ASTM D6136 D6136M-1997(2013)e1 3178 Standard Test Method for Kerosine Number of Unsaturated (Dry) Felt by Vacuum Method 《用真空法对非饱和的 (干的) 毛毡的煤油数量测定的标准试验方法》.pdf

1、Designation: D6136/D6136M 97 (Reapproved 2013)1Standard Test Method forKerosine Number of Unsaturated (Dry) Felt by VacuumMethod1This standard is issued under the fixed designation D6136/D6136M; the number immediately following the designation indicates theyear of original adoption or, in the case o

2、f revision, the year of last revision. A number in parentheses indicates the year of lastreapproval. A superscript epsilon () indicates an editorial change since the last revision or reapproval.1NOTEUnits information was editorially corrected in January 2013.1. Scope1.1 This test method covers the d

3、etermination of the relativesaturating capacity of unsaturated (dry) felt papers used inroofing.1.2 The values stated in either SI units or inch-pound unitsare to be regarded separately as standard. The values stated ineach system may not be exact equivalents; therefore, eachsystem shall be used ind

4、ependently of the other. Combiningvalues from the two systems may result in non-conformancewith the standard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety

5、 and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D585 Practice for Sampling and Accepting a Single Lot ofPaper, Paperboard, Fiberboard, and Related Product(Withdrawn 2010)3D1298 Test Method for Density, Relative

6、Density, or APIGravity of Crude Petroleum and Liquid Petroleum Prod-ucts by Hydrometer MethodD3699 Specification for Kerosine3. Summary of Test Method3.1 The kerosine number of unsaturated (dry) felt is com-puted from the weight of a kerosine of known specific gravityretained by the felt after displ

7、acement of the air from interiorvoids. It is the millilitres of kerosine held /100 g of felt, andthus, is a measure of the quantity of saturant that a given feltwill absorb.4. Significance and Use4.1 The ability to absorb kerosine is an indication of theability to absorb hot asphalt. The kerosine nu

8、mber is used incalculating saturation efficiency.5. Apparatus5.1 Glass Vessel, approximately 1500 mL capacity, forsoaking specimens of felt in kerosine, under vacuum.5.2 Vacuum Pump, capable of reaching and maintaining avacuum of at least 700 mm Hg in the glass vessel.5.3 Lightweight Glass or Metal

9、Weighing Container, withtightly fitting cover, 60 by 140 mm 2.5 by 5.5 in. or larger, tocontain felt strips in a horizontal position without bending ordistortion.5.4 Drying Oven, with dimensions at least 300 by 300 by300 mm 12 by 12 by 12 in.5.5 Other Apparatus Desiccator, wire hook, and ifnecessary

10、, a punch to make a small hole in a corner of thespecimens after they are cut.6. Materials6.1 Water-White Kerosine, complying to the requirements ofSpecification D3699 and having a specific gravity of 0.800 60.025 at 25C, as determined in accordance with PracticeD1298.7. Sampling7.1 Obtain a sample

11、of the felt in accordance with PracticeD585.8. Test Specimen8.1 From each test unit of the sample cut two sets of six testspecimen strips, each strip measuring 51 by 127 6 13 mm 21This test method is under the jurisdiction ofASTM Committee D08 on Roofingand Waterproofing and is the direct responsibi

12、lity of Subcommittee D08.04 on Felts,Fabrics and Bituminous Sheet Materials.Current edition approved Jan. 1, 2013. Published January 2013. Originallyapproved in 1997. Last previous edition approved in 2004 as D6136 97 (2004).DOI: 10.1520/D6136_D6136M-97R13E01.2For referenced ASTM standards, visit th

13、e ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3The last approved version of this historical standard is referenced onwww.astm.org.Copyright ASTM In

14、ternational, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1by 5 612 in. with the longer side parallel to the machinedirection of the sheet.9. Procedure9.1 Place a set of strips in the tared weighing container andexpose them, uncovered, for at least 1 but not mor

15、e than2hinan oven, the interior of which is maintained at a temperature of105 6 3C. Keep the felt strips flat. Do not fold, roll, or distortthem in any way. Handle the six strips as a unit in all of thefollowing operations.9.2 Remove the strips in the weighing container from theoven and place them,

16、with the container still uncovered, in adesiccator to cool.9.3 After cooling, rapidly close the container and weigh itwith enclosed strips to the nearest 10 mg to obtain the netweight of the dry strips.9.4 Insert a wire hook in one corner of the strips andimmerse them at once in a vertical position

17、in 1000 mL ofkerosine at 25 6 1C in the glass vacuum vessel. Apply avacuum of at least 700 mm Hg to the vessel containing thestrips and hold it under these conditions for 15 min or for 5 minafter the bubbles cease to come from the felt strips, whicheverperiod is longer. Remove the felt strips from t

18、he kerosine andlet them drain in the machine direction of the felt for 3 min 61 s, allowing the lower corner of each strip to touch the edgeof the kerosine container.9.5 Return the soaked strips to their weighing container,close the container, and determine the combined weight of thestrips and the a

19、bsorbed kerosine. (WarningCare should beexercised in the use of kerosine because it is flammable. Do notexpose the material and its vapors to open flame or electricalspark.)10. Calculation10.1 Calculate the kerosine number as follows:Kerosine number 5b/a! 2 1c(1)where:a = weight of dry felt in g,b =

20、 weight of dry felt plus absorbed kerosine in g, andc = specific gravity of the kerosine.11. Report11.1 Report the kerosine number as the average of twodeterminations, to three significant figures.12. Precision and Bias12.1 The following criteria shall be used for judging theacceptability of any res

21、ult (95 % confidence level):12.1.1 Repeatability Duplicate results by the same opera-tor should not be considered suspect unless they differ by morethan 2.5 %.12.1.2 Reproducibility Reproducibility has not been de-termined.12.1.3 BiasThe bias of this test method has not beendetermined.13. Keywords13

22、.1 kerosine number; unsaturated (dry) felt; unsaturatedroofing feltASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any

23、such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are inv

24、ited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received

25、 a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of th

26、is standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).D6136/D6136M 97 (2013)12