ASTM D4762-2011a Standard Guide for Testing Polymer Matrix Composite Materials《聚合物基复合材料测试的标准指南》.pdf

1、Designation: D4762 11aStandard Guide forTesting Polymer Matrix Composite Materials1This standard is issued under the fixed designation D4762; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in pa

2、rentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This guide summarizes the application of ASTM stan-dard test methods (and other supporting standards) tocontinuous-fiber reinforced polymer matrix

3、composite materi-als. The most commonly used or most applicable ASTMstandards are included, emphasizing use of standards of Com-mittee D30 on Composite Materials.1.2 This guide does not cover all possible standards thatcould apply to polymer matrix composites and restricts discus-sion to the documen

4、ted scope. Commonly used but non-standard industry extensions of test method scopes, such asapplication of static test methods to fatigue testing, are notdiscussed. A more complete summary of general compositetesting standards, including non-ASTM test methods, is in-cluded in the Composite Materials

5、 Handbook (MIL-HDBK-17).2Additional specific recommendations for testing textile(fabric, braided) composites are contained in Guide D6856.1.3 This guide does not specify a system of measurement;the systems specified within each of the referenced standardsshall apply as appropriate. Note that the ref

6、erenced standardsof ASTM Committee D30 are either SI-only or combined-unitstandards with SI units listed first.1.4 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safe

7、ty and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:32.1.1 Standards of Committee D30 on Composite MaterialsC271/C271M Test Method for Density of Sandwich CoreMaterialsC272 Test Method for Water Absorption of Core

8、Materialsfor Structural Sandwich ConstructionsC273/C273M Test Method for Shear Properties of Sand-wich Core MaterialsC297/C297M Test Method for Flatwise Tensile Strength ofSandwich ConstructionsC363/C363M Test Method for Node Tensile Strength ofHoneycomb Core MaterialsC364/C364M Test Method for Edge

9、wise CompressiveStrength of Sandwich ConstructionsC365/C365M Test Method for Flatwise Compressive Prop-erties of Sandwich CoresC366/C366M Test Methods for Measurement of Thicknessof Sandwich CoresC393/C393M Test Method for Core Shear Properties ofSandwich Constructions by Beam FlexureC394 Test Metho

10、d for Shear Fatigue of Sandwich CoreMaterialsC480/C480M Test Method for Flexure Creep of SandwichConstructionsC481 Test Method for Laboratory Aging of SandwichConstructionsC613/C613M Test Method for Constituent Content of Com-posite Prepreg by Soxhlet ExtractionD2344/D2344M Test Method for Short-Bea

11、m Strength ofPolymer Matrix Composite Materials and Their LaminatesD3039/D3039M Test Method for Tensile Properties ofPolymer Matrix Composite MaterialsD3171 Test Methods for Constituent Content of CompositeMaterialsD3410/D3410M Test Method for Compressive Propertiesof Polymer Matrix Composite Materi

12、als with UnsupportedGage Section by Shear LoadingD3479/D3479M Test Method for Tension-Tension Fatigueof Polymer Matrix Composite MaterialsD3518/D3518M Test Method for In-Plane Shear Responseof Polymer Matrix Composite Materials by Tensile Test ofa 645 LaminateD3529/D3529M Test Method for Matrix Soli

13、ds Content andMatrix Content of Composite PrepregD3530/D3530M Test Method for Volatiles Content of Com-posite Material Prepreg1This guide is under the jurisdiction of ASTM Committee D30 on CompositeMaterials and is the direct responsibility of Subcommittee D30.01 on Editorial andResource Standards.C

14、urrent edition approved Aug. 1, 2011. Published September 2011. Originallyapproved in 1988. Last previous edition approved in 2011 as D4762 11. DOI:10.1520/D4762-11A.2Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:/

15、dodssp.daps.dla.mil.3For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr H

16、arbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.D3531 Test Method for Resin Flow of Carbon Fiber-EpoxyPrepregD3532 Test Method for Gel Time of Carbon Fiber-EpoxyPrepregD3800 Test Method for Density of High-Modulus FibersD3878 Terminology for Composite MaterialsD4018 Test Me

17、thods for Properties of Continuous FilamentCarbon and Graphite Fiber TowsD4102 Test Method for Thermal Oxidative Resistance ofCarbon FibersD4255/D4255M Test Method for In-Plane Shear Propertiesof Polymer Matrix Composite Materials by the Rail ShearMethodD5229/D5229M Test Method for Moisture Absorpti

18、onProperties and Equilibrium Conditioning of Polymer Ma-trix Composite MaterialsD5379/D5379M Test Method for Shear Properties of Com-posite Materials by the V-Notched Beam MethodD5448/D5448M Test Method for Inplane Shear Propertiesof Hoop Wound Polymer Matrix Composite CylindersD5449/D5449M Test Met

19、hod for Transverse CompressiveProperties of Hoop Wound Polymer Matrix CompositeCylindersD5450/D5450M Test Method for Transverse Tensile Prop-erties of Hoop Wound Polymer Matrix Composite Cylin-dersD5467/D5467M Test Method for Compressive Propertiesof Unidirectional Polymer Matrix Composite Materials

20、Using a Sandwich BeamD5528 Test Method for Mode I Interlaminar FractureToughness of Unidirectional Fiber-Reinforced PolymerMatrix CompositesD5687/D5687M Guide for Preparation of Flat CompositePanels with Processing Guidelines for Specimen Prepara-tionD5766/D5766M Test Method for Open-Hole TensileStr

21、ength of Polymer Matrix Composite LaminatesD5961/D5961M Test Method for Bearing Response ofPolymer Matrix Composite LaminatesD6115 Test Method for Mode I Fatigue DelaminationGrowth Onset of Unidirectional Fiber-Reinforced PolymerMatrix CompositesD6264/D6264M Test Method for Measuring the DamageResis

22、tance of a Fiber-Reinforced Polymer-Matrix Com-posite to a Concentrated Quasi-Static Indentation ForceD6415/D6415M Test Method for Measuring the CurvedBeam Strength of a Fiber-Reinforced Polymer-MatrixCompositeD6416/D6416M Test Method for Two-Dimensional Flex-ural Properties of Simply Supported Sand

23、wich CompositePlates Subjected to a Distributed LoadD6484/D6484M Test Method for Open-Hole CompressiveStrength of Polymer Matrix Composite LaminatesD6507 Practice for Fiber Reinforcement Orientation Codesfor Composite MaterialsD6641/D6641M Test Method for Compressive Propertiesof Polymer Matrix Comp

24、osite Materials Using a Com-bined Loading Compression (CLC) Test FixtureD6671/D6671M Test Method for Mixed Mode I-Mode IIInterlaminar Fracture Toughness of Unidirectional FiberReinforced Polymer Matrix CompositesD6742/D6742M Practice for Filled-Hole Tension and Com-pression Testing of Polymer Matrix

25、 Composite LaminatesD6772 Test Method for Dimensional Stability of SandwichCore MaterialsD6790 Test Method for Determining Poissons Ratio ofHoneycomb CoresD6856 Guide for Testing Fabric-Reinforced “Textile” Com-posite MaterialsD6873/D6873M Practice for Bearing Fatigue Response ofPolymer Matrix Compo

26、site LaminatesD7028 Test Method for Glass Transition Temperature(DMA Tg) of Polymer Matrix Composites by DynamicMechanical Analysis (DMA)D7078/D7078M Test Method for Shear Properties of Com-posite Materials by V-Notched Rail Shear MethodD7136/D7136M Test Method for Measuring the DamageResistance of

27、a Fiber-Reinforced Polymer Matrix Com-posite to a Drop-Weight Impact EventD7137/D7137M Test Method for Compressive ResidualStrength Properties of Damaged Polymer Matrix Compos-ite PlatesD7205/D7205M Test Method for Tensile Properties of Fi-ber Reinforced Polymer Matrix Composite BarsD7248/D7248M Tes

28、t Method for Bearing/Bypass Interac-tion Response of Polymer Matrix Composite LaminatesUsing 2-Fastener SpecimensD7249/D7249M Test Method for Facing Properties ofSandwich Constructions by Long Beam FlexureD7250/D7250M Practice for Determining Sandwich BeamFlexural and Shear StiffnessD7264/D7264M Tes

29、t Method for Flexural Properties ofPolymer Matrix Composite MaterialsD7291/D7291M Test Method for Through-Thickness “Flat-wise” Tensile Strength and Elastic Modulus of a Fiber-Reinforced Polymer Matrix Composite MaterialD7332/D7332M Test Method for Measuring the FastenerPull-Through Resistance of a

30、Fiber-Reinforced PolymerMatrix CompositeD7336/D7336M Test Method for Static Energy AbsorptionProperties of Honeycomb Sandwich Core MaterialsD7337/D7337M Test Method for Tensile Creep Rupture ofFiber Reinforced Polymer Matrix Composite BarsD7522/D7522M Test Method for Pull-Off Strength for FRPBonded

31、to Concrete SubstrateD7565/D7565M Test Method for Determining TensileProperties of Fiber Reinforced Polymer Matrix Compos-ites Used for Strengthening of Civil StructuresD7615/D7615M Practice for Open-Hole Fatigue Responseof Polymer Matrix Composite LaminatesD7616/D7616M Test Method for Determining A

32、pparentOverlap Splice Shear Strength Properties of Wet Lay-UpFiber-Reinforced Polymer Matrix Composites Used forStrengthening Civil StructuresD7617/D7617M Test Method for Transverse Shear Strengthof Fiber-reinforced Polymer Matrix Composite BarsD4762 11a2E1309 Guide for Identification of Fiber-Reinf

33、orcedPolymer-Matrix Composite Materials in DatabasesE1434 Guide for Recording Mechanical Test Data of Fiber-Reinforced Composite Materials in DatabasesE1471 Guide for Identification of Fibers, Fillers, and CoreMaterials in Computerized Material Property DatabasesF1645/F1645M Test Method for Water Mi

34、gration in Hon-eycomb Core Materials2.1.2 Standards of Committee D20 on PlasticsC581 Practice for Determining Chemical Resistance ofThermosetting Resins Used in Glass-Fiber-ReinforcedStructures Intended for Liquid ServiceD256 Test Methods for Determining the Izod PendulumImpact Resistance of Plastic

35、sD543 Practices for Evaluating the Resistance of Plastics toChemical ReagentsD570 Test Method for Water Absorption of PlasticsD618 Practice for Conditioning Plastics for TestingD638 Test Method for Tensile Properties of PlasticsD648 Test Method for Deflection Temperature of PlasticsUnder Flexural Lo

36、ad in the Edgewise PositionD671 Test Method for Flexural Fatigue of Plastics byConstant-Amplitude-of-Force4D695 Test Method for Compressive Properties of RigidPlasticsD696 Test Method for Coefficient of Linear Thermal Ex-pansion of Plastics Between 30C and 30C with aVitreous Silica DilatometerD790 T

37、est Methods for Flexural Properties of Unreinforcedand Reinforced Plastics and Electrical Insulating MaterialsD792 Test Methods for Density and Specific Gravity (Rela-tive Density) of Plastics by DisplacementD953 Test Method for Bearing Strength of PlasticsD1505 Test Method for Density of Plastics b

38、y the Density-Gradient TechniqueD1822 Test Method for Tensile-Impact Energy to BreakPlastics and Electrical Insulating MaterialsD2471 Practice for Gel Time and Peak Exothermic Tem-perature of Reacting Thermosetting Resins4D2583 Test Method for Indentation Hardness of RigidPlastics by Means of a Barc

39、ol ImpressorD2584 Test Method for Ignition Loss of Cured ReinforcedResinsD2734 Test Methods for Void Content of Reinforced Plas-ticsD2990 Test Methods for Tensile, Compressive, and Flex-ural Creep and Creep-Rupture of PlasticsD3418 Test Method for Transition Temperatures and En-thalpies of Fusion an

40、d Crystallization of Polymers byDifferential Scanning CalorimetryD3846 Test Method for In-Plane Shear Strength of Rein-forced PlasticsD4065 Practice for Plastics: Dynamic Mechanical Proper-ties: Determination and Report of ProceduresD4473 Test Method for Plastics: Dynamic MechanicalProperties: Cure

41、BehaviorD5083 Test Method for Tensile Properties of ReinforcedThermosetting Plastics Using Straight-Sided SpecimensD6272 Test Method for Flexural Properties of Unreinforcedand Reinforced Plastics and Electrical Insulating Materialsby Four-Point Bending2.1.3 Standards of Other ASTM CommitteesE228 Tes

42、t Method for Linear Thermal Expansion of SolidMaterials With a Push-Rod DilatometerE289 Test Method for Linear Thermal Expansion of RigidSolids with InterferometryE1269 Test Method for Determining Specific Heat Capacityby Differential Scanning CalorimetryE1461 Test Method for Thermal Diffusivity by

43、the FlashMethodE1922 Test Method for Translaminar Fracture Toughness ofLaminated and Pultruded Polymer Matrix Composite Ma-terials3. Terminology3.1 Definitions related to composite materials are defined inTerminology D3878.3.2 Symbology for specifying the orientation and stackingsequence of a compos

44、ite laminate is defined in Practice D6507.3.3 For purposes of this document, “low modulus” compos-ites are defined as being reinforced with fibers having amodulus #20 GPa (#3.0 3 106psi), while “high-modulus”composites are reinforced with fiber having a modulus 20GPa (3.0 3 106psi).4. Significance a

45、nd Use4.1 This guide is intended to aid in the selection of standardsfor polymer matrix composite materials. It specifically sum-marizes the application of standards from ASTM CommitteeD30 on Composite Materials that apply to continuous-fiberreinforced polymer matrix composite materials. For referen

46、ceand comparison, many commonly used or applicable ASTMstandards from other ASTM Committees are also included.5. Standard Specimen Preparation5.1 Preparation of polymer matrix composite test specimensis described in Guide D5687/D5687M.6. Standard Test Methods6.1 ASTM test methods for the evaluation

47、of polymermatrix composites are summarized in the tables. Advantages,disadvantages, and other comments for each test method areincluded where appropriate. Where possible, a single preferredtest method is identified.TEST METHOD CATEGORY TABLELamina/Laminate Static Properties Table 1Lamina/Laminate Dy

48、namic Properties Table 2Laminate/Structural Response Table 3Sandwich Constructions Table 4Constituent/Precursor/Thermophysical Properties Table 5Environmental Conditioning/Resistance Table 64Withdrawn. The last approved version of this historical standard is referencedon www.astm.org.D4762 11a3TABLE

49、 1 Lamina/Laminate Static Test MethodsTest Method Specimen Measured PropertyDescription andAdvantagesDisadvantages CommentsIn-Plane Tensile Test MethodsD3039/D3039M Tensile Strength Straight sidedspecimen. Suitable forboth random,discontinuous andcontinuous-fibercomposites. Tabbedand untabbedconfigurationsavailable.Tabbed configurationsrequire carefuladhesive selectionand special specimenpreparation.Certain laminatelayups prone to edgedelamination whichcan affect tensilestrength results.Preferred for most uses.Provides additionalconfigurations, requirements,and guidance that