ASTM D2919-2001(2014) Standard Test Method for Determining Durability of Adhesive Joints Stressed in Shear by Tension Loading《用拉力负荷法测定胶粘接缝耐剪切的标准试验方法》.pdf

1、Designation: D2919 01 (Reapproved 2014)Standard Test Method forDetermining Durability of Adhesive Joints Stressed in Shearby Tension Loading1This standard is issued under the fixed designation D2919; the number immediately following the designation indicates the year oforiginal adoption or, in the c

2、ase of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope1.1 Thi

3、s test method covers data for assessing the durabilityof adhesive lap-shear joints while stressed in contact with air,air in equilibrium with certain solutions, water, aqueoussolutions, or other environments at various temperatures.1.2 This standard does not purport to address all of thesafety conce

4、rns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use. Specific precau-tionary statements are given in 7.4.1.3 The values stated in SI un

5、its are considered to be thestandard. The values in parentheses are for information only.2. Referenced Documents2.1 ASTM Standards:2D907 Terminology of AdhesivesD1002 Test Method for Apparent Shear Strength of Single-Lap-Joint Adhesively Bonded Metal Specimens by Ten-sion Loading (Metal-to-Metal)D18

6、28 Practice for Atmospheric Exposure of Adhesive-Bonded Joints and StructuresD2294 Test Method for Creep Properties of Adhesives inShear by Tension Loading (Metal-to-Metal)D3165 Test Method for Strength Properties of Adhesives inShear by Tension Loading of Single-Lap-Joint LaminatedAssembliesE4 Prac

7、tices for Force Verification of Testing Machines2.2 ASTM Adjuncts:Durability Test Apparatus Drawings33. Terminology3.1 DefinitionsDefinitions of terms in this test methodmay be found in Terminology D907.4. Significance and Use4.1 The combination of stress and moisture decreases thedurability of most

8、 adhesive joints. Stresses in the presence ofwater or water vapor may cause some adhesive joints to fail atsome small fraction of the stress required to break the dry joint.The time to failure for a given adhesive joint generallydecreases with increasing stress, temperature, and relativehumidity.4.2

9、 This test method may be used as an accelerated screen-ing test for assessing the durability of adhesive joints. It may beused to measure durability of adhesive joints exposed outdoorsor to environmental conditions experienced by adhesive jointsin service. The tests may also be used to determine the

10、 effectsof various surface preparations or substrates on durabilities ofadhesive joints.4.3 The durability performance of various adhesives may becompared by using this test method under uniform sets ofconditions. To assess the overall durability of a given adhesive,lap-shear joints should be tested

11、 under a range of stress,relative humidity, and temperature. For a specific end use itmay be possible to obtain the needed durability data using onlyone set of test conditions.5. Apparatus5.1 Fixture, as shown in Fig. 1,3is required for this testmethod, although a fixture such as described in Test M

12、ethodD2294 may also be suitable for the performance of this test.1This test method is under the jurisdiction of ASTM Committee D14 onAdhesives and is the direct responsibility of Subcommittee D14.80 on MetalBonding Adhesives.Current edition approved March 1, 2014. Published March 2014. Originallyapp

13、roved in 1971. Last previous edition approved in 2007 as D2919 01 (2007).DOI: 10.1520/D2919-01R14.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Docu

14、ment Summary page onthe ASTM website.3Detailed working drawings for the construction of the durability test apparatusare available from ASTM International Headquarters. Order Adjunct No.ADJD2919. Original adjunct produced in 1980.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West

15、 Conshohocken, PA 19428-2959. United States15.2 Testing Machine, or other suitable machine capable ofapplying measured compressive loads. Force measurementshave an accuracy of 61 % of any reading when calibrated incompliance with Practices E4 requirements. Machine that isequipped with a suitable loa

16、ding base as shown in Fig. 1, shallbe used as a loading mechanism.5.3 Outdoor Weathering Racks (Standard) are recom-mended (Practice D1828), but any stable frame may be used(for example, galvanized pipe or painted steel channel). Noother special apparatus is required for outdoor tests.6. Test Specim

17、ens6.1 The successful use of this test method depends onpreparing good quality lap-shear joints. The test joints must beprepared carefully in accordance with the adhesive manufac-turers directions or in accordance with some other specifiedset of conditions agreed upon between the manufacturer andthe

18、 purchaser. It is recommended that the test joints beprepared in accordance with Test Method D1002, except thatthe dimensions of the test specimens shall be as shown in Fig.2.FIG. 1 Durability Test ApparatusD2919 01 (2014)26.2 If the fixture in Fig. 1 is used, test specimens of thedimensions shown i

19、n Fig. 2 must be used. If the fixturedescribed in Test Method D2294 is used, the test specimendescribed in that test method must be used.6.3 If it is desired to use test specimens of thickness oroverlap different from that recommended in this test method orin Test Method D2294, the guidelines set fo

20、rth in Note 2 andNote 3 of Test Method D1002, regarding permissible testspecimen dimensions with respect to thickness and overlap,shall be followed. Test specimen size, of course, must alwaysbe compatible with the appropriate fixture.6.4 An alternative test specimen may be used in accordancewith Tes

21、t Method D3165 with the exception that the lengthwisedimension must be compatible with the test specimen shown inFig. 2.7. Procedure7.1 Test six specimens to destruction at 23.0 6 1C (73.4 61.8F) and 50 6 2 % relative humidity in accordance with TestMethod D1002, after conditioning in this environme

22、nt for notless than 40 h, unless otherwise specified. Compute and recordthe maximum, minimum, and average value of the failingstress.7.2 Place a minimum of six test specimens for each testenvironment in test fixtures. To load each assembled testfixture, after being certain that the safety end plate

23、shields arefirmly in place, place the fixture, supported by the loading base,in the loading machine and apply approximately 1 % of thedesired stress to the springs. Tighten the grip bolts to 0.45 to0.56 Nm (40 to 50 lbfin.) torque, then apply the remainder ofthe stress. Turn the locking nuts directl

24、y under the lower springlocators until they are finger tight. Release the load applied bythe machine and remove the loaded fixture (see 7.4). Do notexceed the average initial failing stress determined above.7.3 Expose the stressed test specimens to one of the stan-dard test environments specified in

25、 Table 1. Expose the testspecimens to the environment in an attitude such that thecondensate of the environment drains properly. Thereforeexpose the test specimens with the edges horizontal and withthe test specimen width perpendicular to the horizontal plane.Make periodic observations of their cond

26、ition and record thelength of time to failure for each test specimen and the averagefor the six test specimens (or more) to the test environment.7.4 Exercise extreme caution to ensure that loading of thefixture and handling of a loaded fixture be carried out in a safemanner, particularly that parts

27、of the body be maintained at asafe distance from the test specimen in case it should acciden-tally break during these operations.8. Report8.1 Report the following information:8.1.1 Complete identification of the adhesive tested, includ-ing type, source, date manufactured, manufacturers codenumbers,

28、form, etc.8.1.2 Complete identification of the adherends used, includ-ing composition, thickness, and temper for metals.8.1.3 Surface preparation, application, and bonding condi-tions used in preparing the test specimens.8.1.4 Length of overlap used and bondline thickness.8.1.5 Maximum, minimum, and

29、 average failing stress of thejoints tested in accordance with Section 7.8.1.6 Number of specimens tested and conditions of testing,including applied stress in megapascals (pounds force persquare inch); test environment number from Table 1, includinga complete description of any special test environ

30、ments;location of outdoor test site and time of year, high, low andaverage temperatures, and sun exposure.FIG. 2 Form and Dimensions of Test SpecimenTABLE 1 Standard Test EnvironmentsTest EnvironmentNumberTemperatureAMoisture ConditionsB1 23C (73.4F) immersed in distilled or de-ionized water2 23C (7

31、3.4F) 50 % RH (relative humidity)3 23C (73.4F) 15 % RH4 35C (95F) 90 % RH5 35C (95F) 100 % RH6 50C (122F) 90 % RH7 50C (122F) 100 % RH8 35C (95F) 5 % salt fog9 ambient (outdoors) ambient (outdoors)10 other (specify) other, including aqueous so-lutions or nonaqueous liq-uids (specify)AThe tolerance f

32、or test temperature shall be 1C or 1.8F for environments 1 to8.BThe moisture condition may be provided by controlling the relative humidity of abox, room, or other chamber by any convenient means.D2919 01 (2014)38.1.7 Maximum, minimum, and average length of time tofailure of the stressed test specim

33、ens exposed to the environ-ment. Test specimens not broken at termination of the testshould be recorded but not included in the average.9. Precision and Bias9.1 Precision and Bias for this test is being determined andwill be available by September 2010.10. Keywords10.1 adhesive joint; durability; ex

34、posure; moisture; shear;stress; tensionASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the

35、riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of

36、this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldma

37、ke your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).D2919 01 (2014)4