1、Designation: C 882 05Standard Test Method forBond Strength of Epoxy-Resin Systems Used With ConcreteBy Slant Shear1This standard is issued under the fixed designation C 882; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year
2、of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope1.1 This test method covers the deter
3、mination of the bondstrength of epoxy-resin-base bonding systems for use withportland-cement concrete. This test method covers bondinghardened concrete to hardened or freshly-mixed concrete.1.2 The values stated in either inch-pound units or SI unitsare to be regarded separately as standard. Within
4、the text, theSI units are shown in brackets. The values stated in eachsystem are not exact equivalents; therefore, each system shallbe used independently of the other. Combining values from thetwo systems may result in nonconformance with this testmethod.1.3 This standard does not purport to address
5、 all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use. A specific hazardstatement is given in Section 8.2. Referen
6、ced Documents2.1 ASTM Standards:2C 39/C 39M Test Method for Compressive Strength of Cy-lindrical Concrete SpecimensC 109/C 109M Test Method for Compressive Strength ofHydraulic Cement Mortars (Using 2-in. or 50-mm CubeSpecimens)C 150 Specification for Portland CementC 192/C 192M Practice for Making
7、and Curing ConcreteTest Specimens in the LaboratoryC511 Specification for Mixing Rooms, Moist Cabinets,Moist Rooms and Water Storage Tanks Used in the Testingof Hydraulic Cements and ConcretesC 617 Practice for Capping Cylindrical Concrete Speci-mensC 881/C 881M Specification for Epoxy-Resin-Base Bo
8、nd-ing Systems for Concrete3. Terminology3.1 See Section on Terminology of Specification C 881/C 881M.4. Summary of Test Method4.1 The bond strength is determined by using the epoxysystem to bond together two equal sections ofa3by6-in. 75by 150-mm portland-cement mortar cylinder, each section ofwhic
9、h has a diagonally cast bonding area at a 30 angle fromvertical. After suitable curing of the bonding agent, the test isperformed by determining the compressive strength of thecomposite cylinder.5. Significance and Use5.1 The strength developed by a bonding system that joinstwo regions of concrete i
10、s its most important property.6. Apparatus6.1 Apparatus to Mix Portland-Cement MortarThis ap-paratus shall be as described in Test Method C 109/C 109M,except for the sections on specimen molds, tamper, and testingmachine.6.2 Specimen MoldsThe molds shall be constructed in theform of right cylinders,
11、 3 6116 in. 75 6 2 mm in insidediameter and 6 6116 in. 150 6 2 mm high. All molds shallbe either selected or machined so that the maximum range ofthe differences in each of the dimensions of the group of moldsis less than164 in. 0.5 mm. The molds shall be made of metalnot attacked by portland-cement
12、 mortar. The side of the moldshall be sufficiently rigid to prevent spreading or warping. Themolds shall be made watertight before use. A satisfactorymaterial for this purpose is the paraffin-rosin mixture describedin Test Method C 109/C 109M.6.3 Dummy SectionA dummy section (Fig. 1) shall bemachine
13、d of a hard material that is not attacked by portland-cement mortar. It shall fit the mold and be equal to half the1This test method is under the jurisdiction of ASTM Committee C09 onConcrete and Concrete Aggregates, and is the direct responsibility of SubcommitteeC09.25 on Organic Materials for Bon
14、ding.Current edition approved Nov. 1, 2005. Published November 2005. Originallyapproved in 1978. Last previous edition approved in 1999 as C 882 99.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandar
15、ds volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.volume of the cylinder, but at an angle of 30 from the vertical.Additional dummy sections can be m
16、ade by casting an epoxy-resin mortar against the machined dummy section contained ina specimen mold. Due precautions, such as waxing, shall betaken to prevent the bonding of the epoxy-resin mortar to themachined dummy section or the mold.6.4 Tamping RodThe tamping rod shall be a round rod ofbrass or
17、 plastic,38 in. 10 mm in diameter and approximately12 in. 300 mm long, having both ends rounded to hemispheri-cal tips.6.5 Apparatus for Mixing Epoxy-Resin Bonding SystemAglass, plastic, or metal container of approximately 3 oz. 0.1 Lcapacity shall be used to hand-mix the bonding system. Atongue dep
18、ressor or wooden stick of similar dimensions shallbe used as a paddle.6.6 Testing MachineThe testing machine shall be asdescribed in Test Method C 39/C 39M.6.7 Moist RoomThe moist room shall conform to therequirements of Specification C511.6.8 Temperature-Conditioning Chambers Rooms orchambers in wh
19、ich the temperature is maintained appropriateto the class of the resin system being tested, in accordance withSpecification C 881/C 881M.7. Materials7.1 Laboratory conditions, materials, proportions, and pro-cedures for mixing the portland-cement mortar shall be inaccordance with Test Method C 109/C
20、 109M. A Type IIIcement (Specification C 150) shall be used.7.2 Lightly oil the dummy section and the cylinder mold.Position the dummy section in the mold with the slant side up.Place the portland-cement mortar in the mold in three layers ofapproximately equal volume. Rod each layer with 25 strokes
21、ofthe tamping rod. Distribute the strokes uniformly over thesection and rod deeply enough to penetrate into any underlyinglayer. Rod the bottom layer as deeply as possible. Strike off thesurface of the top layer with the trowel, and cover the specimenand mold with a glass or metal plate. Cure the mo
22、rtarhalf-cylinder in accordance with Practice C 192/C 192M for atleast 28 days. Then dry the half-cylinder in laboratory air for atleast 7 days.As an alternative, a complete 3 by 6-in. 75 by 150mm cylinder shall be cast and, after cure, may be saw-cut atan angle of 30.7.3 A3 by 6-in. 75 by 150-mm cy
23、linder of the mortar shallhave a compressive strength, when tested in accordance with11.3, of at least 4500 psi 31 MPa at 28-days age.8. Hazards8.1 WarningEpoxy resins contain irritants, especially tothe skin, eyes, and respiratory system. Persons handling thesematerials shall use appropriate protec
24、tive clothing, includingrubber or plastic gloves. If an epoxy resin should contact theskin, it shall be removed immediately with a dry cloth or papertowel, and the area of contact shall be washed thoroughly withsoap and water. Solvents shall not be used, because they carrythe irritant into the skin.
25、 Cured epoxy resins are innocuous.9. Sampling9.1 Take samples in accordance with Specification C 881/C 881M.10. Test Specimens10.1 Three composite test specimens are required for allTypes of resin systems.10.2 Conditioning:10.2.1 Types I, III, IV, VI, and VII SystemsCondition theresin system compone
26、nts, the mortar sections, and all equip-ment that will contact the resin to the temperatures specified inSpecification C 881/C 881M10.2.1.1 Prepare the test specimens and make provision formaintaining them at the appropriate temperature during theentire cure time. Prepare the surface to be bonded by
27、 sand-blasting and dry brushing to remove all loose surface material.10.2.1.2 Use mortar sections and assemblies that have beensoaked in water for 24 h. Place the face of the mortar sectionsto be bonded on an absorbent material for 10 min prior toapplying the adhesive. For assembled test specimens,
28、removeall water by shaking. Allow to air dry for 15 min.10.2.2 Type II and Type V SystemsSince Type II and TypeV resins are appropriate for use only at temperatures thatpermit strength gain of the freshly prepared concrete, only theconditioning temperature for a Class C resin, 73 6 2F2361 C, need be
29、 provided.10.3 Specimen Preparation:10.3.1 Type I, III, IV, VI, and VII, Grade 2 or 3 SystemsTwo mortar sections will be needed for each test specimen.Wrap 4 mil (100 m) of polyethylene film 6 by 20 in. 150 by500 mm around one section of each pair, even with the baseand secure with masking tape. Tho
30、roughly mix the componentsof the bonding system in the proportions recommended by theformulator. A mixing time of 3 min should suffice. Support thefilm-wrapped mortar section so that the prepared bondingsurface is horizontal.10.3.1.1 To test Grade 2 systems, apply a 0.02 in. 0.5 mmlayer of the bondi
31、ng systems to the prepared elliptical surfaceof the film wrapped mortar section. Using Grade 3 systems,apply a 0.02 in. 0.5 mm layer of bonding system on theprepared elliptical surface of the mortar section not filmDimensionsin. mmADiameter 3.000 7562BHeight 5.598 14062CSlant height 6.000 15062DBase
32、 height 0.402 1062FIG. 1 Dummy SectionC882052wrapped. For the determination of contact strength (Specifica-tion C 881/C 881M) of Type VI and VII systems, apply a116-in. 2.0-mm layer to the prepared elliptical surface of bothmortar sections.10.3.1.2 Insert mortar sections not film wrapped into thecyl
33、inder formed by film surrounding other mortar sections andsqueeze out the excess resin through a hole, or holes, punchedin the film at the bondline, while keeping the joint horizontal.Secure the assembly with sufficient additional masking tapeplaced around the film. Be sure the joint is entirely fil
34、led. Keepthe bonded joint horizontal for 48 h, then remove all themasking tape.10.3.2 Type I, III, and IV, Grade 1 SystemsTwo mortarsections will be needed for each test specimen. Prepare theelliptical bonding surface as described in 10.2. Place the twohalves of the specimen together, forming a gap
35、approximately0.02 in. 0.5 mm. Wrap masking tape around the periphery ofthe specimen close to each end. Place additional tape along thejoint. Coat the tape over the joint with hot paraffin to helpcontain the epoxy when it is poured into the slit. Support thespecimen so that the taped joint is vertica
36、l. Cut a slit in the tapeto expose approximately34 in. (20 mm) of the upper portion ofthe joint. Slowly pour the resin bonding system into theexposed joint until it is completely filled. Keep the jointvertical for 48 h, then remove all masking tape.10.3.3 Type II and V SystemsOne hardened mortar sec
37、tionwill be needed for each test specimen. Prepare the mortarsurface as described in 10.2, but do not tape around the edge.Mix the components of the bonding system as described in10.3. Brush the bonding system on the prepared surface. Placethe primed mortar section in the cylinder mold that hasprevi
38、ously been lined with a 4-mil (100-m) polyethylenesheet. Support the mold so that the bonding surface of themortar section is horizontal. Place a layer of freshly mixedportland-cement mortar over the primed surface to a depth ofapproximately12 in. 15 mm. Rod the layer with the tampingrod gently, so
39、as to disturb the layer of resin as little as possible.Place the mold in its normal vertical position, and placeadditional mortar into the mold in two layers of approximatelyequal volume. Rod each layer with 25 strokes of the tampingrod. Distribute the strokes over the cross section, and makethem de
40、ep enough to penetrate into the underlying layer. Strikeoff the surface of the top layer with the trowel, and cover themold with a glass or metal plate.10.4 Curing:10.4.1 Type I, III, IV, VI, and VII SystemsMaintain allspecimens at the preparation temperature in a moist room forthe specified period
41、of time.10.4.2 Type II and V SystemsDemold the test specimensand cure in accordance with the curing section of PracticeC 192/C 192M.11. Procedure11.1 Remove the specimens from the cure environment afterthe specified time.11.2 CappingCap the specimens immediately after re-moval from curing in accorda
42、nce with Practice C 617.11.3 Strength TestingTest the specimens at 73 6 2F236 1 C in compression after capping in accordance with TestMethod C 39/C 39M.12. Calculation12.1 Calculate the bond strength of the resin bondingsystem by dividing the load carried by the specimen at failureby the area of the
43、 bonded surface (Note 1). Reduce the area ofthe bonded surface by that of any voids found in the bond oninspection after test. Only voids larger than18 in. 3 mmshould be counted in reducing the area. Report the results to thenearest 10 psi (0.1 MPa).NOTE 1The area of the elliptical bonding surface o
44、f the test cylindersspecified in this test method is 14.13 in.29116 mm2. The actual areashould be based on measuring the lengths of the two axes for the areas ofan ellipse 0.7854 a b13. Report13.1 Report the following information:13.1.1 Identification number,13.1.2 Bond strength,13.1.3 Bonding area,
45、13.1.4 Number and total area of voids in the bond,13.1.5 Type and position of the fracture (in the bondingmaterial, in the mortar, or in the interface between them), and13.1.6 Defects in either the specimen or the cap.14. Precision and Bias14.1 PrecisionThe standard deviation was found to be365 psi
46、for the 14 day bond strength average of 1790 psi.Therefore, results of two properly conducted tests from twolaboratories on similar batches should not differ from eachother by more than 1022 psi.14.2 BiasThis test method has no bias since the valuesdetermined can only be defined in terms of this tes
47、t method.15. Keywords15.1 adhesives; bonding agents; bond strength; shear bondC882053ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of th
48、e validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. You
49、r comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor
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