ASTM D3732-1982(2017) Standard Practice for Reporting Cure Times of Ultraviolet-Cured Coatings《报告紫外线固化涂层固化时间的标准实施规程》.pdf

1、Designation: D3732 82 (Reapproved 2017)Standard Practice forReporting Cure Times of Ultraviolet-Cured Coatings1This standard is issued under the fixed designation D3732; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of l

2、ast revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S. Department of Defense.1. Scope1.1 This practice applies to all coat

3、ings cured by ultravioletenergy.1.2 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of

4、 this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.1.4 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Prin

5、ciples for theDevelopment of International Standards, Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:2D658 Test Method for Abrasion Resistance of OrganicCoatings by Air Blast Abrasive (Withdrawn

6、1996)3D968 Test Methods for Abrasion Resistance of OrganicCoatings by Falling AbrasiveD1474 Test Methods for Indentation Hardness of OrganicCoatingsD2197 Test Method for Adhesion of Organic Coatings byScrape AdhesionD2336 Guide for Specifying Factory Applied Wood Coat-ings (Withdrawn 2008)3D2793 Tes

7、t Method for Block Resistance of Organic Coat-ings on Wood Panel SubstratesD2794 Test Method for Resistance of Organic Coatings tothe Effects of Rapid Deformation (Impact)D3023 Practice for Determination of Resistance of Factory-Applied Coatings on Wood Products to Stains and Re-agentsD3281 Test Met

8、hod for Formability of Attached OrganicCoatings with Impact-Wedge BendApparatus (Withdrawn1995)3D3359 Test Methods for Rating Adhesion by Tape TestD3363 Test Method for Film Hardness by Pencil Test3. Terminology3.1 Definitions of Terms Specific to This Standard:3.1.1 cure, nthe condition of a coatin

9、g after conversion tothe final state of cure as measured by tests generally related toend-use performance and mutually agreeable to supplier andpurchaser.3.1.2 ultraviolet curing, nconversion of a coating from itsapplication state to its final use state by means of a mechanisminitiated by ultraviole

10、t radiation generated by equipment de-signed for that purpose.4. Significance and Use4.1 This practice provides a guide whereby all pertinentvariables relating to the ultraviolet cure of a coating aredescribed.5. Procedure5.1 Apply the coating to be cured to the desired substrate ata film thickness

11、typical to that normally used. After approxi-mately the time delay encountered in production pass thecoated substrate through the curing equipment and subse-quently test for cure, as defined in 3.1.1, using the appropriatemethods listed in 5.1.1 through 5.1.11. The most commonlyused test methods are

12、 listed in 5.1.1 through 5.1.4.5.1.1 Impact ResistanceTest Method D2794.5.1.2 Film HardnessTest Method D3363.5.1.3 Solvent Rub TestHold a pad of cheesecloth or othercloth saturated with an agreed-upon solvent, usually methylethyl ketone, over two adjacent fingers using a protective1This practice is

13、under the jurisdiction of ASTM Committee D01 on Paint andRelated Coatings, Materials, and Applications and is the direct responsibility ofSubcommittee D01.55 on Factory Applied Coatings on Preformed Products.Current edition approved June 1, 2017. Published June 2017. Originallyapproved in 1978. Last

14、 previous edition approved in 2011 as D3732 82 (2011).DOI: 10.1520/D3732-82R17.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page o

15、nthe ASTM website.3The last approved version of this historical standard is referenced onwww.astm.org.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in accordance with internationally recogniz

16、ed principles on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.1covering. Rub the wet pad back and forth across a 100-mmportion of

17、the cured film using vigorous pressure, one forwardand one backward movement constituting one double rub. Takethe end point as the number of double rubs required to softenor penetrate the film. Fully cured films are normally required toresist a specified number of rubs and the result of the test isg

18、iven as exceeding the limit or failing the test.5.1.4 SandabilityUltraviolet cured fillers are usuallyjudged by their sandability with an agreed-upon grit of paper.This test is often made immediately after the material leavesthe ultraviolet processor.5.1.5 Specifying PropertiesGuide D2336.5.1.6 Abra

19、sion ResistanceTest Methods D658 and D968.5.1.7 Indentation HardnessTest Methods D1474.5.1.8 AdhesionTest Methods D2197 and D3359.5.1.9 Block ResistanceTest Method D2793.5.1.10 FormabilityTest Method D3281.5.1.11 Stain and Reagent ResistancePractice D3023.5.2 Repeat the application, curing, and test

20、ing with freshmaterial on fresh substrates until the shortest time that yields acured film is obtained.6. Report6.1 Ultraviolet curing equipment is available with severaldesign variables. Therefore, include the following informationwith results where applicable:6.1.1 Number of bulbs,6.1.2 Bulb type

21、(intensity, spectral distribution,composition),6.1.3 Bulb age,6.1.4 Bulb location (height from work and orientation toworkpiece),6.1.5 Reflector design,6.1.6 Conveyor speed or exposure time to achieve cure,6.1.7 Substrate,6.1.8 Coating identification and age of sample if known,6.1.9 Wet film thickne

22、ss,6.1.10 Temperature conditions in the curing unit,6.1.11 Curing environment (air, nitrogen, or otheratmosphere),6.1.12 Cure tests used (refer to Section 5), and6.1.13 Age of cured film when tests were run.7. Keywords7.1 cure time; ultraviolet-cured coatingsASTM International takes no position resp

23、ecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This s

24、tandard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM Interna

25、tional Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown bel

26、ow.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 82 (2017)2