ASTM D3258-2004(2014) Standard Test Method for Porosity of White or Near White Paint Films by Staining《采用染色法测定白色或近白色涂料薄膜孔隙度的标准试验方法》.pdf

1、Designation: D3258 04 (Reapproved 2014)Standard Test Method forPorosity of White or Near White Paint Films by Staining1This standard is issued under the fixed designation D3258; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the y

2、ear of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers the determination of the poros-ity of a white or near white mineral spirits insoluble p

3、aint filmto indicate the degree to which a subsequent coat will pen-etrate.1.2 The texture of the film can affect cleanup that willinfluence the results of the test. A stain applied to a high-hidingpaint will not lower the reflectance as much as the same stainapplied to a low-hiding paint of equal p

4、orosity. These pointsmust be considered in comparing different paints.1.3 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.1.4 This standard does not purport to address all of thesafety concerns, if any, associated with its use.

5、 It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2E1347 Test Method for Color and Color-Difference Mea-surement by Tristimulus

6、Colorimetry3. Summary of Test Method3.1 The test paint is applied to a nonporous surface, airdried, then measured for reflectance. A special colored pen-etrating medium is applied, the excess removed in a specifiedmanner, and reflectance measured again. The difference be-tween the two readings indic

7、ates the degree of porosity; thesmaller the difference, the lower the porosity of the film and thegreater its ability to resist penetration.4. Apparatus and Materials4.1 Film Applicator, 150 mm (6 in.) wide with a clearanceof 300 m (12 mils).4.2 Film Applicator, 140 mm (512 in.) wide with a clearanc

8、eof 250 m (10 mils).4.3 Reflectometer, meeting the requirements of Test MethodE1347.4.4 Vacuum Drawdown Plate.4.5 Camelhair Brush (approximately 13 mm (12 in.) wide).4.6 Plastic Wash Bottle, containing odorless mineral spirits(about 500 mL (16 oz).4.7 Test PanelSmooth nonporous panel such as sealedw

9、hite, cardboard chart, or white plastic sheet.4.8 Penetrating MediumA composition of pigment anddark-colored dye dispersed in organic liquid vehicle.4.9 Filter Paper.5. Procedure5.1 Place the test panel on the vacuum plate and apply thepaint under test with the 30-m (12-mil) clearance drawdownblade.

10、 Remove the test panel from the vacuum plate and air dry48 h under standard conditions of 23 6 2C (73 6 3.5F) and50 6 5 % relative humidity.5.2 Determine the percent reflectance of the dry film usingthe green filter on the reflectometer. When making this reading,back up the panel with a flat rigid o

11、paque object and mark thearea on which the reading was made.5.3 Place the panel containing the dry paint film on thevacuum plate. Using the 25-m (10-mil) clearance blade, applythe penetrating medium over the test paint, covering the areamarked as above and drawing the applicator blade in the samedir

12、ection as before.5.4 After 5 min 6 15 s wash off excess penetrating medium.To do this, hold the panel vertically and remove the mediumusing the camelhair brush wet with odorless mineral spirits.Repeat the process until most of the excess is removed. Thencontinue to remove more of the excess by apply

13、ing mineralspirits directly from the wash bottle to the area above the stainso that it flows across the stained area. Pause to observe thebead that forms at the bottom of the panel. If the bead is not1This test method is under the jurisdiction of ASTM Committee D01 on Paintand Related Coatings, Mate

14、rials, and Applications and is the direct responsibility ofSubcommittee D01.42 on Architectural Coatings.Current edition approved Dec. 1, 2014. Published December 2014. Originallyapproved in 1973. Last previous edition approved in 2010 as D3258 04 (2010)1.DOI: 10.1520/D3258-04R10R14.2For referenced

15、ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Consho

16、hocken, PA 19428-2959. United States1clear, continue washing with mineral spirits until the bead isessentially clear. Test with filter paper to be sure no dyeremains in the bead.5.5 Hang the panel in a vertical position and air dry for 3 h.As before, read the percent reflectance over the same area o

17、fthe panel with the same flat rigid opaque object behind thepanel.6. Report6.1 Report the difference between the percent reflectance ofthe untested film and that of the penetrated film.7. Precision7.1 On the basis of an interlaboratory study of this testmethod in which one operator in each of ten la

18、boratories testedpaint films of two nominally different levels of porosity, thewithin-laboratory and between-laboratories standard devia-tions were found to be:Nominal Differencein Reflectance, %Standard DeviationsWithin-Laboratory Between-Laboratories7 0.27 1.2635 0.60 4.22Based on these standard d

19、eviations the following criteriashould be used to judge the precision or results at the 95 %confidence level:7.1.1 RepeatabilityDuplicate results, obtained by a singleoperator, should be considered suspect if they differ by morethan 0.8 % relative for difference in reflectance levels of about7 % and

20、 more than 1.8 % relative for difference in reflectancelevels of about 35 %.7.1.2 ReproducibilityTwo results, each the mean of dupli-cate measurements obtained in different laboratories should beconsidered suspect if they differ by more than 4.0 % relativefor difference in reflectance levels of abou

21、t 7 % and 14 %relative for difference in reflectance levels of about 35 %.8. Keywords8.1 film porosity; porosity; resistancepenetration (intopaint films)ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. U

22、sers of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed eve

23、ry five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible techn

24、ical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohock

25、en, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 04 (2014)2