.1 Orders fo

16、r material under this specification shall includethe following:4.1.1 This specification number and date,4.1.2 Type or types allowable. If no type is specified, TypeI shall be supplied,4.1.3 Any optional chemical requirements from Table 2,ifdesired, and4.1.4 Any optional physical requirements from Ta

17、ble 4,ifdesired.5. Ingredients5.1 The cement covered by this specification shall containno ingredients except as follows:5.1.1 Portland cement clinker.5.1.2 Water or calcium sulfate, or both. The amounts shallbe such that the limits shown in Table 1 for sulfur trioxide andloss-on-ignition are not ex

18、ceeded.5.1.3 Limestone. The amount shall not be more than 5.0 %by mass such that the chemical and physical requirements ofthis standard are met (See Note 3). The limestone, defined inTerminology C51, shall be naturally occurring and consist ofat least 70 % by mass of one or more of the mineral forms

19、 ofcalcium carbonate.NOTE 3The standard permits up to 5 % by mass of the final cementproduct to be naturally occurring, finely ground limestone, but does notrequire that limestone be added to the cement. Cement without groundlimestone can be specified in the contract or order.5.1.4 Processing additi

20、ons. They shall have been shown tomeet the requirements of Specification C 465 in the amountsused or greater.5.1.5 Air-entraining addition (for air-entraining portlandcement only). The interground addition shall conform to therequirements of Specification C 226.6. Chemical Composition6.1 Portland ce

21、ment of each of the eight types shown inSection 1 shall conform to the respective standard chemicalrequirements prescribed in Table 1. In addition, optionalchemical requirements are shown in Table 2.NOTE 4The limit on the sum, C3S + 4.75C3A, in Table 1 providescontrol on the heat of hydration of the

22、 cement and is consistent with a TestMethod C 186 7-day heat of hydration limit of 335 kJ/kg (80 cal/g).7. Physical Properties7.1 Portland cement of each of the eight types shown inSection 1 shall conform to the respective standard physicalrequirements prescribed in Table 3. In addition, optionalphy

23、sical requirements are shown in Table 4.8. Sampling8.1 When the purchaser desires that the cement be sampledand tested to verify compliance with this specification, performsampling and testing in accordance with Practice C 183.8.2 Practice C 183 is not designed for manufacturing qualitycontrol and i

24、s not required for manufacturers certification.TABLE 1 Standard Composition RequirementsCement TypeAApplicable TestMethodI andIAII andIIAIII andIIIAIV VAluminum oxide (Al2O3), max, % C114 . 6.0 . . .Ferric oxide (Fe2O3), max, % C114 . 6.0B,C. 6.5 .Magnesium oxide (MgO), max, % C114 6.0 6.0 6.0 6.0 6

25、.0Sulfur trioxide (SO3),Dmax, % C114When (C3A)Eis 8 % or less 3.0 3.0 3.5 2.3 2.3When (C3A)Eis more than 8 % 3.5F4.5FFLoss on ignition, max, % C114 3.0 3.0 3.0 2.5 3.0Insoluble residue, max, % C114 0.75 0.75 0.75 0.75 0.75Tricalcium silicate (C3S)E, max, % See Annex A1 . . . 35B.Dicalcium silicate (

26、C2S)E, min, % See Annex A1 . . . 40B.Tricalcium aluminate (C3A)E, max, % See Annex A1 . 8 15 7B5CSum of C3S+4.75C3AG, max, % See Annex A1 . 100H. . .Tetracalcium aluminoferrite plus twice the tricalcium aluminate (C4AF+2(C3A),or solid solution (C4AF+C2F), as applicable, max, % See Annex A1 . . . . 2

27、5CASee Note 2.BDoes not apply when the heat of hydration limit in Table 4 is specified.CDoes not apply when the sulfate resistance limit in Table 4 is specified.DThere are cases where optimum SO3(using Test Method C 563) for a particular cement is close to or in excess of the limit in this specifica

28、tion. In such cases whereproperties of a cement can be improved by exceeding the SO3limits stated in this table, it is permissible to exceed the values in the table, provided it has beendemonstrated by Test Method C 1038 that the cement with the increased SO3will not develop expansion in water excee

29、ding 0.020 % at 14 days. When the manufacturersupplies cement under this provision, he shall, upon request, supply supporting data to the purchaser.ESee Annex A1 for calculation.FNot applicable.GSee Note 4.HIn addition, 7-day heat of hydration testing by Test Method C 186 shall be conducted at least

30、 once every six months. Such testing shall not be used for acceptanceor rejection of the cement, but results shall be reported for informational purposes.C1500729. Test Methods9.1 Determine the applicable properties enumerated in thisspecification in accordance with the following test methods:9.1.1

31、Air Content of MortarTest Method C 185.9.1.2 Chemical AnalysisTest Methods C114.9.1.3 StrengthTest Method C 109/C 109M.9.1.4 False SetTest Method C 451.9.1.5 Fineness by Air PermeabilityTest Method C 204.9.1.6 Fineness by TurbidimeterTest Method C115.9.1.7 Heat of HydrationTest Method C 186.9.1.8 Au

32、toclave ExpansionTest Method C 151.9.1.9 Time of Setting by Gillmore NeedlesTest MethodC 266.9.1.10 Time of Setting by Vicat NeedlesTest MethodC 191.TABLE 2 Optional Composition RequirementsACement TypeApplicableTest MethodI andIAII andIIAIII andIIIAIV V RemarksTricalcium aluminate (C3A)B, max, % Se

33、e AnnexA1. . 8 . . for moderate sulfate resistanceTricalcium aluminate (C3A)B, max, % See AnnexA1. . 5 . . for high sulfate resistanceEquivalent alkalies (Na2O + 0.658K2O), max, % C114 0.60C0.60C0.60C0.60C0.60Clow-alkali cementAThese optional requirements apply only when specifically requested. Veri

34、fy availability before ordering. See Note 2.BSee Annex A1 for calculation.CSpecify this limit when the cement is to be used in concrete with aggregates that are potentially reactive and no other provisions have been made to protect the concretefrom deleteriously reactive aggregates. Refer to Specifi

35、cation C33for information on potential reactivity of aggregates.TABLE 3 Standard Physical RequirementsCement TypeAApplicableTestMethodI IA II IIA III IIIA IV VAir content of mortar,Bvolume %: C 185max 12 22 12 22 12 22 12 12min . 16 . 16 . 16 . .Fineness,Cspecific surface, m2/kg (alternative methods

36、):Turbidimeter test C115Average value, minD160 160 160 160 . . 160 160Any one sample, minE150 150 150 150 . . 150 150Average value, maxD. . 240F240F. . 240 .Any one sample, maxE. . 245F245F. . 245 .Air permeability test C 204Average value, minD280 280 280 280 . . 280 280Any one sample, minE260 260 2

37、60 260 . . 260 260Average value, maxD. . 420F420F. . 420 .Any one sample, maxE. . 430F430F. . 430 .Autoclave expansion, max, % C 151 0.80 0.80 0.80 0.80 0.80 0.80 0.80 0.80Strength, not less than the values shown for the agesindicated as follows:GCompressive strength, MPa (psi): C 109/C 109M1 day .

38、. . . 12.0(1740)10.0(1450). .3 days 12.0(1740)10.0(1450)10.0(1450)7.0H(1020)H8.0(1160)6.0H(870)H24.0(3480)19.0(2760). 8.0(1160)7 days 19.0(2760)16.0(2320)17.0(2470)12.0H(1740)H14.0(2030)9.0H(1310)H. . 7.0(1020)15.0(2180)28 days . . . . . . 17.0(2470)21.0(3050)Time of setting; Vicat test:IC 191Time o

39、f setting, min, not less than 45 45 45 45 45 45 45 45Time of setting, min, not more than 375 375 375 375 375 375 375 375ASee Note 2.BCompliance with the requirements of this specification does not necessarily ensure that the desired air content will be obtained in concrete.CThe testing laboratory sh

40、all select the fineness method to be used. However, when the sample fails to meet the requirements of the air-permeability test, the turbidimetertest shall be used, and the requirements in this table for the turbidimetric method shall govern.DAverage value shall be determined on the last consecutive

41、 five samples from a source.EThe value of any one sample shall be the result of a test or average of tests on any one sample.FMaximum average and maximum single sample fineness limits do not apply if the sum of C3S+4.75C3A is less than or equal to 90.GThe strength at any specified test age shall be

42、not less than that attained at any previous specified test age.HWhen the optional heat of hydration in Table 4 is specified.IThe time of setting is that described as initial setting time in Test Method C 191.C1500739.1.11 Sulfate ResistanceTest Method C 452 (sulfate ex-pansion).9.1.12 Calcium Sulfat

43、e (expansion of) MortarTestMethod C 1038.9.1.13 Optimum SO3Test Method C 563.10. Inspection10.1 Inspection of the material shall be made as agreed uponbetween the purchaser and the seller as part of the purchasecontract.11. Rejection11.1 The cement shall be rejected if it fails to meet any ofthe req

44、uirements of this specification.11.2 At the option of the purchaser, retest, before using,cement remaining in bulk storage for more than 6 months orcement in bags in local storage in the custody of a vendor formore than 3 months after completion of tests and reject thecement if it fails to conform t

45、o any of the requirements of thisspecification. Cement so rejected shall be the responsibility ofthe owner of record at the time of resampling for retest.11.3 Packages shall identify the mass contained as netweight.At the option of the purchaser, packages more than 2 %below the mass marked thereon s

46、hall be rejected and if theaverage mass of packages in any shipment, as shown bydetermining the mass of 50 packages selected at random, is lessthan that marked on the packages, the entire shipment shall berejected.12. Manufacturers Statement12.1 At the request of the purchaser, the manufacturer shal

47、lstate in writing the nature, amount, and identity of anyair-entraining addition and of any processing addition used,and also, if requested, shall supply test data showing compli-ance of such air-entraining addition with Specification C 226and of such processing addition with Specification C 465.12.

48、2 When limestone is used, the manufacturer shall state inwriting the amount thereof and, if requested by the purchaser,shall supply comparative test data on chemical and physicalproperties of the cement with and without the limestone (SeeNote 5). The comparative tests do not supersede the normaltest

49、ing to confirm that the cement meets chemical and physicalrequirements of this standard. The amount of limestone incement shall be determined in accordance with Annex A2.NOTE 5Comparative test data may be from qualification tests per-formed by the manufacturer during formulation of the cement withlimestone.13. Packaging and Package Marking13.1 When the cement is delivered in packages, the words“Portland Cement,” the type of cement, the name and brand ofthe manufacturer, and the mass of the cement contained thereinshall be plainly marked on each package