1、Designation: D4562 01 (Reapproved 2013)Standard Test Method forShear Strength of Adhesives Using Pin-and-CollarSpecimen1This standard is issued under the fixed designation D4562; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the
2、year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope1.1 This test method covers the d
3、etermination of the shearstrength of curing liquid adhesives used for retaining cylindri-cal assemblies or for locking and sealing threaded fasteners.1.2 The values stated in inch-pound units are to be regardedas standard. The values given in parentheses are mathematicalconversions to SI units that
4、are provided for information onlyand are not considered standard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the appl
5、ica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2A108 Specification for Steel Bar, Carbon and Alloy, Cold-FinishedD907 Terminology of AdhesivesD2651 Guide for Preparation of Metal Surfaces forAdhesiveBondingE177 Practice for Use of the Terms Precision and
6、Bias inASTM Test MethodsE691 Practice for Conducting an Interlaboratory Study toDetermine the Precision of a Test Method3. Terminology3.1 DefinitionsMany of the terms in this standard aredefined in Terminology D907.4. Summary of Test Method4.1 This test method consists of bonding a metal pin insidea
7、 metal collar and determining the force required to shear theadhesive joint.5. Significance and Use5.1 This test method provides reasonably accurate informa-tion with regard to the ability of an adhesive to withstandshearing forces. It may also be used to determine degree ofcure and the effect of en
8、vironment on shear strength.6. Apparatus6.1 Universal Test Machine, or equivalent, for applyingforce to the specimen. Details of the test specimen (pin-and-collar) are given in Fig. 1.6.2 Specimen Curing Rack, as shown in Fig. 2, or equiva-lent.7. Preparation of Test Specimens7.1 Assemble five speci
9、mens for each test as described inthe following paragraphs:7.1.1 Each specimen is comprised of a pin 0.498 to 0.499 in.(12.65 to 12.675 mm) in diameter and a slip collar 0.500 to0.501 in. (12.7 to 12.725 mm) inside diameter by 0.435 to0.439 in. (11.05 to 11.15 mm) wide, both components finishedto 32
10、 to 64 in (0.8 to 1.6 m) with 0.001 to 0.003 in. (0.025to 0.075 mm) diametrical clearance between the pin and collar(see Fig. 1). The pin and collar, by agreement, may be made ofany material (see Appendix X1), but the most commonmaterial is steel, as specified in Specification A108.7.1.2 Degrease al
11、l pins and collars (refer to Guide D2651),store in an atmosphere of low humidity (20 % relativehumidity), and keep them clean. Use degreased specimenswithin four days or discard. (Oxidation affects the test resultsafter this time. Prior to vapor degreasing, it is permissible tosoak or wash hard-grea
12、sed or waxed parts in solvent.) Do notprime or activate unless specified for the material to be tested.7.1.3 To apply the adhesive, assemble the parts to be surethat there are no nicks that will cause them to stick or drag.Disassemble the parts. Apply sufficient adhesive to the circum-ference of the
13、 pin, beginning at one end, to completely cover an1This test method is under the jurisdiction of ASTM Committee D14 onAdhesives and is the direct responsibility of Subcommittee D14.60 on AdhesiveMaterial Classification System.Current edition approved July 1, 2013. Published July 2013. Originally app
14、rovedin 1986. Last previous edition approved in 2007 as D4562 01 (2007). DOI:10.1520/D4562-01R13.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Docum
15、ent Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1area the width of the collar in its final position. Also applysufficient adhesive to completely cover the interior of the collar360. Slip the collar o
16、ver the coated end of the pin with at least180 of rotation as the collar travels over the adhesive. Repeata back-and-forth rotation three times, or until the collarexhibits a smooth, consistent resistance to rotation.7.1.4 Rack the assembly with the fillet up so that the collardoes not slip out of t
17、he bond area. Take care that the rack is atthe required temperature and do not place onto a hot or coldsurface. There should be excess material on the leading edge ofthe collar; if not, apply sufficient adhesive to create a fillet.7.1.5 Cure the specimens in accordance with the manufac-turers instru
18、ctions.7.1.5.1 For primed or activated surfaces, when specified orrecommended, use the manufacturers primer. Apply theprimer and adhesive according to the manufacturers instruc-tions. Assemble and cure the specimens for a time andtemperature in accordance with the manufacturers recommen-dation.8. Pr
19、ocedure8.1 After allowing for cure and any planned environmentalconditioning, determine the static shear strength as follows:8.1.1 Place the pin and collar assembly on the universal testmachine as shown in Fig. 3. Load the specimen smoothly atabout 500 lb/s (2200 N/s) using a free crosshead speed of
20、 0.05in./min (1.3 mm/min). Record the maximum load in pounds(Newtons). Calculate the static shear strength by dividing thebreakaway load by the bond area as follows:Shear Strength 5 Maximum Load/Diameter 33.14 3Width9. Report9.1 Report the following information:9.1.1 Complete identification of the a
21、dhesive tested, includ-ing type, source, date manufactured, manufacturers codenumbers, and form.9.1.2 Complete identification of the metal used and themethod of cleaning and preparing its surfaces prior to bonding.9.1.3 Application and bonding conditions used in preparingthe specimens.9.1.4 Conditio
22、ning procedure used for specimens prior totesting.9.1.5 Number of specimens tested.9.1.6 Maximum, minimum, and average values for failingload, and shear strength.10. Precision and Bias10.1 PrecisionAn interlaboratory study of the shearstrength of anaerobic adhesives was run in 1989. Each of sixFIG.
23、1 Pin-and-Collar AssemblyFIG. 2 Specimen RackFIG. 3 Test DeviceD4562 01 (2013)2laboratories tested ten test specimens from each of six adhe-sives ranging in viscosity from 125 to 2000 cP. Relativehumidity was controlled between 48 and 62 % at 72 to 76F,and all samples were cured for 24 h. All shear
24、strengths wereobtained by dividing maximum loads by a nominal bond areaof 0.69 in2. Practice E691 was followed for the design andanalysis of the data. The following repeatability and reproduc-ibility limits were obtained for each of the six materials as aresult of the interlaboratory study:Adhesive
25、Shear Strength, psi 95 % limit, psiRepeatability ReproducibilityE 2742 703 977F 3320 778 1008C 3377 930 1022A 3630 862 1005D 3717 1341 2134B 4006 778 1126The above terms repeatability limit and reproducibility limitare used as specified in Practice E177. The respective standarddeviations among test
26、results may be obtained by dividingcolumns 3 and 4 by 2.8.10.2 BiasSince there is no accepted reference material,method, or laboratory suitable for determining the bias for theprocedure in this test method for measuring shear strength ofadhesives, no statement on bias is being made.11. Keywords11.1
27、pin and collar; shear strengthAPPENDIX(Nonmandatory Information)X1. SPECIMEN MATERIALSX1.1 Specimens may be made of other materials or withfinishes other than steel. Mixing of materials is not recom-mended unless the results of differential thermal expansion arespecifically desired. Some material an
28、d finish standards are asfollows:X1.1.1 ASTM Standard:B633 Specification for Electrodeposited Coatings of Zinc onIron and Steel2X1.1.2 Federal Specifications:3QQ-A-250/4 Aluminum Alloy 2024, Plate and SheetQQ-B-613 Brass, Leaded and Nonleaded: Flat Products(Plate, Bar, Sheet, and Strip)QQ-P416 Plati
29、ng, Cadmium (Electrodeposited)QQ-A-200/4 Aluminum Alloy 5083, Bar, Rod, Shapes, Tubeand Wire, ExtrudedQQ-A-200/5 Aluminum Alloy 5006, Bar, Rod, Shapes, Tubeand Wire, ExtrudedQQ-A-200/6 Aluminum Alloy 5454, Bar, Rod, Shapes, Tubeand Wire, ExtrudedQQ-A-200/7 Aluminum Alloy 5456, Bar, Rod, Shapes, Tube
30、and Wire, ExtrudedQQ-A-200/8 Aluminum Alloy 6061, Bar, Rod, Shapes, Tubeand Wire, ExtrudedQQ-A-200/15 Aluminum Alloy, Bar, Rod, and Shapes,Extruded. 7075-76 (Improved Exfoliation Resistant)QQ-S-763 Steel Bars, Wire Shapes, and Forgings,Corrosion-ResistingTT-C-490 Cleaning Method and Pretreatment of
31、FerrousSurfaces for Organic CoatingsX1.1.3 Military Specification:3MIL-A-8625Anodic Coatings for Aluminum and Alumi-num AlloysX1.1.4 Society of Automotive Engineers (SAE) AeronauticalMaterials Specification:4AMS 4935 Titanium Alloy Extrusions and Flash WeldedRings, 6A14V Annealed, Beta Processed3Ava
32、ilable from Standardization Documents Order Desk, DODSSP, Bldg. 4,Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:/www.dodssp.daps.mil.4Available from Society of Automotive Engineers (SAE), 400 CommonwealthDr., Warrendale, PA 15096-0001, http:/www.sae.org.D4562 01 (2013)3ASTM Internat
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35、be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standar
36、ds, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).D4562 01 (2013)4
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