ASTM D7733-2012(2016) 3017 Standard Specification for Acrylic Dispersion Ground《丙烯酸分散地的标准规格》.pdf

1、Designation: D7733 12 (Reapproved 2016)Standard Specification forAcrylic Dispersion Ground1This standard is issued under the fixed designation D7733; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A numb

2、er in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This standard specifies test methods which measureminimum qualities for acrylic dispersion grounds.1.2 The values stated in SI units are to

3、 be regarded as thestandard. The values given in parentheses are for informationonly.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices an

4、d determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D1640 Test Methods for Drying, Curing, or Film Formationof Organic CoatingsD3359 Test Methods for Measuring Adhesion by Tape Test3. Terminology3.1 Definitions:3.1.1 flash-through, nthe vi

5、sible evidence of oil on theopposite side of a support to which it was applied; also referredto as strike-through.3.1.2 gesso grounds, n:3.1.2.1 calcium hydroxide and water (“slaked lime”).3.1.2.2 calcium sulfate (“plaster of Paris”) or calcium car-bonate (chalk) prepared with a natural protein glue

6、 water.3.1.2.3 in contemporary usage, the term “gesso” is some-times used by manufacturers of acrylic dispersion products todescribe their products in a brand name.3.1.3 ground, na surface onto which an artist appliesdecorative coatings and paints.3.1.4 polymer, na long chain synthetic or naturally

7、occur-ring molecule composed of smaller, repeating units calledmonomers.3.1.5 size, na liquid material that absorbs and penetratesinto a substrate preparing the substrate for a primer or groundby at least partially sealing the surface and creating moreintegrity and less absorption of the surface.3.1

8、.6 strike-through, nsee flash-through.4. Significance and Use4.1 This specification establishes quality and performancerequirements and provides a basis for common understandingamong producers, distributors and users.4.2 It is not intended that all grounds meeting this require-ment be identical nor

9、have uniform excellence in all respects.Variation in manufacture not covered in this specification maycause some artists to prefer one brand to another, either ofwhich may be acceptable by this specification.5. Labeling Requirements5.1 Acrylic dispersion products conforming to this standardwill incl

10、ude acrylic, polymer, dispersion polymer, or acrylicdispersion in their description to differentiate them fromtraditional gessoes.6. Quality Assurance6.1 Conditions not covered in this specification that affectthe quality of acrylic dispersion grounds:6.1.1 SubstrateFactors such as the texture, glos

11、s, effectivepH, porosity, chemical composition and condition of thesubstrate will affect gloss, gloss uniformity, drying time,adhesion and the flexibility of the dried ground.6.1.2 Environmental ConditionsFactors such astemperature, humidity, airflow and light conditions affectapplication properties

12、, film formation, drying time and adhe-sion.6.1.3 StorageFactors such as aging and high and lowtemperatures may cause changes in consistency.6.2 Wet Ground Properties:6.2.1 Viscosity/ConsistencyGrounds shall be smooth andconsistent except for functional particles that provide tooth.Paste type ground

13、s may not flow or level; ready to brushgrounds will flow evenly.1This specification is under the jurisdiction of ASTM Committee D01 on Paintand Related Coatings, Materials, and Applications and is the direct responsibility ofSubcommittee D01.57 on Artist Paints and Related Materials.Current edition

14、approved July 1, 2016. Published July 2016. Originally approvedin 2012. Last previous edition approved in 2012 as D7733 12. DOI: 10.1520/D773312R16.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandar

15、ds volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States16.2.2 pHThe pH shall be 7.0 to 10.0.6.2.3 Fineness of Dispersion (Grind)Grind will vary andmay cont

16、ain coarse particles for adhesion, promoting thefunctional tooth of the dry ground.6.2.4 Freeze-Thaw StabilityUsing a freezer that has atemperature of -7C (20F) or lower, subject the ground to fivefreeze thaw cycles. A freeze thaw cycle shall consist offreezing the ground to a solid state (minimum 1

17、8 h) and thenthawing the ground (minimum of 5 h) to room temperature,22 6 2C (72 6 5F). The ground shall then meet therequirements of 6.2, 6.3, 6.4.6.2.5 DryingUse a 6 mil film applicator (drawdown bar)to make a uniform drawdown on a lacquer sealed card or panel.At a relative humidity of 50 to 75 %

18、and at a temperature of 18to 27C (65 to 80F) the dust free drying time determined inaccordance with Test Methods D1640 shall be not less than 10min.6.3 Dry Properties:6.3.1 Adhesion by Test Methods D3359Measuring Adhe-sion by Tape Test.6.3.2 Painting Media on the GroundTesting adhesion ofartist acry

19、lic and oil paints, and each type of painting media, tothe ground shall achieve a classification of 5B when tested inaccordance with Test Methods D3359.6.3.3 Ground on SubstrateTesting adhesion of the ground/substrate interface shall achieve a classification of 5B whentested in accordance with Test

20、Methods D3359.6.4 Oil Hold Out by Described Method:6.4.1 Scope:6.4.1.1 This test method is to determine oil absorption andpenetration into an acrylic dispersion ground. The procedure isqualitative and the test will result in a pass/fail determination.6.4.2 Significance and Use:6.4.2.1 The oxidation

21、of drying oils used in artists mediacontributes to the embrittlement and degradation of naturalfibered substrates. One attribute of the acrylic dispersionground is to prevent the penetration of oil into the substratewhile also providing adequate absorbency to promote adhesionof the oil media.6.4.3 A

22、pparatus:6.4.3.1 Eye-dropper.6.4.4 Reagents and Materials:6.4.4.1 Unless otherwise indicated, references to oil shall beunderstood to mean raw alkali-refined linseed oil.6.4.5 Procedure:6.4.5.1 Test substrates shall be untreated stretched #10cotton duck canvas on stretcher bars that allow for open b

23、ackaccess to the canvas. Prepare the stretched canvas by evenbrush application of the ground. Create a matrix of layers thatallow a 15 by 15 cm (6 by 6 in.) test area of single, double andtriple coats of the ground. Each coat shall dry for a minimumof 24 h before application of the subsequent coat.6

24、.4.5.2 Apply three drops of raw alkali-refined linseed oilvia eyedropper to the center of each of the 15 by 15 cm (6 by6 in.) test areas. Each drop shall be .025 6 .00125 ml, withtotal volume for the three drops equaling .075 6 .00375 ml.The eyedropper can be any type, available in any pharmacy.6.4.

25、5.3 Oil PenetrationSix week after the oil has beenapplied, observe the oil drops. For penetration, observe theback side of the canvas. There must be no evidence of the oilflashing through the three-coat section.6.4.5.4 Oil AbsorptionSix weeks after the oil has beenapplied, observe the front side of

26、the canvas. The oil dropsmust not be dried as a bead on the surface: there should besome absorption of the oil into the surface, leaving the surfaceslightly glossier than the ground and having some visualevidence of the oil still remaining on the surface. The oil shallnot have wicked or bled more th

27、an five times the originaldrops area (5 to 7 cm).6.4.6 Report:6.4.6.1 Report the following information:6.4.6.2 The evidence or lack of evidence of flash-through.6.4.6.3 The evidence or lack of evidence of the oil drophaving dried as a bead on the surface.6.4.6.4 The evidence or lack of evidence of o

28、il spreadwithin or beyond the proscribed area.6.4.7 Precision and Bias:6.4.7.1 No information is presented about either the preci-sion or bias for measuring oil hold out by described methodsince the test results are nonquantitative.6.5 Flexibility by Described Method:6.5.1 Scope:6.5.1.1 This test me

29、thod is to determine adequate flexibilityand resistance to cracking of the acrylic dispersion ground oncanvas. The procedure is qualitative and the test will result ina pass/fail determination.6.5.2 Significance and Use:6.5.2.1 Canvas coated with acrylic dispersion grounds areexpected to resist crac

30、king when placed under stress and strainduring preparation, storage, and handling.6.5.3 Procedure:6.5.3.1 Test substrates shall be untreated stretched #10cotton duck canvas on stretcher bars that allow for open backaccess to the canvas. The cotton duck may not be sized afterstretching. Prepare the s

31、tretched canvas by even brush appli-cation of two coats of the ground allowing adequate dryingtime between coats.6.5.3.2 After the canvas has dried for a minimum of twoweeks, carefully remove the canvas from the stretcher bars.Allow the canvas to acclimate for a minimum of1hinanenvironment of 20 to

32、22.2C (68 to 72F) and 25 to 35 % RH,carefully take the acclimated canvas and bend it over a sharp90-degree corner. Repeat this test ten times, using a new areaof the prepared canvas and being careful not to handle the areasof the canvas intended to be bent for testing. There shall be nocracking of t

33、he ground in all ten attempts.6.5.4 Report:6.5.4.1 Report the following information:6.5.4.2 The evidence or lack of evidence of cracking of theground.6.5.5 Precision and Bias:6.5.5.1 No information is presented about either the preci-sion or bias for measuring flexibility by described method sinceth

34、e test results are nonquantitative.D7733 12 (2016)27. Keywords7.1 acrylic; dispersion polymer; gesso; ground; oil hold out;polymer; primerASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this st

35、andard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years a

36、ndif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee,

37、 which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-29

38、59,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 12 (2016)3