ASTM D716-1986(2007) Standard Test Methods for Evaluating Mica Pigment《云母颜料的标准试验方法》.pdf

1、Designation: D 716 86 (Reapproved 2007)Standard Test Methods forEvaluating Mica Pigment1This standard is issued under the fixed designation D 716; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number

2、in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 These test methods cover the evaluation of mica pig-ment.1.2 The values stated in SI units are to be regarded as thestandard. The values give

3、n in parentheses are for informationonly.1.3 This standard does not purport to address all of thesafety concerns associated with its use. It is the responsibilityof the user of this standard to establish appropriate safety andhealth practices and determine the applicability of regulatorylimitations

4、prior to use.2. Referenced Documents2.1 ASTM Standards:2D 185 Test Methods for Coarse Particles in PigmentsD 280 Test Methods for Hygroscopic Moisture (and OtherMatter Volatile Under the Test Conditions) in PigmentsE11 Specification for Wire Cloth and Sieves for TestingPurposes3. Significance and Us

5、e3.1 These test methods are used to determine apparentdensity of mica pigments and the grit level. This information issignificant to the user of mica pigments for inclusion incoatings.APPARENT DENSITY4. Apparatus4.1 VolumeterA Scott volumeter or similar apparatusmodified as follows: The screen used

6、shall conform to therequirements of a No. 40 (425-m) sieve as prescribed inSpecification E11. The funnel below the screen shall bereplaced by a conical funnel having a bottom opening 25 mm(1 in.) in diameter. It may be found necessary to replace the topglass baffle with one that is longer to ensure

7、that all of the siftedmica is caught.5. Procedure5.1 Transfer convenient quantities of the mica pigment tothe funnel of the modified volumeter and brush the pigmentthrough the screen with a camel-hair brush until the receiver isslightly more than full. Scrape off the excess and weigh thepigment. Car

8、e must be taken not to jar the apparatus during theprocedure.6. Calculation6.1 Calculate the apparent density of the mica pigment andconvert to pounds per cubic foot.7. Report7.1 Report the mean of three determinations as the apparentdensity of the mica pigment.8. Reproducibility of Results8.1 The m

9、ean of the three determinations should checkwithin 5 %.MOISTURE AND OTHER VOLATILE MATTER9. Procedure9.1 Determine the moisture and other volatile matter inaccordance with Test Methods D 280.GRIT10. Apparatus10.1 Beaker, 600-mL, low-form.10.2 Metal TubingAn L-shape metal tube (Fig. 1) 6.4 mm(14 in.)

10、 in outside diameter with a foot 25 mm (1 in.) in length.The foot of the tube shall be drilled to 4.4 mm (0173 in.) (No.17 drill) in inside diameter for a depth of 12.7 mm (12 in.). Thetube shall be placed in the beaker with the long arm in thevertical position, and the foot of the L parallel to the

11、 bottom ofthe beaker and perpendicular to the radius of the bottom at a1These test methods are under the jurisdiction of ASTM Committee D01 onPaint and Related Coatings, Materials, and Applications and are the directresponsibility of Subcommittee D01.31 on Pigment Specifications.Current edition appr

12、oved Nov. 1, 2007. Published November 2007. Originallyapproved in 1943. Last previous edition approved in 2003 as D 716 86 (2003).2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume informat

13、ion, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.point such that there is about 1.5-mm (116-in.) clearancebetween the tubing and both the bottom and side of the beak

14、er.The center of the foot shall be placed 90 from the lip of thebeaker.11. Procedure11.1 Transfer 10 g of the sample to the 600-mL beaker, add100 mL of water, and swirl the beaker until the mica isdispersed. Insert the metal tubing into the beaker as describedin 10.2 and connect the upper end to a w

15、ater faucet. Regulatethe flow of water by a constant head to a rate of 800 mL/minover the lip of the beaker. When the elutriation has progressedso that the body of the water in the beaker is clear, stop theflow, and lower the water level to prevent spilling.11.2 Swirl the beaker again to bring the r

16、emaining micapigment into suspension and repeat the elutriation procedure asdescribed in 11.1 three times. After final clearing, decant partof the water, and filter the residue. Transfer the paper andresidue to a weighed crucible, and ash slowly, cool, and weigh.12. Calculation12.1 Calculate the per

17、cent grit, G, as follows:G,%5 A 2 B!/S 3 100 (1)where:A = ash, g,B = filter paper ash, g, andS = sample used, g.COARSE PARTICLES13. Procedure13.1 Determine the course particles in accordance with TestMethods D 185.COLOR14. Standard Pigments14.1 Standard Mica Pigment.14.2 Standard Zinc Oxide.15. Proc

18、edure15.1 Compare pastes made by rubbing a standard micapigment and standard zinc oxide, mutually agreed upon by thepurchaser and the seller, in linseed oil with a similar pasteusing the sample to be tested. Rub9gofzinc oxide, and 3 gof mica pigment on a glass plate with a glass muller or rubberspat

19、ula to avoid staining, with 4 mL of bleached linseed oil.Spread the pastes adjacently on a clear glass plate anddetermine the color by viewing the spreadouts on the glass.16. Precision and Bias16.1 Insufficient data are available to develop acceptableprecision and bias statements. The information pr

20、esented inSection 8 (Reproducibility of Results) was obtained in 1943,and no documentation is currently available. The informationwill remain in Section 8.17. Keywords17.1 analysis of; detection in mica pigment; grit; micapigment; pigmentASTM International takes no position respecting the validity o

21、f any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to

22、 revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters.

23、Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is c

24、opyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).FIG. 1 Grit Test ApparatusD 716 86 (2007)2