ASTM D3705-1986(2009) Standard Test Method for Misting Properties of Lubricating Fluids《润滑液雾状属性的标准试验方法》.pdf

1、Designation: D 3705 86 (Reapproved 2009)An American National StandardStandard Test Method forMisting Properties of Lubricating Fluids1This standard is issued under the fixed designation D 3705; the number immediately following the designation indicates the year oforiginal adoption or, in the case of

2、 revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers the determination of the mistingcharacteristics of lubricating fluids.N

3、OTE 1This test method should not be used to evaluate fluidscontaining solid additives such as graphite.1.2 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and h

4、ealth practices and determine the applica-bility of regulatory limitations prior to use. For specificwarning statements, see Sections 6 and 7.2. Referenced Documents2.1 ASTM Standards:2D91 Test Method for Precipitation Number of LubricatingOilsD 235 Specification for Mineral Spirits (Petroleum Spiri

5、ts)(Hydrocarbon Dry Cleaning Solvent)3. Summary of Test Method3.1 The mist generator is charged with oil and installed inthe mist system. The unit is operated for 19 h; the mistgenerator, line condensate bottles, and reclassified oil collectorare weighed before and after the test. The output from th

6、egenerator and percentages of reclassified oil, line condensate,and stray mist are determined from changes in weight.NOTE 2Line condensate is the commonly accepted term used todescribe the oil that coalesces in the mist distribution lines. In this test, theoil that coalesces in the 38-mm (112-in.) t

7、ubing and the diagonal 19-mm(34-in.) tubing is collected and weighed as line condensate. Oil thatcoalesces in the vertical 19-mm (34-in.) tubing becomes part of thereclassified oil.4. Significance and Use4.1 This test provides a guide for evaluating the mistingcharacteristics of oils for use in indu

8、strial mist lubricationsystems. The degree of correlation between this test and serviceperformance has not been fully determined.5. Apparatus5.1 The basic system consists of the following:5.1.1 Oil Mist Generator,3,4with specialASTM-ASLE misthead assembly.5.1.2 Air Temperature Regulator.4,55.1.3 Mis

9、t Distribution Manifold, as shown in Fig. 1.5.1.4 Mist Reclassifier Fitting, as shown in Fig. 2.5.1.5 Reclassified Oil Collector, as shown in Fig. 3.5.2 Balance, 20-kg capacity open pan, with 1-g sensitivity.5.3 Air Supply, from a source capable of maintaining an airflow rate up to 2 dm3/s. The air

10、should be dry, oil-free, andfiltered through a 1-m filter.NOTE 3The oil mist generator head and mist reclassifier fitting areavailable from the Alemite Co. Orders should specify Special ASTM-ASLE mist head and reclassifier fitting.6. Reagents6.1 Stoddard Solvent, as specified in Specification D 235(

11、Type 1). (WarningFlammable.)6.2 Precipitation Naphtha, as specified in Test MethodD91.(WarningFlammable.)7. Preparation of Apparatus7.1 Thorough cleaning of the apparatus with solvent isrequired prior to initiating a test on a new oil. For a duplicatetest on the same oil, the mist generator should b

12、e thoroughlydrained but the apparatus need not be cleaned with solvent.7.2 Drain the oil thoroughly and rinse the generator withStoddard solvent. (WarningCombustible. Vapor harmful.)7.3 Charge the generator with 2 L of clean Stoddard solventand mist the Stoddard solvent through the manifold for 30 m

13、in.(WarningDo not use the air heater while misting theStoddard solvent.)1This test method is under the jurisdiction of ASTM Committee D02 onPetroleum Products and Lubricants and is the direct responsibility of SubcommitteeD02.L0.02 on Machinery Lubricants.Current edition approved April 15, 2009. Pub

14、lished July 2009. Originallyapproved in 1978. Last previous edition approved in 2003 as D 370586(2003)1.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standard

15、s Document Summary page onthe ASTM website.3The sole source of supply of Alemite No. 383802-4 known to the committee atthis time isAlemite Co., Stewart Warner, 1826 West Diversey Parkway, Chicago, IL60614.4If you are aware of alternative suppliers, please provide this information toASTM Internationa

16、l Headquarters. Your comments will receive careful consider-ation at a meeting of the responsible technical committee1, which you may attend.5The sole source of supply of Alemite thermo-aire unit No. 383808-A4 knownto the committee at this time is Alemite Co., Stewart Warner, 1826 West DiverseyParkw

17、ay, Chicago, IL 60614.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.7.4 Drain the Stoddard solvent from the generator, rinse thegenerator with naphtha, and blow dry with compressed air.(WarningExtremely flammable. Harmful if inhale

18、d. Vaporsmay cause flash fire.)7.5 Disconnect the mist head and remove the oil adjustmentscrew; rinse the head and screw with naphtha and blow dry.7.6 Remove the reclassifier fitting and rinse it with naphtha;examine the orifices for deposits or buildup. If necessary, theorifices may be cleaned with

19、 a fine pipe cleaner.8. Procedure8.1 Break-In Period:8.1.1 Charge the mist generator with 4 6 0.1 L of test oil.Assemble the test apparatus.8.1.2 Turn the oil flow adjusting screw clockwise to a fullyclosed position and then open the screw by turning it counter-clockwise to a full open position.8.1.

20、3 Open the air regulator until a pressure of 37 millibars(37 KPa) is obtained on the manifold gage.8.1.4 Activate the oil heater and inlet air heater and adjustboth to 40 6 1C.8.1.5 Allow the unit to run for1htostabilize.NOTE 4The full open position for the oil flow adjusting screw, that is,the posi

21、tion beyond which further opening of the adjusting screw does notincrease oil output from the mist generator, should be determined for eachmist test unit. The full open position on most test units is attained byturning the adjusting screw counterclockwise 2-12 turns from the fullyclosed position.8.2

22、 Test Start-Up:8.2.1 Following the 1-h break-in, deactivate the air and oilheaters and turn off the air supply.8.2.2 Disconnect and weigh the mist generator (W1) andinstall clean, tared line condensate bottles (LC1) and reclassi-fied oil collector (RC1).8.2.3 Reassemble the apparatus. Turn on the in

23、let air andactivate the air and oil heaters to start the test.8.2.4 Record the air flow rate in dm3/s.8.2.5 Check the inlet air temperature, oil reservoir tempera-ture and manifold temperature. Make adjustments, if necessary,30 min after starting the test to bring the manifold pressure to37 6 1 mill

24、ibars, (3.7 6 0.1 KPa) and the inlet air temperatureto 40C.MIST MANIFOLD (12)34 in. Fig 3 C 45 deg Fig. ellProposed ASTM Bill of Materials (13)34 in. Fig 3 C 90 deg Fig ell(1) 112 C 3 112 in. MPT union (14)34 C 312 in. F adapter(2) 112 in. Copper tubing, 3 in. Long (15)12 in. Reclassifier fitting 12

25、 holes(3) 112 in. C 3 C Return bend (16) Collector bottles(4) 112 in. C Union (17) Thermometer(5) 112 334 3 112 in. C 3 C 3 C tee (18) Pressure regulator with gage(6) 112 in. C 45 deg Fig. ell (straight ell) (19) Flow meter(7)34 in. Fig 3 MPT adapter (20) Pressure gage(8) 112 3 112 334 in. C 3 C 3 C

26、 tee (21) Air filter(9)34 in. C 45 deg Fig. ell (22) Oil mist head assembly special ASTM-ASLE(10) 112 in. Fig. 334 in. C extended bushing (23) Oil mist generator(11)34 in. C Union (24) Thermo-aire unitFIG. 1 Mist Test ApparatusD 3705 86 (2009)28.2.6 At the end of the 19-h test, deactivate the heater

27、s andturn off the air supply. Disconnect and weigh the mist generator(W2), line condensate bottles (LC2), and reclassified oil collec-tor ( RC2) within 15 min.FIG. 2 Mist Reclassifier FittingFIG. 3 Reclassified Oil CollectorD 3705 86 (2009)39. Calculation and Report9.1 Calculate and report the oil o

28、utput from the mistgenerator after break-in in grams per hour as follows:oil output 5W12 W219(1)where:W1= weight of the mist generator at the start of the test, g,andW2= weight of the mist generator after 19 h, g.9.2 Calculate and report the percent of reclassified oil asfollows:% reclassified oil 5

29、RC22 RC1W12 W23 100 (2)where:RC1= weight of the reclassified oil collector at the start ofthe test, g,RC2= weight of the reclassified oil collector at the end ofthe test, g.9.3 Calculate and report the percent of line condensate asfollows:% line condensate 5LC22 LC1W12 W23 100 (3)where:LC1= weight o

30、f the line condensate bottles at the start ofthe test, andLC2= weight of the line condensate bottles at the end ofthe test.9.4 Calculate and report the percent of stray mist as follows:% stray mist 5 1002% reclassified oil 1 % line condensate!(4)NOTE 5For design considerations, it may be desirable t

31、o calculate theoutput oil mist density or effective oil mist density, or both. Thesecalculations are made as follows:Oil output mist density, mg/m35oil output g/h!31000air flow rate dm3/s!33.6(5)Effective oil mist density, mg/m3(6)5reclassified oil RC22 RC1! 3 1000air flow rate dm3/s! 3 68.410. Prec

32、ision and Bias610.1 The precision of this test method as determined bystatistical examination of interlaboratory results is as follows:10.1.1 RepeatabilityThe difference between successiveresults obtained by the same operator with the same apparatusunder constant operating conditions on identical te

33、st materialwould, in the long run, in the normal and correct operation ofthe test method, exceed the following values only in one casein twenty:Oil output, g/h 8 %Percent reclassified oil 6 %Percent line condensate 22 %10.1.2 ReproducibilityThe difference between two singleand independent results ob

34、tained by different operators work-ing in different laboratories on identical test material would, inthe long run, exceed the following values only in one case intwenty:Oil output, g/h 41 %Percent reclassified oil 57 %Percent line condensate 73 %10.2 BiasThe procedure in this test method has no bias

35、because the values of Oil Output, percent Reclassified Oil, andpercent Line Condensate can be defined only in terms of a testmethod.NOTE 6The percent of stray mist is obtained by calculation ratherthan by a direct determination. Therefore, no precision data are includedfor percent of stray mist.APPE

36、NDIX(Nonmandatory Information)X1. METHOD FOR HANDLING STRAY MISTX1.1 Fig. X1.1 shows a container that has been foundsatisfactory for handling the stray mist generated during thetest.X1.2 The stray mist is sucked from the container through afilter-coalescer unit which removes approximately 99 % of th

37、eoil. The suction is obtained using an air jet exhauster; theexhaust can be fed into the laboratory exhaust system.4,7X1.3 The exhaust system should be started after a mist testhas been initiated and must not affect the manifold pressure. Ifa decrease in manifold pressure is noted when the exhaustsy

38、stem is started, the vent hole should be enlarged.X1.4 The baffles must be included as an integral part of thecontainer to prevent air flow directly across the top of thereclassified oil collector.6Supporting data (derived from results of the cooperative tests on oils L-II-3-M,N, O, P, Q, R, S, T, U

39、, V, W, and X) have been filed at ASTM InternationalHeadquarters and may be obtained by requesting Research Report RR: D02-1056.7The sole source of supply of the Figure 431 1-in. jet exhauster known to thecommittee at this time is Schulte and Koerting, State Rd and Traylor Ave.,Cornwells Heights, PA

40、 19020.D 3705 86 (2009)4ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringe

41、ment of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard o

42、r for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views k

43、nown to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).FIG. X1.1 Apparatus For Removing Stray MistD 3705 86 (2009)5