ASTM D5301-1992(2016) Standard Practice for Physical Characterization of Paint Brushes《涂料刷的物理特性的标准操作规程》.pdf

1、Designation: D5301 92 (Reapproved 2016)Standard Practice forPhysical Characterization of Paint Brushes1This standard is issued under the fixed designation D5301; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revi

2、sion. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice covers the dimensions, terminology, ma-terials and characteristics generally considered of importanceto those wit

3、hin, or dealing with paint brushes, and describesmethods of determining these parameters. This practice is notmeant to be a definitive analytical method to deformulatebrushes.1.2 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.

4、1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Terminology2

5、.1 Definitions:2.1.1 chisel (or chiseled), na description of the configu-ration of the tip of the brush as being of a more or less convexshape across the thickness dimension.2.1.2 flat tip, na description of the configuration of the tipof the brush as being flat or of uniform length across thethickn

6、ess dimension.2.1.3 flagged, na term describing the tip of a filament orbristle as being split resulting in a multiplicity of filament ends.2.1.4 tipped, na term describing the tip of a filament orbristle as coming to a point.2.1.5 microtome, na device for holding a number offilament or bristle mate

7、rials in a rigid state for a cross sectionalexamination under a microscope (see Fig. 1).3. Significance and Use3.1 It is important to recognize that a brush can be a mixtureof several chemically different filaments or bristles, or both, inseveral cross sections, thicknesses and lengths. The followin

8、gprocedures will be helpful in identifying brush composition.4. Determination of Head Dimensions4.1 WidthDetermine the width by measuring the brushingmaterial adjacent to the ferrule in the wide or broad dimension,using any accurate linear measuring device. Report dimensionsto the nearest 3 mm (18 i

9、n.).4.2 ThicknessDetermine the thickness by measuring thebrushing material adjacent to the ferrule, in the narrowdimension, using any accurate linear measuring device. Reportdimensions to the nearest 1 mm (116 in.).4.3 Length Clear (Length Out)Determine the length bymeasuring the exposed filament or

10、 bristle length from the edgeof the ferrule to its tip, using any accurate linear measuringdevice. Measure the brush on each end of the width andaverage the measurements so obtained to give the mean value.Report dimensions to the nearest 1 mm (116 in.).NOTE 1In the case of an angular sash brush, ind

11、icate whether theferrule is angular or straight.5. Brush Tip Configuration5.1 Describe the configuration at the tip of the head aschiseled or flat (see 2.1.1 and 2.1.2).6. Brushing Material Characteristics6.1 Cross-Sectional ShapeDetermine the cross-sectionalshape of the filaments or bristles by ins

12、erting a representativesample of brushing material into the slot of a microtome,cutting the material flush with the surface of the microtomewith a razor blade, and examining it visually with a 30 orgreater microscope. Report the observations of filament shapesfor example, round, solid, hollow or oth

13、ers.6.2 Filament or Bristle LengthDetermine the lengths ofthe filaments or bristles used in a brush by opening the ferruleand removing the filaments from that portion of the brushunaffected by the chisel. Measure a representative number ofspecimens to the nearest 1 mm (116 in.), and report the lengt

14、hor various lengths.6.3 Filament or Bristle Thickness and ProfileRemove arepresentative sample of filaments or bristles (10 to 20) fromthe brush as described in 6.2 and measure their thickness or1This practice is under the jurisdiction of ASTM Committee D01 on Paint andRelated Coatings, Materials, a

15、nd Applications and is the direct responsibility ofSubcommittee D01.61 on Paint Application Tools.Current edition approved Dec. 1, 2016. Published December 2016. Originallyapproved in 1992. Last previous edition approved in 2012 as D5301 92 (2012).DOI: 10.1520/D5301-92R16.Copyright ASTM Internationa

16、l, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides

17、and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.1diameter using a micrometer. Take measurements with a dialmicrometer near each end. Those having the same measure-ment on each end are termed “level” and only one dimensionis expressed; those havi

18、ng differences by 2 mils or more aretermed “tapered” and the two dimensions are expressed as“thicker dimension/thinner dimension.” Express dimensions inthousandths of an inch or hundredths of a millimeter.6.4 Filament or Bristle ColorDetermine how many dif-ferent color filaments are present. This wi

19、ll assist in separatingthe filament sample, once taken, into the various filament typesfor proper analysis. Often, filaments of different compositionare colored differently as well.6.5 Chemical CompositionMaterial chemical compositionmay be determined by removing a representative sample offilaments

20、or bristles and subjecting them to conventionalanalytical methods. Burning odor and behavior, solubility,density, melting point, and infra red spectroscopy are all usefultechniques for estimating chemical composition. It is importantwhen determining chemical composition that a uniform andhomogeneous

21、 sample of filaments be used.6.6 Finishing (Processing)Observe finishing on the tips ofthe filaments or bristles, such as tipping or flagging, by visualexamination with a 10 magnifying glass (see 2.1.3 and 2.1.4).7. Ferrule Characteristics7.1 Ferrule Dimensions:7.1.1 Measure the shorter dimension (t

22、hickness) of theopening of the ferrule to the nearest 1 mm (116 in.).7.1.2 Measure longer dimension (width) of the opening ofthe ferrule to the nearest 3 mm (18 in.).7.1.3 Measure dimension across the closed part of theferrule (height) to the nearest 1 mm (116 in.).7.2 Ferrule Material:7.2.1 Determi

23、ne the surface material of the ferrule byconventional chemical analysis. Usual materials are tin platedsteel, nickel plated steel, lacquer coated brass or copper platedsteel and stainless steel.7.2.2 Determine if the surface is lacquered by vigorouslyrubbing the ferrule using a cloth wetted with a s

24、olvent such asacetone or butyl acetate. If lacquered, the finish will dissolve.7.3 Ferrule ShapeDescribe the shape of the ferrule open-ing as rectangular (having corners), straight with rounded ends,oval, or other.8. Handle8.1 Determine the length of the handle by simple measure-ment from the handle

25、 tip to the ferrule expressed to the nearest116 in. (1 mm).8.2 Describe the handle material as wood, plastic, or other.8.3 Describe the handle finish (sealed, lacquered, none).8.4 Describe the handle style, for example, beavertail, flatsash, kaiser, pencil or others (see Fig. 2).9. Handle Attachment

26、s9.1 Describe the attachment method of the ferrule to thehandle as stapled, nailed or crimped.9.2 Describe the fit of the handle to the ferrule.10. Brush Style10.1 Report the style of the brush, such as varnish/enamel,wall, flat sash, angular sash or other (see Fig. 3).11. Keywords11.1 paint brush;

27、physical characterizationFIG. 1 MicrotomeFIG. 2 Common Brush Handle StylesFIG. 3 Common Paint Brush StylesD5301 92 (2016)2ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expre

28、ssly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised

29、, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may a

30、ttend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States

31、. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 92 (2016)3