ASTM D3808-2001(2013) Standard Test Method for Qualitative Determination of Adhesion of Adhesives to Substrates by Spot Adhesion《用点粘试验法定性测定胶粘剂与基底间粘性的标准试验方法》.pdf

1、Designation: D3808 01 (Reapproved 2013)Standard Test Method forQualitative Determination of Adhesion of Adhesives toSubstrates by Spot Adhesion1This standard is issued under the fixed designation D3808; the number immediately following the designation indicates the year oforiginal adoption or, in th

2、e case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers a simple qualitative procedurefor quickly screening whether an

3、 adhesive will, under recom-mended application conditions, bond to a given substratewithout actually making bonded assemblies.1.2 The values stated in SI units are to be regarded as thestandard. The values in parentheses are for information only.1.3 This standard does not purport to address all of t

4、hesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D907 Terminology of Adhesi

5、vesE171 Practice for Conditioning and Testing Flexible BarrierPackaging3. Terminology3.1 DefinitionsMany of the terms used in this test methodare defined in Terminology D907.3.1.1 spot adhesion, na qualitative method of determiningadhesion by attempting to pry a “spot” of cured adhesive froma substr

6、ate.4. Summary of Test Method4.1 Spots of adhesive (size can vary, but generally about 6mm (14 in.) in diameter) are placed onto a substrate using theapplication procedure and curing conditions acceptable to bothuser and supplier of the adhesive.4.2 The substrate preparation and environmental exposu

7、reof the spot of adhesive after cure or setting can be varied asdesired.4.3 The determination of whether an adhesive bonds to thesubstrate is made by simply trying to pry the spot of adhesivefrom the substrate.4.4 The mode of failure is readily evident by examiningwhether the bond separated adhesive

8、ly or cohesively, either inthe adhesive or substrate.5. Significance and Use5.1 This is a quick, simple, and inexpensive test method forqualitatively determining, without the need to prepare bondedtest specimens, whether the adhesive under consideration willbond to a particular substrate. If the res

9、ults are acceptable, thenstandard quantitative adhesive test procedures can be used toobtain quantitative measurements of the adhesives perfor-mance.5.2 This test method can also be used to compare relativeadhesion of several adhesives to given substrates.5.3 It can be used to determine whether an a

10、dhesive willcontinue to adhere to the substrate under specified environmen-tal conditions.5.4 It can be used to evaluate adhesion of a particularadhesive to a variety of substrates.5.5 It can be used to obtain “subjective” comparative databetween several adhesives on a given substrate by noting ther

11、elative ease of inducing failure between the adhesives tested.5.6 It should be most applicable to adhesives that cure or setwhen exposed to “air” (ambient, heated, etc.) and could beused for anaerobic adhesives if testing is carried out in anoxygen-free atmosphere.6. Apparatus6.1 No special equipmen

12、t is needed for application of theadhesive to the test substrate(s). When using hot-meltadhesives, for example, it would be desirable to have ahand-gun applicator or equivalent apparatus to allow deposi-tion of the hot-melt at a recommended application temperature.The use of such equipment is not ma

13、ndatory as a hot plate can1This test method is under the jurisdiction of ASTM Committee D14 onAdhesives and is the direct responsibility of Subcommittee D14.40 on Adhesives forPlastics.Current edition approved July 1, 2013. Published July 2013. Originally approvedin 1979. Last previous edition appro

14、ved in 2007 as D3808 01 (2007). DOI:10.1520/D3808-01R13.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyr

15、ight ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1be used to melt a quantity of the hot melt to the applicationtemperature in a deformable container such as an aluminumweighing dish. Upon reaching proper temperature, the hot meltcan be poure

16、d onto the substrate after forming a pouring spoutin the container.6.2 For some applications it is desirable to preheat thesubstrate. For this reason an oven or other heat source would beuseful.6.3 To test adhesion of the adhesive spot, a thin stainlesssteel spatula or similar probe is needed to pry

17、 or lift the spotfrom the substrate.7. Test Specimen7.1 Any form or shape of the substrate is acceptable. It isadvisable to place several spots of the same adhesive onto thesubstrate.7.2 In most cases, it is most efficient to test severaladhesives on the same substrate sample.8. Conditioning8.1 Stor

18、e the test specimens at the test conditions for 24 h,unless other test time is described. Note this when recordingdata. If other conditions are not specified, the storage and testconditions shall be 23 6 2C and 50 6 5 % relative humidity.Specification E171 details these and other test conditions.9.

19、Failure9.1 Failure is a visible separation of the adhesive spot eitheradhesively from the substrate or cohesively in the adhesive orsubstrate.9.2 The ease of separation of the adhesive spot can be usedto compare the relative performance of the adhesives.10. Procedure10.1 Run the tests in the same en

20、vironment used to condi-tion the test specimens and test apparatus.10.2 Using a thin-bladed stainless steel spatula or probe, tryto separate the adhesive spot from the substrate.10.3 Note the type and ease of failure as described inSection 9.11. Report11.1 Report the following information:11.1.1 Met

21、hod of specimen preparation, that is, adhesiveused, method of cure, substrate preparation, preheating ofsubstrate, if hot-melt was used, application temperature, andany other relevant information.11.1.2 Conditioning exposure.11.1.3 Mode of failure, that is, adhesive to substrate orcohesive in adhesi

22、ve or substrate, or both; relative ease offailure and any visible change in substrate due to adhesiveattack, for example, discoloration, crazing, softening, etc.12. Precision and Bias12.1 No information is presented about either precision orbias of this test method, since the test result is nonquant

23、itative.13. Keywords13.1 hot melt adhesive; spot adhesion; structural adhesiveASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the valid

24、ity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comme

25、nts are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have n

26、ot received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple co

27、pies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).D3808 01 (2013)2