ASTM D2152-2013 Standard Test Method for Adequacy of Fusion of Extruded Poly(Vinyl Chloride) (PVC) Pipe and Molded Fittings by Acetone Immersion《用丙酮浸渍法测定挤压制聚氯乙烯(PVC)管和模制配件溶合度的标准试验方.pdf

1、Designation: D2152 13 An American National StandardStandard Test Method forAdequacy of Fusion of Extruded Poly(Vinyl Chloride) (PVC)Pipe and Molded Fittings by Acetone Immersion1This standard is issued under the fixed designation D2152; the number immediately following the designation indicates the

2、year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Depar

3、tment of Defense.1. Scope*1.1 This test method covers the determination of the ad-equacy of fusion of extruded rigid poly(vinyl chloride) (PVC)pipe and molded fittings as indicated by reaction to immersionin anhydrous acetone.1.2 The values stated in inch-pound units are to be regardedas the standar

4、d except where instruments are calibrated in SIunits.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility o

5、f regulatory limitations prior to use. Specific hazardsstatements are given in Annex A1.2. Referenced Documents2.1 ASTM Standards:2D618 Practice for Conditioning Plastics for Testing3. Significance and Use3.1 This test method is applicable only for distinguishingbetween inadequately fused and adequa

6、tely fused PVC. Thedifference between thermally degraded and adequately fusedPVC cannot be detected by this test method. Acetone immer-sion is not a substitute for burst, impact, or other physical orchemical tests on PVC pipe or fittings and it, therefore, shallnot be used as the only test specifica

7、tion for purchasing of PVCpipe and fittings. This test only detects inadequate fusion anddoes not determine the over-all quality of the PVC pipe orfittings.3.2 This test method is useful in determining whetherinadequate fusion contributed to failure of PVC pipe or fittingsin other physical or chemic

8、al tests, or in service.3.3 This test method is useful in evaluating the adequacy ofPVC fusion obtained in process or materials trials.3.4 This test method determines adequacy of fusion on asingle, relatively small specimen. This test method requires theuse of a hazardous reagent which must be prope

9、rly handled anddisposed. Therefore, this test method may not be cost-effectiveto employ as a routine quality control test.4. Apparatus4.1 ContainerEither individual, sealable containers foreach specimen or one large, airtight container capable ofholding several specimens without touching one another

10、.4.2 Hydrometer and CylinderPrecision hydrometer,graduated in thousandths, with a minimum range of 0.780 to0.790 g/mL and a cylinder large enough to immerse thehydrometer.4.3 ThermometerASTM 12C total immersionthermometer, range from 20C to 102C accurate to 0.2C, orequivalent.5. Reagent5.1 AcetoneAm

11、erican Chemical Society Reagent Grade,having a maximum density of 0.7857 g/mL at 25C.NOTE 1See AnnexA1 for the safety and health precautions to be usedwith acetone.5.2 Prior to conducting the test, check the density of theacetone with a precision hydrometer to determine its dryness.If the density of

12、 the acetone is greater than 0.7890 g/mL at23C, (corresponding to approximately 1 % water by mass (seeFig. X1.1), use fresh acetone or dry the wet acetone with adrying agent. Recheck the density of the fresh or dried acetonebefore using.NOTE 2Wet acetone can be dried by thoroughly agitating it with

13、atleast 15 g of anhydrous calcium sulfate (CaSO4) for each gram of waterpresent.NOTE 3The presence of water in the acetone reduces its sensitivity todifferences in the degree of fusion of rigid poly(vinyl chloride) (PVC). It1This test method is under the jurisdiction of ASTM Committee F17 on Plastic

14、Piping Systems and is the direct responsibility of Subcommittee F17.25 on VinylBased Pipe.Current edition approved May 1, 2013. Published June 2013. Originallyapproved in 1963T. Last previous edition approved in 2010 as D2152 95(2010).DOI: 10.1520/D2152-13.2For referenced ASTM standards, visit the A

15、STM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr

16、Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1is important to dry the acetone properly and conduct the test in a sealedcontainer, because acetone rapidly absorbs moisture from the atmosphere.NOTE 4Round-robin testing between four laboratories showed thattest results are

17、not significantly altered with up to 2 % water by weight inthe acetone.6. Sampling6.1 Specimens shall be taken from individual pipe sections,fittings, or remnant portions of pipe or fittings. Specimens shallbe taken from locations which are to be evaluated for adequacyof fusion, or immediately adjac

18、ent to them.6.2 The number of individual specimens to be tested andtheir locations shall be chosen to be representative of the pipeor fittings being evaluated for adequacy of fusion.7. Test Specimens7.1 Size of SpecimenSpecimen shall be a size that isconvenient to immerse in the test container but n

19、ot less than12in. (13 mm) in height. For small diameter pipe, the specimenshall be a complete circumferential section of the pipe. Forlarge diameter pipe, the specimen shall be a full pipe sectionbut it may be cut into smaller pieces to facilitate testing. Smallmolded parts shall be immersed as a si

20、ngle item. For largemolded fittings, the specimen shall be a complete circumfer-ential section which may be cut into segments before beingimmersed. If the pipe or fitting to be evaluated has fractured orfragmented in other tests or in service, specimens of any shapeand size may be tested.7.2 Specime

21、n PreparationFor pipe having a wall thick-ness greater than 0.125 in. (3.2 mm) the wall thickness shall bereduced to allow testing of the entire wall thickness of thespecimen at six or more intervals around the circumference ofone end of the specimen. The mid-wall surface exposed fortesting shall be

22、 from the interior wall surface to the exteriorwall surface at a minimum of 45 degrees from the square cuton the end of the pipe as shown in Fig. 1. Removal shall beeffected by filing, wet sanding, or other means that willminimize localized heating of the surface. It is not necessary toreduce the wa

23、ll thickness on molded fittings.8. Conditioning8.1 Unless otherwise specified, condition the specimens inairfor1hat236 2C (73.4 6 3.6F) prior to testing. Thespecimens shall not be conditioned in water because of theeffect water has on the acetone. For referee purposes condi-tioning shall be in accor

24、dance with Procedure A of PracticeD618.9. Procedure9.1 Conduct the tests in a Standard Laboratory Atmosphereof 23 6 2C unless otherwise specified.9.2 Place sufficient dried acetone into the container toensure complete immersion of the specimen.9.3 Place the test specimen in the acetone, seal thecont

25、ainer, and do not agitate. Allow specimen to stand im-mersed for 20 min.9.4 After 20 min, remove the specimen from the containerand inspect for signs of attack.9.5 Attack is described as a lifting, raising, or removing, orboth, of any material outside surface, inside surface, ormid-wall, of the spec

26、imen. Swelling or softening of the testspecimen shall not be considered attack.10. Fusion Criteria10.1 At least 50 % attack of the inside, outside, or mid-wallsurface or at least 10 % attack on more than one surface shallbe considered to be indicative of inadequate fusion.11. Report11.1 The report s

27、hall include the following:11.1.1 Complete identification of the PVC compound,11.1.2 Production code number of the pipe or fittings,11.1.3 Nominal dimensions of the pipe or fittings,11.1.4 Observations after 20 min immersion shall be re-ported indicating attack or no attack,11.1.5 The area attacked,

28、 inside, outside, or mid-wall, andthe estimated percentage of that area attacked, and11.1.6 Date of test.12. Precision and Bias12.1 This test method is subjective, based on operatorjudgement. Therefore a statement on precision and bias is notapplicable.13. Keywords13.1 acetone; fusion; pipe; poly(vi

29、nyl chloride); PVCFIG. 1 Specimen PreparationD2152 132ANNEX(Mandatory Information)A1. RECOMMENDED SAFETY PRECAUTIONS TO BE USED WITH ACETONEA1.1 Safety Requirements:A1.1.1 No source of ignition is to be permitted whereacetone is used.A1.1.2 Dispense acetone only from approved safety con-tainers.A1.1

30、.3 Dispose of used acetone, or acetone-impregnatedcloths only in an approved safety waste receptacle.A1.1.4 Avoid prolonged breathing of acetone. Use acetoneonly in a well ventilated area.A1.1.5 Use proper eye protection such as chemical-workers goggles or a face shield when handling acetone.A1.1.6

31、Avoid prolonged exposure to the skin. If prolongedexposure to the skin cannot be avoided, use protective clothing.A1.2 Health Hazards:A1.2.1 Acetone is a mild irritant to eyes, nose and throat butonly minor residual injury will occur if no medical treatment isgiven.A1.2.2 Prolonged or continuous exp

32、osure of acetone to theskin may cause acute or chronic dermatitis. Exposed skin areasshould be washed and dried. Consult a physician if a rashdevelops.A1.3 Fire Hazard:A1.3.1 Acetone is a very flammable liquid having a flashpoint of 18C (0F). Use dry chemical, alcohol foam, orcarbon dioxide to fight

33、 a fire. Use water to keep fire-exposedcontainers cool or to wash away or dilute spills which have notignited.APPENDIX(Nonmandatory Information)X1. DENSITY OF ACETONE VERSUS PERCENT WATER AT FOUR TEMPERATURESFIG. X1.1 Density of Acetone versus Percent Water at Four TemperaturesD2152 133SUMMARY OF CH

34、ANGESCommittee F17 has identified the location of selected changes to this standard since the last issue(D2152 95(2010) that may impact the use of this standard.(1) 7.2 was revised. (2) Fig. 1 was added.ASTM International takes no position respecting the validity of any patent rights asserted in con

35、nection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the respon

36、sible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful

37、consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 1

38、00 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).D2152 134