ASTM D3430-1995(2002) Standard Test Method for Clarity and Yellowness of Liquid Water-Based Clear Floor Polishes《液态水基透明地板抛光剂透明度及泛黄度的标准试验方法》.pdf

1、Designation: D 3430 95 (Reapproved 2002)Standard Test Method forClarity and Yellowness of Liquid Water-Based Clear FloorPolishes1This standard is issued under the fixed designation D 3430; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revi

2、sion, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers measurement of the degree ofclarity and depth of yellowness of water-based

3、clear floorpolishes.1.2 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to

4、 use.2. Terminology2.1 Definition:2.1.1 absorbancethe negative logarithm, to the base 10,of the ratio of the radiant power transmitted through a sampleto the radiant power incident upon the sample. Hence, as theclarity decreases or the depth of the yellowness increases theabsorbance increases.3. Sig

5、nificance and Use3.1 The laboratory technique described in this test method isused to evaluate the clarity and yellowness of water-based“clear” floor polishes for product development or qualitycontrol purposes.4. Apparatus4.1 Colorimeter,2equipped with cylindrical 20-mm matchedcells. (If 20-mm cells

6、 are not available, 10-mm matched cellsmay be substituted.)4.2 Any colorimeter having equivalent resolution and sen-sitivity may be used with the appropriate matched cells.5. Sampling5.1 The sample shall be representative of the material to betested and the portion used for the test shall be represe

7、ntativeof the sample itself.5.2 Calibration SampleAny emulsion polymer that visu-ally exhibits little or no yellowness, selected for dilution (see6.1).6. Preparation of Correction Graph6.1 Prepare minimum of five dilutions of the calibrationsample with distilled water so that absorbance reading betw

8、een0.00 and 0.16 at 500 nm are obtained. Measure the absorbanceat both 500 nm and 400 nm for each dilution (see Section 7).6.2 Plot the absorbance at 500 nm versus that at 400 nm andfit a straight line through the resulting points starting from theorigin (see Fig. 1).6.3 It is necessary to prepare a

9、 correction graph only oncefor a given instrument and set of cells.7. Procedure7.1 Adjustment of ColorimeterSet the colorimeter at 500nm and at 0 absorbance with distilled water as a blank in oneof the matched cells.7.2 AbsorbanceFill the companion cell with sample andplace in the cell holder. Read

10、and record the absorbance. Thisreading is indicative of the degree of turbidity.7.3 Adjustment of ColorimeterReset the colorimeter at400 nm and at 0 absorbance with distilled water as a blank inone of the matched cells.7.4 AbsorbanceRead and record the absorbance of thesample. This reading is indica

11、tive of the uncorrected yellow-ness.7.5 CorrectionThe corrected value for yellowness is therecorded absorbance from 7.2 corrected to 400 nm from thecorrection graph. Subtract this value from the total absorbanceat 400 nm, 7.4. The difference is the absorbance due toyellowness.8. Report8.1 Report the

12、 absorbance, indicating the cell size, to thenearest 0.01 unit based on duplicate determinations.9. Precision and Bias9.1 PrecisionDuplicate determinations obtained on thesame colorimeter that agree within 60.02 units are acceptablefor averaging. Results are comparable only when the same type1This t

13、est method is under the jurisdiction of ASTM Committee D21 onPolishes, and is the direct responsibility of Subcommittee D21.03 on Chemical andPhysical Testing.Current edition approved May 15, 1995. Published July 1995. Originallypublished as D 3430 75. Last previous edition D 3430 75 (1989).2Spectro

14、nic 70 has been found satisfactory and is available from Milton-Roy,820 Linden Ave., Rochester, NY.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.colorimeter and the same size cells are used.9.2 BiasThis test method has no bias beca

15、use the resultsdeveloped are defined only in terms of this test method.10. Keywords10.1 floor polishes; polishesASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advis

16、ed that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either r

17、eapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If

18、you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individu

19、al reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).NOTE 1Three polymers gave identical results.FIG. 1 Correction GraphD 3430 95 (2002)2