ASTM D6753-2002(2008) 459 Standard Specification for Coal Tar Adhesive.pdf

1、Designation: D 6753 02 (Reapproved 2008)Standard Specification forCoal Tar Adhesive1This standard is issued under the fixed designation D 6753; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in

2、parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers coal tar adhesive with orwithout polymer modification suitable for brush, spray, squee-gee and trowel application to co

3、al tar built up and coal tarmodified bitumen membrane roofings and flashings.1.2 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationpurposes only.1.3 This standard does not purport to address all of thesafety concerns, if any, associat

4、ed with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory requirements prior to use.2. Referenced Documents2.1 ASTM Standards:2D 903 Test Method for Peel or Stripping Strength of Adhe-siv

5、e BondsD 6511 Test Methods for Solvent Bearing BituminousCompounds3. Classification3.1 Type IBrush, squeegee, or spray consistency intendedfor use in the application of field sheet membranes.3.2 Type IIHeavy brushing or trowel consistency intendedfor use in the repair of coal tar roofing and flashin

6、gs andinstallation of flashings.4. Materials and Manufacture4.1 Coal tar adhesive shall consist of a processed coal tarbase, volatile solvents, mineral stabilizers, with or withoutpolymer modifiers excluding asbestos, mixed to a smoothconsistency.5. Physical Requirements5.1 The material shall confor

7、m to the requirements pre-scribed in Table 1.5.2 UniformityA thoroughly stirred sample shall show noseparation of solvent or settling that cannot be overcome bymoderate stirring after standing for 72 h at room temperature ina closed container.6. Sampling and Test Methods6.1 Test Methods D 6511:6.2 S

8、trength of LapTest Methods D 6511 as modifiedbelow:6.2.1 Three sets of four specimens shall be prepared, con-ditioned, and tested at three different temperatures for lap shearstrength.6.2.2 Temperatures are to be 10, 25, and 60C (50, 77, and140F), for conditioning and 10, 25, and 32C (50, 77, and90F

9、) for testing. Preparation of specimens shall be done at alaboratory temperature of 23 6 1.8C (73.4 6 3.6F).6.2.3 Test Specimen and Sample:6.2.3.1 Use a sample of the actual roofing membraneintended for use with the adhesive.6.2.3.2 For each specimen, cut a 1- by 12-in. (25- by305-mm) transverse str

10、ip of membrane that includes theselvage; then cut this strip in half so that one piece contains theselvage and the other is plain.6.2.3.3 Spread the amount of coal tar adhesive recom-mended by the manufacturer evenly over the selvage and thenplace the reverse side of the plain half over the adhesive

11、 coatedselvage in the same manner as a field lap would be made.1This specification is under the jurisdiction of ASTM Committee D08 onRoofing and Waterproofing and is the direct responsibility of Subcommittee D08.05on Solvent-Bearing Bituminous Compounds for Roofing and Waterproofing.Current edition

12、approved May 1, 2008. Published June 2008. Originallyapproved in 2002. Last previous edition approved in 2002 as D 6753 02.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, re

13、fer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.6.2.3.4 Place a 10-lb (4.5-kg) mass over the lap. The massshall be large enough to cover the area containing adhesive.After

14、 2 min, remove the mass and condition the specimens asprescribed in Table 1. Use care when handling or movingsamples.6.2.4 ProcedureTest each specimen immediately after thespecified conditioning period in accordance with Test MethodsD 6511. If any specimen fails to meet the minimum valuesspecified i

15、n Table 1, report the material as failing the lapstrength.6.3 Peel Strength:6.3.1 Test each specimen immediately after the specifiedconditioning period in accordance with Test Method D 903.Specimens prepared as in 6.2.3. If any specimen fails to meetthe minimum values specified in Table 1, report th

16、e material asfailing the peel strength.7. Inspection7.1 Inspection of the material shall be as agreed uponbetween the purchaser and the suppler as part of the purchasecontract.8. Rejection and Resubmittal8.1 Failure to conform to any of the requirements prescribedin this specification may constitute

17、 grounds for rejection. In thecase of rejection, the seller shall have the right to reinspect therejected material and resubmit the lot after removal of thosepackages not conforming to the requirements.9. Packaging and Package Marking9.1 Unless otherwise agreed upon, all products shall bepackaged an

18、d labeled in accordance with applicable regula-tions. Each package shall be marked to indicate the applicabletype and ASTM specification.10. Keywords10.1 adhesive; coal tar; peel strength; shear strengthASTM International takes no position respecting the validity of any patent rights asserted in con

19、nection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the respon

20、sible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful

21、consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 1

22、00 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM

23、website(www.astm.org).TABLE 1 Requirements for Coal Tar AdhesiveAType I Type IINon-volatile matter, % min 73 60Water, % max. 2.0 3Ash (% of nonvolatile matter), min. 4 12Lap shear strength, min, kN/m 24 h 72 h 7 days 28 days 24 h 72 h 7 days 28 daysConditioned and tested at 10C (50F) 25 60 MFBMF 60

24、65 MF MFConditioned and tested at 25C (77F) 15 40 70 MF 70 75 MF MFConditioned at 60C (140F) and tested at 32C (90F) 6 15 20 MF 25 30 MF MFPeel strength min, kN/m 24 h 72 h 7 days 28 days 24 h 72 h 7 days 28 daysConditioned and tested at 10C (50F) 0.25 0.45 0.81 1.75 0.50 0.70 2.80 2.90Conditioned and tested at 25C (77F) 0.20 0.50 0.95 2.50 0.80 2.0 5.50 7.0Conditioned at 60C (140F) and tested at 32C (90F) 0.40 1.36 2.0 2.10 2.40 2.50 2.80 3.00AValues in table developed with a coal tar modified bitumen sheet adhered to itself.BMF denotes substrate failure.D 6753 02 (2008)2