ASTM D1062-2002 Standard Test Method for Cleavage Strength of Metal-to-Metal Adhesive Bonds《金属之间胶粘剂粘结力抗裂强度的标准测试方法》.pdf

1、Designation: D 1062 02Standard Test Method forCleavage Strength of Metal-to-Metal Adhesive Bonds1This standard is issued under the fixed designation D 1062; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision.

2、 A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.INTRODUCTIONThe accuracy of the results of strength tests of a

3、dhesive bonds will depend on the conditions underwhich the bonding process is carried out. Unless otherwise agreed upon by the manufacturer and thepurchaser, the bonding conditions shall be prescribed by the manufacturer of the adhesive. In order toensure that complete information is available to th

4、e individual conducting the tests, the manufacturerof the adhesive shall furnish numerical values and other specific information for each of the followingvariables:(1) Procedure for preparation of surfaces prior to application of the adhesive, the cleaning anddrying of metal surfaces, and special su

5、rface treatments such as sanding that are not specificallylimited by the pertinent test method.(2) Complete mixing directions for the adhesive.(3) Conditions for application of the adhesive, including the rate of spread or thickness of film,number of coats to be applied, whether to be applied to one

6、 or both surfaces, and the conditions ofdrying where more than one coat is required.(4) Assembly conditions before application of pressure, including the room temperature, length oftime, and whether open or closed assembly is to be used.(5) Curing conditions, including the amount of pressure to be a

7、pplied, the length of time underpressure, and the temperature of the assembly when under pressure. State whether this temperature isthat of the bond line or of the atmosphere at which the assembly is to be maintained.(6) Conditioning procedure before testing, unless a standard procedure is specified

8、, including thelength of time, temperature, and relative humidity.A range may be prescribed for any variable by the manufacturer of the adhesive if it can be assumedby the test operator that any arbitrarily chosen value within such a range or any combination of suchvalues for several variables will

9、be acceptable to both the manufacturer and the purchaser of theadhesive.1. Scope1.1 This test method covers the determination of the com-parative cleavage properties of adhesive bonds when tested onstandard shape metal specimens under specified conditions ofpreparation and testing. It may be used al

10、so to compareadhesives used with other metallic materials having anyspecified surface treatment.1.2 The values stated in SI units are to be regarded as thestandard. The values in parentheses are for information only.1.3 This standard does not purport to address all of thesafety concerns, if any, ass

11、ociated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:A 108 Specification for Steel Bars, Carbon, Cold-Finished

12、,Standard Quality2B 16/B 16M Specification for Free-Cutting Brass Rod, Bar,and Shapes for Use in Screw Machines3B 133 Specification for Copper Rod, Bar, and Shapes4B 139/B 139M Specification for Phosphor Bronze Rod, Bar,and Shapes31This test method is under the jurisdiction of ASTM Committee D14 onA

13、dhesives and is the direct responsibility of Subcommittee D14.80 on MetalBonding Adhesives.Current edition approved Sept. 10, 2002. Published November 2002. Originallypublished as D 1062 49 T. Last previous edition D 1062 96e1.2Annual Book of ASTM Standards, Vol 01.05.3Annual Book of ASTM Standards,

14、 Vol 02.01.4Discontinued; see 1995 Annual Book of ASTM Standards, Vol 02.01.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.B 211 Specification for Aluminum and Aluminum-AlloyBar, Rod, and Wire5D 907 Terminology of Adhesives62.2 Othe

15、r Documents:AISI 102073. Terminology3.1 DefinitionsMany of the terms in this test method aredefined in Terminology D 907.3.2 Definitions of Terms Specific to This Standard:3.2.1 contact failure, nin characterizing the locus of anadhesive joint failure, the lack of adhesive being in contactwith the s

16、ubstrate.3.2.1.1 DiscussionContact failure may be due to condi-tions such as uneven surfaces, poor pressure distribution, orinsufficient adhesive in the bondline.4. Apparatus4.1 Use a testing machine capable of maintaining the rate ofloading specified in 8.2, and consisting essentially of thefollowi

17、ng:4.1.1 Fixed MemberA fixed or essentially stationarymember, carrying one grip.4.1.2 Movable Member, carrying a second grip.4.1.3 Grips, for holding a test specimen between the fixedmember and the movable member. The grips are of theself-aligning type; that is, they shall be attached to the fixedan

18、d movable member, respectively, in such a way that they willmove into alignment as soon as any load is applied, so that thedirection of pull is at right angles to the point of adhesion.Recommended grips are shown in Figs. 1 and 2.5. Test Specimens5.1 The test specimens consist of metal pieces, confo

19、rmingto the dimensions and conditions shown in Fig. 3, and gluedtogether as described in Section 6 with the adhesive to betested. Various metallic materials and surface treatments maybe specified to simulate surface conditions. The followinggrades of metal are recommended for the test specimens, asb

20、eing representative of a wide range of metallic materials:Metal DesignationBrass ASTM B 16, C36000; half-hard temperCopper ASTM B 133, C11000; hard temperAluminum ASTM B 211, A92024; specify temperSteel AISI 1020, G10200 cold-finished barPhosphor bronze ASTM B 139, C544005.2 The metal pieces may be

21、reused after testing, providedthe adhesive is completely removed from the adhering surfacesand the surfaces are reconditioned.5.3 Unless otherwise agreed upon by the purchaser and themanufacturer, test at least ten specimens for each adhesive, but5Annual Book of ASTM Standards, Vol 02.02.6Annual Boo

22、k of ASTM Standards, Vol 15.06.7Available from American Iron and Steel Institute (AISI), 1101 17th St., NW,Suite 1300, Washington, DC 20036.AUpper grip CLower gripBPin connecting upper and lower grips DPin for attaching grip to specimenmm(in.)2.3(332)4.5(316)6(14)7.5(516)9(38)10.5(716)12.7(12)18.5(1

23、316)19(34)21(78)28(118)30(1316)38(112)44(134)FIG. 1 Details of Test GripsD1062022in no case less than five.6. Bonding6.1 Prepare the areas to be cemented and bond with theprocedure outlined by the manufacturer of the adhesive.6.2 It is important that all squeezeout be carefully removedfrom the edges

24、 of the specimen.7. Conditioning7.1 Unless special conditioning procedures are agreed uponby the purchaser and the manufacturer the adhesive is ready fortest when it has been applied in accordance with Section 6.8. Procedure8.1 Place the specimen in the grips of the testing machine;take care to alig

25、n the specimen as indicated in Fig. 2.8.2 Apply tensile load at the rate of 270 to 320 kg (600 to700 lb)/min, or the crosshead speed of the testing machine shallbe such that the load can be accurately weighed but shall notexceed 1.27 mm (0.050 in.)/min when the machine is runningidle.8.3 Record the

26、maximum load in pounds carried by thespecimen at failure. Record the percent of cohesion, adhesion,and contact failures.9. Calculation9.1 Cleavage strength is the breaking load, expressed inpounds per inch. If possible, report the results to threesignificant figures.10. Report10.1 Report the followi

27、ng information:10.1.1 Complete identification of the adhesive tested, in-cluding type, source, manufacturers code numbers, form, etc.,10.1.2 Method of preparing test specimens,10.1.3 Average thickness of adhesive layer after formationof the joint, within 0.001 in. Describe the method of obtainingthe

28、 thickness of the adhesive layer. Include procedure, locationof measurements, and range of measurements.10.1.4 Conditioning procedure used,10.1.5 Conditions of testing room,10.1.6 Number of specimens tested,10.1.7 Rate of loading,10.1.8 Maximum, minimum, and average value of cleavagestrength. Option

29、ally, by agreement between the purchaser andthe manufacturer of the adhesive, all individual test results orthe standard deviation, or both, may also be required in thereport.10.1.9 Average value of the percentage of cohesion failure.11. Precision and Bias11.1 The precision and bias statement for th

30、is test methodhas not been determined yet. Archival and round-robin infor-mation is being reviewed, and the results are expected bySeptember 2004.12. Keywords12.1 adhesive bonding; cleavage strengthAUpper gripBPin connecting upper and lower gripsCLower gripDPin for attaching grip to specimenEMetal p

31、iecesFGlue lineFIG. 2 Assembly of Grips and Test Specimen for CleavageStrength Testmm (in.)0.000 (0.000)0.127 (0.005)4.5 (316)6(14)12.7 (12)15 (58)25 (1)32 (114)NOTE 1The 1-in. (25-mm) square surface to be glued shall be groundflat and parallel with the opposite surface.FIG. 3 Metal Piece for Use in

32、 Test SpecimenD1062023ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringeme

33、nt of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or

34、for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views kno

35、wn to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).D1062024