ASTM D2832-1992(2005) Standard Guide for Determining Volatile and Nonvolatile Content of Paint and Related Coatings《涂料和相关覆层中挥发和不挥发物含量测定的标准指南》.pdf

1、Designation: D 2832 92 (Reapproved 2005)Standard Guide forDetermining Volatile and Nonvolatile Content of Paint andRelated Coatings1This standard is issued under the fixed designation D 2832; the number immediately following the designation indicates the year oforiginal adoption or, in the case of r

2、evision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This guide is intended to aid in the selection of theproper ASTM standard for determining the vo

3、latile and non-volatile content of paint and related coatings.NOTE 1Test methods for determining the composition of the volatilefraction are not covered by this guide.1.2 The standards included are as follows:Type of Coating SectionASTMDesignationAerosol coatings 4.1 D 3062Architectural wall coating

4、s, interior, highperformance4.3 D 1644Asphalt roof coatings 4.4 D 2823Asphalt roof coatings, aluminum-pigmented 4.5 D 2824Bitumens, emulsified 4.6 D 2939Bleached lac varnish 4.7 D 1650Coil coatings 4.8 D 1353D 2697Electrical insulation varnishes 4.9 D 115House paints, gloss D 2697Industrial baking e

5、namel D 2697Lacquers, clear and pigmented 4.11 D 1644D 333Latex paint, exterior D 2697Latex paint, interior D 2697Magnet wire enamels 4.12 D 3288Plastics, coatings for 4.13 D 1644Powder coatings 4.14 D 3451Shellac varnish, orange 4.7 D 1650Silanes, Siloxanes and Silane-Siloxane Blends 4.18 D 5095Sol

6、vent-reducible coatings 4.2 D 2369Traffic paints 4.15 D 2205Varnishes 4.16 D 1644Wall and trim enamels, interior semigloss,solvent-based4.17 D 2697Wall paints, flat 4.10 D 2697Water-reducible coatings 4.2 D 23691.3 The values stated in SI units are to be regarded as thestandard. The values given in

7、parentheses are for informationonly.1.4 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limi

8、tations prior to use.2. Referenced Documents2.1 ASTM Standards:2D115 Test Methods for Testing Solvent Containing Var-nishes Used for Electrical InsulationD 333 Guide for Clear and Pigmented LacquersD 1353 Test Method for Nonvolatile Matter in VolatileSolvents for Use in Paint, Varnish, Lacquer, and

9、RelatedProductsD 1644 Test Methods for Nonvolatile Content of VarnishesD 1650 Test Methods of Sampling and Testing ShellacVarnish3D 2205 Guide for Selection of Tests for Traffic PaintsD 2369 Test Method for Volatile Content of CoatingsD 2697 Test Method for Volume Nonvolatile Matter inClear or Pigme

10、nted CoatingsD 2823 Specification for Asphalt Roof CoatingsD 2824 Specification for Aluminum-Pigmented AsphaltRoof Coatings Non-Fibered, Asbestos Fibered, and Fi-bered without AsbestosD 2939 Test Methods for Testing Emulsified BitumensUsed as Protective CoatingsD 3062 Test Method for Solids Content

11、ofAerosol CoatingsD 3288 Test Method for Magnet-Wire EnamelsD 3451 Practices for Testing Polymeric Powders and Pow-der CoatingsD 5095 Test Method for Determination of the NonvolatileContent in Silanes, Siloxanes and Silane-Siloxane BlendsUsed in Masonry Water Repellant Treatments3. Significance and

12、Use3.1 The nonvolatile content of paint and related coatings isuseful to producers and users and to environmental and healthand safety interests in comparing the coverage of competingproducts and in estimating the volatile organic content.1This guide is under the jurisdiction of ASTM Committee D01 o

13、n Paint andRelated Coatings, Materials, and Applications and is the direct responsibility ofSubcommittee D01.21 on Chemical Analysis of Paints and Paint Materials.Current edition approved Jan. 1, 2005. Published February 2005. Originallyapproved in 1969. Last previous edition approved in 1999 as D 2

14、832 85 (1999).2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Withdrawn.1Copyright ASTM International, 100 B

15、arr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.4. Procedure4.1 Aerosol CoatingsTest Method D 3062 covers thedetermination of solids content (weight %) in aerosol coatings.4.2 Volatile Content of Coatings (Test Method D 2369)This test method covers the determination of

16、 the volatilecontent of coatings. It is considered to be applicable to mostsolvent-reducible and water-reducible paints.4.3 High Performance Interior Architectural Wall Coatings(HIPAC)Determine the nonvolatile content of HIPAC coat-ings in accordance with Test Methods D 1644. Calculate thevolatile c

17、ontent (weight %) by difference.4.3.1 Method A3 h at 105C for paints with nonsolventcomponents that decompose at higher temperature.4.3.2 Method B10 min at 149C for most paints withnonsolvent components that are reasonably stable at 149C.4.4 Asphalt Roof CoatingsDetermine the nonvolatile con-tent (w

18、eight %) of asphalt roof coatings of brushing or spray-ing consistency in accordance with the Physical RequirementsConsistency section of Specification D 2823.4.5 Aluminum-Pigmented Asphalt Roof CoatingsThenonvolatile content (weight %) of asphalt-based aluminumroof coatings suitable for application

19、 to roofing or masonrysurfaces by brush or spray is determined in accordance with thePhysical Requirements Consistency section of SpecificationD 2824.4.6 Emulsified Bitumens Used as Protective CoatingsSection 8 of Test Methods D 2939 contains a method fordetermining residue by evaporation (weight %)

20、 of emulsifiedbitumens used in relatively thick films as protective coatingsfor metals and built-up roofs.4.7 Shellac VarnishDetermine the nonvolatile matter inorange shellac and bleached lac varnishes in accordance withSections on Drying Time Procedure and Nonvolatile MatterMaterials and Procedure

21、sections of Methods D 1650.4.8 Coil CoatingsAlthough stated to be for solvents,determine the nonvolatile matter (weight %) in accordancewith Test Method D 1353. Determine volume solids in accor-dance with Test Method D 2697.4.9 Electrical Insulation Varnishes:4.9.1 Sections on Procedure, Report, Sig

22、nificance and Use,Apparatus, and Procedure of Test Methods D115on nonvola-tile matter by weight, are applicable to the following classifi-cations of varnishes used for electrical insulation: alcohol-soluble varnishes, oxidizing air-drying varnishes,thermosetting varnishes, oxidizing baking varnishes

23、, air-dryingasphaltic varnishes, silicone varnishes, and thermo-settinglaminating varnishes.4.9.2 Determine nonvolatile matter in electrical insulatingvarnishes intended for electrical equipment operating at 180Cand above in accordance with Test Methods D115except thatthe temperature used shall be 1

24、35 6 3C (275 6 5.5F) or ata temperature agreed upon between the producer and the user.4.10 Volume Nonvolatile Matter in Clear or PigmentedCoatings (Test Method D 2697) This test method is appli-cable to the determination of the volume nonvolatile matter ofcoatings. A gloss enamel, a flat wall paint,

25、 a gloss house paint,an industrial baking enamel, an interior latex paint, and anexterior latex paint included in formal collaborative studies ofthis test method.4.11 Lacquer CoatingsDetermine the nonvolatile contentof clear and pigmented lacquers as described in Test MethodsD 1644. As an additional

26、 requirement, the specimen shall bereheated and reweighed until the weight is constant to within 1mg. Method A of Test Methods D 1644 is preferred sinceMethod B is potentially dangerous when used with lacquers.4.12 Magnet Wire EnamelsThe Determined Solids andStack Loss sections of Test Method D 3288

27、 cover the determi-nation of nonvolatile content (weight %) in magnet wireenamels.4.13 Coatings for PlasticsDetermine nonvolatile matterin clear and pigmented coatings designed for use on rigid orsemirigid plastic substrates in accordance with Test MethodsD 1644.4.14 Polymeric Powders and Powder Coa

28、tingsDeterminenonvolatile content (weight %) in accordance with the Accel-erated Storage Stability section of Coating Powder Propertiesof Practices D 3451. Determine volatile content at baking orfusion temperature in accordance with the Cured Weight Lossfor Thermosetting Coating Powders section of P

29、racticesD 3451.4.15 Traffc PaintsDetermine the nonvolatile content oftraffic paints, ready-mixed, of spraying consistency of thepremix, drop-in, or combination type in accordance with TestMethods D 1644, and state any necessary larger specimen sizefor beaded paint. Either of the two methods can be u

30、sed asfollows:4.15.1 Method A3 h at 105C for paints with nonsolventcomponents that decompose at higher temperature.4.15.2 Method B10 min at 149C for most paints withnonsolvent components that are reasonably stable at 149C.4.16 VarnishesNonvolatile content (weight %) of var-nishes is determined using

31、 Test Methods D 1644. These testmethods may give high results due either to incompleteelimination of volatile matter or to absorption of oxygen byoxidizing-type varnishes.4.17 Solvent-Based Interior Semigloss Wall and TrimEnamelsUse Test Method D 2369 to determine volatilecontent. Volume nonvolatile

32、 matter is determined in accor-dance with Test Method D 2697.4.18 Silanes, Siloxanes and Silane-Siloxane Blends Used inMasonry Water Repellant TreatmentsTest Method D 5095describes a procedure for the determination of the nonvolatilecontent of silanes, siloxanes and the blended silane-siloxanemateri

33、als used in masonry water repellent treatments and isapplicable to both solvent and water-borne materials.5. Precision5.1 Some of the referenced ASTM standards have precisionlimits. Reference to the individual standards for precisionstatements is recommended.6. Keywords6.1 nonvolatile content of pai

34、nts and related coatings; vola-tile content of paints and related coatingsD 2832 92 (2005)2ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination

35、 of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdraw

36、n. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your co

37、mments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).D 2832 92 (2005)3